CA2335500A1 - Process for the production of an aqueous monoester peroxycarboxylic acid solution, the solution obtainable by this process, and its use as disinfectant - Google Patents

Process for the production of an aqueous monoester peroxycarboxylic acid solution, the solution obtainable by this process, and its use as disinfectant Download PDF

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Publication number
CA2335500A1
CA2335500A1 CA002335500A CA2335500A CA2335500A1 CA 2335500 A1 CA2335500 A1 CA 2335500A1 CA 002335500 A CA002335500 A CA 002335500A CA 2335500 A CA2335500 A CA 2335500A CA 2335500 A1 CA2335500 A1 CA 2335500A1
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CA
Canada
Prior art keywords
production
acid solution
peroxycarboxylic acid
solution
disinfectant
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
CA002335500A
Other languages
French (fr)
Other versions
CA2335500C (en
Inventor
Graham Carr
Alun P. James
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Solvay SA
Original Assignee
Solvay (Societe Anonyme)
Graham Carr
Alun P. James
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Solvay (Societe Anonyme), Graham Carr, Alun P. James filed Critical Solvay (Societe Anonyme)
Publication of CA2335500A1 publication Critical patent/CA2335500A1/en
Application granted granted Critical
Publication of CA2335500C publication Critical patent/CA2335500C/en
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C409/00—Peroxy compounds
    • C07C409/24—Peroxy compounds the —O—O— group being bound between a >C=O group and hydrogen, i.e. peroxy acids
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
    • A01N37/16—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing the group; Thio analogues thereof
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C407/00—Preparation of peroxy compounds

Abstract

Process for the production of an aqueous monoester peroxycarboxylic acid solution by reaction of a peroxygen compound with at least one dicarboxylic acid and with at least one alcohol optionally in the presence of an acid catalyst. Aqueous monoester peroxycarboxylic acid solution obtainable by this process. Use of the aqueous monoester peroxycarboxylic acid solution as disinfectant.

Claims (5)

1 - Process for the production of an aqueous monoester peroxycarboxylic acid solution by reaction of a peroxygen compound with at least one polycarboxylic acid and with at least one alcohol optionally in the presence of an acid catalyst.
2 - Process according to claim 1, wherein the polycarboxylic acid is a dicarboxylic acid containing up to 20 carbon atoms, and wherein the dicarboxylic acid is used in an amount from 0,05 to 65 % wt.
3 - Process according to claim 1 or 2, wherein the peroxygen compound is chosen from hydrogen peroxide, inorganic peracids, organic peracids, persalts, wherein the peroxygen compound is used in an amount of 0,05 to 30 % wt of the reaction mixture.
4 - Process according to any one of claims 1 to 3, wherein the alcohol is chosen from monoalcohols, dialcohols and polyols containing up to 20 carbon atoms, wherein the alcohol is used in an amount from 0,05 to 45 % wt of the reaction mixture and wherein the molar ratio of alcohol to dicarboxylic acid is from 0,1 :1 to 10 :1.
5 - Process according to any one of claims 1 to 4, wherein an acid catalyst is used chosen from inorganic or organic acids having a Pka of 3 or lower, wherein the acid catalyst is used in an amount from 0,05 to 10 % wt of the reaction mixture.
CA2335500A 1998-06-22 1999-06-01 Process for the production of an aqueous monoester peroxycarboxylic acid solution, the solution obtainable by this process, and its use as disinfectant Expired - Fee Related CA2335500C (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP98304892A EP0967203A1 (en) 1998-06-22 1998-06-22 Process for the production of an aqueous monoester peroxycarboxylic acid solution, the solution obtainable by this process, and its use as disinfectant
EP98304892.7 1998-06-22
PCT/EP1999/003837 WO1999067213A1 (en) 1998-06-22 1999-06-01 Process for the production of an aqueous monoester peroxycarboxylic acid solution, the solution obtainable by this process, and its use as disinfectant

Publications (2)

