CH124677A - Process for the preparation of a monoazo dye. - Google Patents
Process for the preparation of a monoazo dye.Info
- Publication number
- CH124677A CH124677A CH124677DA CH124677A CH 124677 A CH124677 A CH 124677A CH 124677D A CH124677D A CH 124677DA CH 124677 A CH124677 A CH 124677A
- Authority
- CH
- Switzerland
- Prior art keywords
- dye
- preparation
- red
- monoazo dye
- amino
- Prior art date
Links
- 238000000034 method Methods 0.000 title claims description 4
- NYGZLYXAPMMJTE-UHFFFAOYSA-M metanil yellow Chemical group [Na+].[O-]S(=O)(=O)C1=CC=CC(N=NC=2C=CC(NC=3C=CC=CC=3)=CC=2)=C1 NYGZLYXAPMMJTE-UHFFFAOYSA-M 0.000 title claims description 3
- 238000002360 preparation method Methods 0.000 title claims description 3
- 239000000975 dye Substances 0.000 claims description 7
- 238000004043 dyeing Methods 0.000 claims description 3
- 239000000835 fiber Substances 0.000 claims description 3
- 239000000843 powder Substances 0.000 claims description 2
- 239000001054 red pigment Substances 0.000 claims description 2
- 239000000987 azo dye Substances 0.000 claims 1
- 239000000758 substrate Substances 0.000 claims 1
- HEMHJVSKTPXQMS-UHFFFAOYSA-M sodium hydroxide Inorganic materials [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 5
- IISBACLAFKSPIT-UHFFFAOYSA-N bisphenol A Chemical group C=1C=C(O)C=CC=1C(C)(C)C1=CC=C(O)C=C1 IISBACLAFKSPIT-UHFFFAOYSA-N 0.000 description 1
- 238000004090 dissolution Methods 0.000 description 1
- 239000002244 precipitate Substances 0.000 description 1
- 239000001044 red dye Substances 0.000 description 1
- UIIMBOGNXHQVGW-UHFFFAOYSA-N sodium;hydron;carbonate Chemical compound [Na+].OC(O)=O UIIMBOGNXHQVGW-UHFFFAOYSA-N 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Landscapes
- Coloring (AREA)
Description
Verfahren zur Darstellung eines Monoazofarbstoffes. Es wurde gefunden, dass man einen wert vollen roten Farbstoff erhält, wenn man diazotiertes p-T'oluolsulfon-methylamino-2- amino-4-chlorbenzol (p-Toluolsulfo-2-amino- 4-chlormethylanilid) mit 2-Oxynaphtalin-3- carbonsäure - a - naphtylamid kuppelt. Der Farbstoff kann sowohl in ,Substanz, als auch auf einer Grundlage erzeugt werden.
Der Farbstoff bildet getrocknet ein rotes Pulver; auf der Faser liefert er rote Färbungen von vorzüglicher Wasch-, Soda- und Laugeecht- heit und sehr guter Lichtechtheit.
<I>Beispiel:</I> 6,2 Gewichtsteile p-Toluolsulfon-methyl- amino-2-amino-4-chlorbenzol werden diano tiert. Der erhaltene Brei wird eingerührt in eine Auflösung, bereitet aus 7,5 Gewichts teilen 2-Oxynaphtalin-3-carbonsäure-a-naph- tylamid, 400 Gewichtsteilen Wasser und 10 Gewichtsteilen Natronlauge 40' B6.
Es entsteht ein roter Niederschlag, der abfiltriert und getrocknet werden kann. Der Farbstoff kann als roter Pigment- farbstoff verwendet werden; er liefert auf der Faser rote Färbungen von vorzüglicher Echtheit.
Process for the preparation of a monoazo dye. It has been found that a valuable red dye is obtained if diazotized p-toluenesulfonemethylamino-2-amino-4-chlorobenzene (p-toluenesulfo-2-amino-4-chloromethylanilide) with 2-oxynaphthalene-3 - carboxylic acid - a - naphthylamide couples. The dye can be produced both in substance and on a base.
The dye forms a red powder when dried; On the fiber it provides red dyeings with excellent wash, soda and lye fastness and very good light fastness.
<I> Example: </I> 6.2 parts by weight of p-toluenesulfone-methyl-amino-2-amino-4-chlorobenzene are diano tated. The resulting paste is stirred into a dissolution prepared from 7.5 parts by weight of 2-oxynaphthalene-3-carboxylic acid-a-naphthylamide, 400 parts by weight of water and 10 parts by weight of sodium hydroxide solution 40 'B6.
A red precipitate forms, which can be filtered off and dried. The dye can be used as a red pigment dye; it produces red dyeings of excellent fastness on the fiber.
Claims (1)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE124677X | 1925-07-07 | ||
| CH122069T | 1926-07-06 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CH124677A true CH124677A (en) | 1928-02-16 |
Family
ID=25709850
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CH124677D CH124677A (en) | 1925-07-07 | 1926-07-07 | Process for the preparation of a monoazo dye. |
Country Status (1)
| Country | Link |
|---|---|
| CH (1) | CH124677A (en) |
-
1926
- 1926-07-07 CH CH124677D patent/CH124677A/en unknown
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