CN101205436B - Novel aqueous insulation paint - Google Patents

Novel aqueous insulation paint Download PDF

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Publication number
CN101205436B
CN101205436B CN2007101952897A CN200710195289A CN101205436B CN 101205436 B CN101205436 B CN 101205436B CN 2007101952897 A CN2007101952897 A CN 2007101952897A CN 200710195289 A CN200710195289 A CN 200710195289A CN 101205436 B CN101205436 B CN 101205436B
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CN
China
Prior art keywords
coating
thermal insulation
insulation coatings
emulsion
hollow beads
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Expired - Fee Related
Application number
CN2007101952897A
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Chinese (zh)
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CN101205436A (en
Inventor
宋德强
田辉
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Beijing Shijibaicheng Decoration Engineering Co Ltd
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Beijing Shijibaicheng Decoration Engineering Co Ltd
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Priority to CN2007101952897A priority Critical patent/CN101205436B/en
Publication of CN101205436A publication Critical patent/CN101205436A/en
Application granted granted Critical
Publication of CN101205436B publication Critical patent/CN101205436B/en
Expired - Fee Related legal-status Critical Current
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Abstract

The invention relates to a water thermal-insulation paint used in constructions, comprising the following raw materials: ceramic hollow micro bead, emulsion, latent solvent, filler, pigment, wetting agent, dispersing agent, thickening agent, antifoam agent, germicide and water. The ceramic hollow micro bead, which is added in the paint, can form a paper-thin enclosed hollow cavity layer when coated on the surface of a building, thereby effectively preventing thermal conduction and thermal radiation.