Publication Number Publication Date
CA2335500A1 true CA2335500A1 (en) 1999-12-29
CA2335500C CA2335500C (en) 2010-05-25

Family

ID=8234886

Family Applications (1)

Application Number Title Priority Date Filing Date
CA2335500A Expired - Fee Related CA2335500C (en) 1998-06-22 1999-06-01 Process for the production of an aqueous monoester peroxycarboxylic acid solution, the solution obtainable by this process, and its use as disinfectant

Country Status (21)

Country Link
US (1) US6423868B1 (en)
EP (2) EP0967203A1 (en)
JP (1) JP4417563B2 (en)
KR (1) KR100646673B1 (en)
CN (1) CN1170818C (en)
AT (1) ATE248815T1 (en)
AU (1) AU747354B2 (en)
BR (1) BR9911431B1 (en)
CA (1) CA2335500C (en)
DE (1) DE69911016T2 (en)
HU (1) HUP0102465A3 (en)
IL (1) IL140391A (en)
MX (1) MXPA00012721A (en)
MY (1) MY117968A (en)
NO (1) NO326455B1 (en)
NZ (1) NZ509068A (en)
PL (1) PL194864B1 (en)
TR (1) TR200003829T2 (en)
UA (1) UA70329C2 (en)
WO (1) WO1999067213A1 (en)
ZA (1) ZA200007597B (en)

Families Citing this family (30)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6010729A (en) 1998-08-20 2000-01-04 Ecolab Inc. Treatment of animal carcasses
US7150884B1 (en) 2000-07-12 2006-12-19 Ecolab Inc. Composition for inhibition of microbial growth
US6514556B2 (en) 2000-12-15 2003-02-04 Ecolab Inc. Method and composition for washing poultry during processing
WO2002088076A2 (en) * 2001-03-09 2002-11-07 Ecolab Inc. Stabilized ester peroxycarboxylic acid compositions
US6627593B2 (en) * 2001-07-13 2003-09-30 Ecolab Inc. High concentration monoester peroxy dicarboxylic acid compositions, use solutions, and methods employing them
US7060301B2 (en) * 2001-07-13 2006-06-13 Ecolab Inc. In situ mono-or diester dicarboxylate compositions
US7029588B2 (en) * 2003-03-19 2006-04-18 Samuel Rupert Owens Oxidizing solution and process for contaminants
EP1550376A1 (en) 2003-12-29 2005-07-06 SOLVAY (Société Anonyme) Process for the disinfection and/or preservation of harvested plant material
WO2005070205A1 (en) 2004-01-09 2005-08-04 Ecolab Inc. Medium chain peroxycarboxylic acid compositions
US7504123B2 (en) 2004-01-09 2009-03-17 Ecolab Inc. Methods for washing poultry during processing with medium chain peroxycarboxylic acid compositions
US7887641B2 (en) 2004-01-09 2011-02-15 Ecolab Usa Inc. Neutral or alkaline medium chain peroxycarboxylic acid compositions and methods employing them
US8999175B2 (en) 2004-01-09 2015-04-07 Ecolab Usa Inc. Methods for washing and processing fruits, vegetables, and other produce with medium chain peroxycarboxylic acid compositions
US7507429B2 (en) 2004-01-09 2009-03-24 Ecolab Inc. Methods for washing carcasses, meat, or meat products with medium chain peroxycarboxylic acid compositions
US7771737B2 (en) 2004-01-09 2010-08-10 Ecolab Inc. Medium chain peroxycarboxylic acid compositions
ATE508756T1 (en) 2004-03-05 2011-05-15 Gen Probe Inc METHOD FOR DEACTIVATION OF NUCLEIC ACIDS
DE102004022392B4 (en) * 2004-05-06 2009-04-02 Gerhard Ruff Gmbh Disinfectant composition containing at least one peracid compound and their use for space and air disinfection
US7384787B2 (en) 2005-06-06 2008-06-10 Regents Of The University Of Minnesota Increasing perhydrolase activity in esterases and/or lipases
US7754670B2 (en) 2005-07-06 2010-07-13 Ecolab Inc. Surfactant peroxycarboxylic acid compositions
EP1860176A1 (en) * 2006-05-22 2007-11-28 Akzo Nobel N.V. Aqueous hydrogen peroxide-containing composition and its use for cleaning surfaces
US7547421B2 (en) 2006-10-18 2009-06-16 Ecolab Inc. Apparatus and method for making a peroxycarboxylic acid
US8075857B2 (en) 2006-10-18 2011-12-13 Ecolab Usa Inc. Apparatus and method for making a peroxycarboxylic acid
JP2010184869A (en) * 2009-02-10 2010-08-26 Mitsubishi Gas Chemical Co Inc Method for producing persuccinate-containing composition
EP2407529A1 (en) 2010-07-12 2012-01-18 Solvay SA Peroxygen composition
US8906963B2 (en) 2011-07-14 2014-12-09 Ecolab Usa Inc Deodorization of peracids
US8883848B2 (en) * 2011-07-14 2014-11-11 Ecolab Usa Inc. Enhanced microbial peracid compositions and methods of use at reduced temperatures in aseptic cleaning
US9752105B2 (en) 2012-09-13 2017-09-05 Ecolab Usa Inc. Two step method of cleaning, sanitizing, and rinsing a surface
US20140308162A1 (en) 2013-04-15 2014-10-16 Ecolab Usa Inc. Peroxycarboxylic acid based sanitizing rinse additives for use in ware washing
WO2015120216A1 (en) 2014-02-07 2015-08-13 Gojo Industries, Inc. Compositions and methods with efficacy against spores and other organisms
US9578879B1 (en) 2014-02-07 2017-02-28 Gojo Industries, Inc. Compositions and methods having improved efficacy against spores and other organisms
JP7334174B2 (en) 2018-02-14 2023-08-28 エコラボ ユーエスエー インコーポレイティド Compositions and methods for reducing biofilms and spores from membranes

