CH103142A - Process for the production of a new indigoid dye. - Google Patents

Process for the production of a new indigoid dye.

Info

Publication number
CH103142A
CH103142A CH103142DA CH103142A CH 103142 A CH103142 A CH 103142A CH 103142D A CH103142D A CH 103142DA CH 103142 A CH103142 A CH 103142A
Authority
CH
Switzerland
Prior art keywords
production
new
indigoid dye
dye
brown
Prior art date
Application number
Other languages
German (de)
Inventor
Gesellschaft Fuer Chemis Basel
Original Assignee
Chem Ind Basel
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Chem Ind Basel filed Critical Chem Ind Basel
Publication of CH103142A publication Critical patent/CH103142A/en

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
    • C09B7/00—Indigoid dyes
    • C09B7/12—Other thionaphthene indigos

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Coloring (AREA)

Description

  

      Verfahren    zur Herstellung eines neuen     indigoiden        Farbstoffes.       Es wurde gefunden, dass man einen neuen       indigoiden        Farbstoff    erhält, wenn man das       5-Chlor-2    .     1-thionaphthisatin,    welches durch  Kondensieren von     5-Chlor-2-thionaphthol    mit       Oxalylchlorid    erhalten werden kann, mit     Ace-          naphthenon    kondensiert.  



  Der neue Farbstoff stellt ein braunes Pul  ver dar und löst sich in     konz.    Schwefelsäure  mit blauer Farbe. Er bildet eine gelbbraune       Küpe    und färbt Baumwolle sehr echt in reinen  braunen Nuancen.  



  <I>Beispiel:</I>  248,5 Teile     5-Chlor-2    .     1-thionaphthisatin,     168 Teile     Acenaphthenon    und 200 Teile Zink  chlorid werden in 2000 Teilen Chlorbenzol  mehrere Stunden rückfliessend gekocht. Nach    dem Erkalten wird filtriert; der ausgeschie  dene Farbstoff mit Alkohol gewaschen und  getrocknet.



      Process for the production of a new indigoid dye. It has been found that a new indigoid dye is obtained if the 5-chloro-2. 1-thionaphthisatin, which can be obtained by condensing 5-chloro-2-thionaphthol with oxalyl chloride, condensed with acenaphthenone.



  The new dye is a brown powder and dissolves in conc. Sulfuric acid of blue color. It forms a yellow-brown vat and dyes cotton very realistically in pure brown shades.



  <I> Example: </I> 248.5 parts of 5-chloro-2. 1-thionaphthisatin, 168 parts of acenaphthenone and 200 parts of zinc chloride are refluxed for several hours in 2000 parts of chlorobenzene. After cooling, it is filtered; the excreted dye washed with alcohol and dried.

Claims (1)

PATENTANSPRUCH: Verfahren zur Herstellung eines neuen in- digoidenFarbstoffes, dadurch gekennzeichnet, dass man 5-Chlor-2 .1-thionaphthisatin mit Acenaphthenon kondensiert. Der neue'Farbstoff stellt ein braunes Pul ver dar und löst sich in konz. Schwefelsäure mit. blauer Farbe. Er bildet eine gelbbraune Küpe und färbt Baumwolle sehr echt in rei nen braunen Nuancen. PATENT CLAIM: Process for the production of a new indigoid dye, characterized in that 5-chloro-2 .1-thionaphthisatin is condensed with acenaphthenone. The new dye is a brown powder and dissolves in conc. Sulfuric acid with. blue color. It forms a yellow-brown vat and dyes cotton very realistically in pure brown shades.
CH103142D 1922-11-18 1922-12-07 Process for the production of a new indigoid dye. CH103142A (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
CH100705T 1922-11-18
CH103142T 1922-12-07

Publications (1)

Publication Number Publication Date
CH103142A true CH103142A (en) 1924-01-16

Family

ID=25705823

Family Applications (1)

Application Number Title Priority Date Filing Date
CH103142D CH103142A (en) 1922-11-18 1922-12-07 Process for the production of a new indigoid dye.

Country Status (1)

Country Link
CH (1) CH103142A (en)

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