Description

Novel aqueous insulation paint
Technical field
Design building material of the present invention field, aqueous insulation paint field, particularly a kind of house
Background technology
Under country set up advocating of conservation-minded society and guides, every profession and trade all in research energy-conservation novel method, novel process, because coating application technology is simple, can realize jointless construction, reduces the existence of heat bridge in recent years, and the research of thermal insulation coatings becomes focus.
Thermal insulation coatings generally is divided into two classes: 1, the isolation-type thermal insulating coating is that high thermal resistance by coating self realizes heat insulation a kind of coating.Be to belong to thick film coating.Be coated with during coating application and dress up certain thickness, be generally 5-20mm, after solidifying through thorough drying, because thermal conductivity is very little behind the material drying and forming-film, so coating has the ability that certain hot-fluid that slows down transmits.2, reflective heat-insulation paint is development and come on the basis of aluminium base reflection and heat insulation coating, by selecting appropriate resin, metal or metal oxide color stuffing and production technique, makes the coating of high-reflectivity, and the reflection solar heat is to reach heat insulation purpose.
The thermal insulation coatings of isolation-type is present most widely used thermal insulation coatings, belongs to the silicates composite coating, and this class coating is a class novel heat insulation material that grows up late 1980s.This heat preserving and insulating material principle of work is to form one " air bag " to be used for preventing thermal conduction.Air is a heat conducting material of very good opposing, but he does not stop thermal radiation.He will reach basic unit with heat in case this absorbed heat reaches capacity.There are last hundred tame research units and enterprise in China in the research work of carrying out this class coating, each factory is not quite similar to the address of product, as " composite aluminium-magnesium-silicate thermal insulating coating ", " rare earth thermal insulation coatings ", " application type composition silicate thermal insulating coating " etc., formulation for coating material, performance, constructional method are different,, waterproof hydrophobic etc. hard as fast dried speed also has nothing in common with each other, and is coating but all belong to silicate.As the publication number insulating rare earth composite coatings production method that is that CN1113259A discloses a kind of (rapid-curing cutback), CN 1080939 A disclose a kind of with the perlite asbestos powder, high-temp glue, slag wool, rock wool is the production method of the composite heat insulation coating of main component, CN 1087663 A disclose a kind of hydrophobic nature compound silicate insulating paint production technique, CN 1094080 A disclose by asbestos wool, it is a kind of by hollow silicon that a kind of insulating rare earth composite coatings that aluminum silicate fiber is made, the patent No. are that ZL 02132991.5 discloses, the compound building thermal-insulating coating that forms of diatomite etc.This class coating is experiencing one by the transformation of industrial heat-insulation and heat-preservation to building heat insulation now, but because the defective that existence self material structure brings, as coated bed thickness, drying cycle is long, and construction is subjected to season and weather effect big, a little less than the impact resistance, dry shrinkage is big, rate of moisture absorption is big, remains further to be improved etc. to the cohesive strength of body of wall is on the low side and ornamental, is used for the external wall application so this class thermal insulating coating is still less.
Existing reflective heat-insulation paint is development and come on the basis of aluminium base reflection and heat insulation coating, by sheet metal being carried out special processing or not adopting the water-based reflective heat-insulation paint of sheet metal to become one of focus of domestic and international thermal insulating coating research.Publication number is that the patent of invention of CN 1810900 A discloses a kind of method that the altar legal system is equipped with reflection type thermal insulation coating of rolling, by selecting appropriate resin, metal or metal oxide face, filler and production technique, make highly reflective coatint, reflected sunlight reaches heat insulation purpose.Its mechanism of heat insulation mainly is because metal or metal oxide for the heat reflectivity height, can effectively reduce radiative transfer and transmission of heat by convection.But this coating material production time is long, and the metal mold coating is affected by environment huge, and dust, acid rain all can have tremendous influence to this coating property.Publication number is that to disclose a kind of be the thermal insulation coatings of addition material with the hollow glass micropearl to the patent of invention of CN 1986664 A, can reduce multiple body surface, reduce its surface temperature and internal temperature, thereby improve Working environment, reach energy saving purposes, but existing hollow glass micropearl and water infiltration ability are difficult to dispersion and are storing central segregation easily in coating, poor durability be pasted not strongly coated with the back with basic unit.Publication number is that the patent of invention of CN1995250A discloses with the ceramic hollow microballon is a kind of thermostable heat-isolating coating of addition material, be applied to high temperature equipment places such as oil, chemical industry, metallurgy, electric power, to keep comparatively high temps in the higher reflecting device, its main range of application is a hot industry coating, because its reflective infrared wave band is higher, heat-insulating capability is also not obvious at normal temperatures.
The present invention mainly is suspended in by some small ceramic hollow particles to have superior heat resistance, constitutes in the acrylic emulsion of weathering resistance, corrosion-resistant and water resistance and the water-base fluorocarbon emulsion, has high-reflectivity, high radiant rate, low thermal conductivity, thermal property such as low heat storage coefficient and it is imposed on the leakage problems that can reduce roof maintenance and displacement expense on the building waterproof layer and can solve roofing.Reflection, refraction and the scattering of thermal insulation coatings utilization pottery hollow beads get mode and stop thermal radiation, and the hollow cavity that utilizes hollow beads to form stops thermal conduction.Be a kind of water-based, height adhere to, easily dry, can toning, the coating of long lifetime, heat insulation, insulation, moistureproof, environmental protection.
Summary of the invention
The novel aqueous insulation paint that The present invention be directed to the prior art deficiency and provide, the grating hollow ceramic particle that adds in this coating is blended in and has formed hollow cavity layer as thin as a wafer in the coating after being coated in building surface, has constituted effective thermodynamic barrier.This ceramic particle not only self thermal resistance is big, and thermal conductivity is low, and the heat reflectivity height, reduces the absorption of buildings to solar radiant heat.The remarkable resistance of transmitting by reinforcing reflex solar heat and convection current can reduce radiative transfer and heat transfer by conduction effectively like this, thereby reduces lining surface and internal space temperature.
Coating of the present invention has formed hollow cavity layer as thin as a wafer after being coated in the building surface drying, has constituted effective thermodynamic barrier.This ceramic particle not only self thermal resistance is big, and thermal conductivity is low, and the heat reflectivity height.The heat energy that is to say part when thermal radiation enters buildings and collides these hollow ceramic particles is reflected back, thereby reaches the inside and outside heat exchange of control buildings, increases the heat insulating ability of whole buildings, has reduced the consumption of the energy significantly.