Family Cites Families (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB9412051D0 (en) * 1994-06-16 1994-08-03 Solvay Interox Ltd Novel peroxygen compounds
EP0778270A1 (en) * 1995-12-06 1997-06-11 The Procter & Gamble Company Process for manufacturing monoperacids
GB9626637D0 (en) * 1996-12-21 1997-02-12 Solvay Interox Ltd Percarboxyilic acid solutions

Also Published As

Publication number Publication date
TR200003829T2 (en) 2001-07-23
AU747354B2 (en) 2002-05-16
AU4505699A (en) 2000-01-10
NO326455B1 (en) 2008-12-08
CN1313852A (en) 2001-09-19
DE69911016T2 (en) 2004-07-08
JP2002518476A (en) 2002-06-25
IL140391A0 (en) 2002-02-10
MY117968A (en) 2004-08-30
US6423868B1 (en) 2002-07-23
CN1170818C (en) 2004-10-13
NZ509068A (en) 2002-02-01
ATE248815T1 (en) 2003-09-15
KR100646673B1 (en) 2006-11-17
HUP0102465A2 (en) 2001-12-28
DE69911016D1 (en) 2003-10-09
IL140391A (en) 2004-08-31
JP4417563B2 (en) 2010-02-17
EP1089971A1 (en) 2001-04-11
KR20010053069A (en) 2001-06-25
CA2335500C (en) 2010-05-25
BR9911431A (en) 2001-03-20
WO1999067213A1 (en) 1999-12-29
EP0967203A1 (en) 1999-12-29
BR9911431B1 (en) 2010-07-13
PL345015A1 (en) 2001-11-19
ZA200007597B (en) 2001-12-18
HUP0102465A3 (en) 2003-02-28
NO20006606D0 (en) 2000-12-22
NO20006606L (en) 2001-02-01
MXPA00012721A (en) 2002-06-21
PL194864B1 (en) 2007-07-31
UA70329C2 (en) 2004-10-15
EP1089971B1 (en) 2003-09-03

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Effective date: 20130603