The hollow ceramic microballon is to be formed by 45~150 microns gratings, and closely knit coated with the hollow cavity layer as thin as a wafer that the back forms, resistance to impact shock is big, the reflectivity height, and it is wide that the light that is reflected covers wave band, and heat-insulating capability is strong.
The hollow ceramic microballon is handled through hydrophilic surface, and is big with the avidity of water, and extraordinary wetting capacity is arranged, and it is central not easily separated with matrix to add coating to, and the coating film forming ability of institute's modification is good.
The hollow ceramic microballon is to adopt by being rich in compounded hollow beads such as metallic element silicon, aluminium, titanium, and extremely low heat storage capacity is arranged, and the variation of the temperature difference is constant to its influence, thereby weather resistance improves greatly.
This hollow ceramic microballon has very high unreactiveness and ultimate compression strength, and the variation of external environment is little to itself performance impact.
Hollow ceramic microballon color is light grey, can the color of coating itself not exerted an influence, but the color of coating can have very big influence for Energy efficiency.When can not noting selecting emulsion paint, most of people consider the influence of painting color for the energy.The dark refrigeration expense that can increase you in summer is because the thermal efficiency ratio of dark painting color is lower.But this does not represent that you can not select dark coating for use.Invention utilizes reflection, refraction and the scattering of ceramic hollow beads to get mode to stop thermal radiation, obtain sun power thereby the hollow cavity that utilizes hollow beads to form stops thermal conduction to reduce.Even you select dark color for use in other words, also can be than using common coating to reduce the consumption of the energy.
The present invention has reduced water vapour in surface condensation in heat insulating, thereby has stoped mould and gone mouldy.The dark moist place of mould-growth and breeding, these can both support their growth on timber, paper, cabinet, the food.The present invention can reduce moisture on house sidings and the gathering of top ceiling.The present invention can prevent mould basically and go mouldy because it has good protection against the tide and prevents the effect of hydrogenesis, thereby eliminate mould and the key factor-humidity of the propagation of going mouldy.
The present invention can be reflected, refraction, scattering thermal radiation and stop heat conducting coating, and the ceramic microspheres reflective qualities influences Greenhouse effect, and this hollow beads is just as small one by one thermos flask.Winter it intercepting when freezing air imports into, can reflect the heat that your domestic heating is sent, thereby your family's temperature is risen rapidly and can save energy.
The object of the present invention is achieved like this:
A kind of aqueous insulation paint for building is made up of following main raw material: ceramic hollow beads, water, emulsion, solubility promoter, filler, pigment, wetting base, dispersion agent, thickening material, defoamer and sterilant.It respectively forms content (by weight):
(1) ceramic hollow beads 5~20%
(2) emulsion 20~40%
(3) solubility promoter 5~20%
(4) filler 5~40%
(5) pigment 5~40%
(6) wetting agent 0.1~1%
(7) dispersion agent 0.1~2%
(8) thickening material 0.5~4%
(9) defoamer 0.01~1%
(10) sterilant 0.01~1%
(11) water 5~20%
Its principal character is to have added ceramic hollow beads in the described coating, and ceramic hollow beads has formed hollow cavity layer as thin as a wafer after being coated in building surface, can effectively stop the conduction and the radiation of heat.
Described ceramic hollow beads is 45~150 microns grating microballons of particle diameter, can effectively improve the density of material, thereby the degree of compactness of increase coated surface has improved the heat reflectivity and the resistance to impact shock of coated surface.
The thermal conductivity of described ceramic hollow beads is 0.04~0.08W/m.K.
The heat reflectivity of described ceramic hollow beads is greater than 80%.
The specific refractory power of described ceramic hollow beads is 1.53.
The major metal element of described ceramic hollow beads is silicon, aluminium, titanium elements.
Described thermal insulation coatings emulsion is one or more in pure-acrylic emulsion, benzene emulsion, acrylate and vinyl acetate emulsion, organosilicon crylic acid latex, the fluorine carbon emulsion.
Described thermal insulation coatings solubility promoter is ethylene glycol or propylene glycol.
The filler of described thermal insulation coatings is one or more in coarse whiting, fine particle calcium carbonate, process white, talcum powder, mica powder, kaolin, silica powder, the wollastonite powder.
The wetting agent of described thermal insulation coatings is one or more in alkyl aryl polyether, polyoxyethylene alkyl aryl ether, polyethoxye nonyl phenol, alkyl amber sodium sulfonate, the polyxyethylated alkylphenol.As Triton CF-10, Triton X-405, Hyonic PE-100, Hydropalat 875, OP-10 etc.
The dispersion agent of described thermal insulation coatings is one or more among poly-phosphate, polyacrylate, polystyrene/maleic acid salt, polyisobutene diacid salt or the AMP-95.As SN-5040, Tamol 731, Disperbyk 154, Disper A40, Disper N40, DA, Sodium hexametaphosphate 99, Calgon N, HX-5320, HX-5310 etc.
The thickening material of described thermal insulation coatings is one or more in ether of cellulose and derivative thereof, polyacrylic ester, the urethane.As Natvosol, methyl hydroxyethylcellulose, methylhydroxypropylcellulose, methylcellulose gum, ASE-60, TT-615, TT-935, RM-8W etc.
The pigment of described thermal insulation coatings is one or more in mineral dye and the pigment dyestuff.Form as titanium dioxide, zinc sulfide white, zinc oxide, stibium trioxide and shades of colour color paste deployment.
The defoamer that described thermal insulation coatings uses is among silicone oil, siloxanes-polyester copolymer, organophosphate, the lipid acid one or more.
Described thermal insulation coatings sterilant is one or more in isothiazole ketone, benzimidazole class, the substituted arene class.As Proxel GXL, Troysan586, fungicidal preservative PT, Kathon LEX, Hua Ke-88, Acticide HF, WS-44, Troysan174 etc.
The coating thickness of described thermal insulation coatings is 0.1~5mm.
Embodiment
Preparation of the present invention may further comprise the steps:
(1) solubility promoter, dispersion agent, wetting agent, sterilant, defoamer are put into portion water, stirring velocity is 800~1200r/min, stirs 10~30min;
(2) add mineral dye and filler, stirring velocity is 1200~2000r/min, stirs 30~550 it is uniformly dispersed;
(3) stirring velocity is reduced to 600~1000r/min, adds emulsion and portion water, stir 10~30min;
(4) keep stirring velocity constant, add ceramic hollow beads;
(5) add thickening material and regulate the coating denseness, make it reach application standard, and regulate painting color as requested.
Embodiment 1:
Select raw material for use according to following tabulation, preparation process is (1000g) as mentioned above:
Raw material Model Consumption (g) Raw material Model Consumption
The pottery hollow beads 100 Wetting agent OP-10 2
Emulsion Pure third 300 Dispersion agent 5040 5
Solubility promoter Propylene glycol 18 Thickening material 8W 20
Filler Coarse whiting 150 Defoamer 345 2
Pigment Titanium dioxide 300 Sterilant HF 1
Water 102
Embodiment 2:
Embodiment 3:
Above embodiment is used for enumerating purpose, technology contents, characteristics and the effect that explanation is invented, the not limited thereto embodiment of protection domain of the present invention.

Claims (11)

1. an aqueous insulation paint for building is made up of following main raw material: ceramic hollow beads, emulsion, solubility promoter, filler, pigment, wetting agent, dispersion agent, thickening material, defoamer, sterilant and water.It respectively forms content (by weight):
(1) ceramic hollow beads 5~20%
(2) emulsion 20~40%
(3) solubility promoter 5~20%
(4) filler 5~40%
(5) pigment 5~40%
(6) wetting agent 0.1~1%
(7) dispersion agent 0.1~2%
(8) thickening material 0.5~4%
(9) defoamer 0.01~1%
(10) sterilant 0.01~1%
(11) water 5~20%;
Wherein, the major metal element of ceramic hollow beads is silicon, aluminium, titanium elements;
The ceramic hollow beads of being added is 45~150 microns grating microballons of particle diameter;
The heat reflectivity of pottery hollow beads is greater than 80%;
The specific refractory power of pottery hollow beads is 1.53.
2. according to right 1 described coating, wherein the thermal insulation coatings emulsion is one or more in pure-acrylic emulsion, benzene emulsion, acrylate and vinyl acetate emulsion, organosilicon crylic acid latex, the fluorine carbon emulsion.
3. according to right 1 described coating, wherein the thermal insulation coatings solubility promoter is ethylene glycol or propylene glycol
4. according to right 1 described coating, wherein the filler of thermal insulation coatings is one or more in coarse whiting, fine particle calcium carbonate, process white, talcum powder, mica powder, kaolin, silica powder, the wollastonite powder.
5. according to right 1 described coating, wherein the wetting agent of thermal insulation coatings is one or more in alkyl aryl polyether, polyoxyethylene alkyl aryl ether, polyethoxye nonyl phenol, alkyl amber sodium sulfonate, the polyxyethylated alkylphenol.
6. according to right 1 described coating, wherein the dispersion agent of thermal insulation coatings is one or more among poly-phosphate, polyacrylate, polystyrene/maleic acid salt, polyisobutene diacid salt or the AMP-95.
7. according to right 1 described coating, wherein the thickening material of thermal insulation coatings is one or more in ether of cellulose and derivative thereof, polyacrylic ester, the urethane.
8. according to right 1 described coating, wherein the pigment of thermal insulation coatings is one or more in mineral dye and the pigment dyestuff.
9. according to right 1 described coating, wherein the defoamer that uses of thermal insulation coatings is among silicone oil, siloxanes-polyester copolymer, organophosphate, the lipid acid one or more.
10. according to right 1 described coating, wherein the thermal insulation coatings sterilant is one or more in isothiazole ketone, benzimidazole class, the substituted arene class.
11. according to right 1 described coating, wherein the coating thickness of thermal insulation coatings is 0.1~5mm.
CN2007101952897A 2007-12-06 2007-12-06 Novel aqueous insulation paint Expired - Fee Related CN101205436B (en)

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Application Number Priority Date Filing Date Title
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Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN2007101952897A CN101205436B (en) 2007-12-06 2007-12-06 Novel aqueous insulation paint

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CN101205436B true CN101205436B (en) 2010-06-02

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