CA2234086A1 - Process for making a low density detergent compositon by agglomeration with an inorganic double salt - Google Patents
Process for making a low density detergent compositon by agglomeration with an inorganic double saltInfo
- Publication number
- CA2234086A1 CA2234086A1 CA002234086A CA2234086A CA2234086A1 CA 2234086 A1 CA2234086 A1 CA 2234086A1 CA 002234086 A CA002234086 A CA 002234086A CA 2234086 A CA2234086 A CA 2234086A CA 2234086 A1 CA2234086 A1 CA 2234086A1
- Authority
- CA
- Canada
- Prior art keywords
- detergent
- low density
- double salt
- agglomeration
- making
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000003599 detergent Substances 0.000 title abstract 8
- 238000000034 method Methods 0.000 title abstract 3
- 150000003839 salts Chemical class 0.000 title abstract 2
- 238000005054 agglomeration Methods 0.000 title 1
- 230000002776 aggregation Effects 0.000 title 1
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 abstract 2
- 239000000463 material Substances 0.000 abstract 2
- 239000002253 acid Substances 0.000 abstract 1
- 239000003945 anionic surfactant Substances 0.000 abstract 1
- 238000001035 drying Methods 0.000 abstract 1
- 239000007788 liquid Substances 0.000 abstract 1
- 239000002243 precursor Substances 0.000 abstract 1
- 229910000029 sodium carbonate Inorganic materials 0.000 abstract 1
- 239000004094 surface-active agent Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/02—Inorganic compounds ; Elemental compounds
- C11D3/04—Water-soluble compounds
- C11D3/10—Carbonates ; Bicarbonates
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D11/00—Special methods for preparing compositions containing mixtures of detergents
- C11D11/0082—Special methods for preparing compositions containing mixtures of detergents one or more of the detergent ingredients being in a liquefied state, e.g. slurry, paste or melt, and the process resulting in solid detergent particles such as granules, powders or beads
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D11/00—Special methods for preparing compositions containing mixtures of detergents
- C11D11/04—Special methods for preparing compositions containing mixtures of detergents by chemical means, e.g. by sulfonating in the presence of other compounding ingredients followed by neutralising
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D17/00—Detergent materials or soaps characterised by their shape or physical properties
- C11D17/06—Powder; Flakes; Free-flowing mixtures; Sheets
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Detergent Compositions (AREA)
Abstract
A process for continuously preparing low density detergent agglomerates having a density of below about 500 g/l is provided. The process comprises the steps of: (a) agglomerating a detergent surfactant paste or liquid acid precursor of anionic surfactant and dry starting detergent material in a high speed mixer to obtain detergent agglomerates, wherein the dry starting detergent material includes an inorganic double salt and sodium carbonate in a weight ratio of from about 1:10 to about 10:1; and (b) drying the detergent agglomerates so as to form the low density detergent composition having a density below about 600 g/l.
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US08/539,212 US5576285A (en) | 1995-10-04 | 1995-10-04 | Process for making a low density detergent composition by agglomeration with an inorganic double salt |
| US08/539,212 | 1995-10-04 | ||
| PCT/US1996/015648 WO1997012955A1 (en) | 1995-10-04 | 1996-10-01 | Process for making a low density detergent compositon by agglomeration with an inorganic double salt |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CA2234086A1 true CA2234086A1 (en) | 1997-04-10 |
| CA2234086C CA2234086C (en) | 2001-12-18 |
Family
ID=24150289
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CA002234086A Expired - Fee Related CA2234086C (en) | 1995-10-04 | 1996-10-01 | Process for making a low density detergent compositon by agglomeration with an inorganic double salt |
Country Status (10)
| Country | Link |
|---|---|
| US (1) | US5576285A (en) |
| EP (1) | EP0858500B1 (en) |
| JP (1) | JPH11512775A (en) |
| CN (1) | CN1111595C (en) |
| AR (1) | AR003789A1 (en) |
| AT (1) | ATE205251T1 (en) |
| BR (1) | BR9610810A (en) |
| CA (1) | CA2234086C (en) |
| DE (1) | DE69615042D1 (en) |
| WO (1) | WO1997012955A1 (en) |
Families Citing this family (38)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5756445A (en) * | 1993-11-11 | 1998-05-26 | The Proctor & Gamble Company | Granular detergent composition comprising a low bulk density component |
| US6207635B1 (en) * | 1995-05-31 | 2001-03-27 | The Procter & Gamble Company | Process for manufacture of high density detergent granules |
| GB9513327D0 (en) * | 1995-06-30 | 1995-09-06 | Uniliver Plc | Process for the production of a detergent composition |
| GB9526097D0 (en) * | 1995-12-20 | 1996-02-21 | Unilever Plc | Process |
| US5668099A (en) * | 1996-02-14 | 1997-09-16 | The Procter & Gamble Company | Process for making a low density detergent composition by agglomeration with an inorganic double salt |
| US6017873A (en) * | 1996-03-08 | 2000-01-25 | The Procter & Gamble Compnay | Processes for making agglomerated high density detergent composition containing secondary alkyl sulfate surfactant |
| CA2247499A1 (en) * | 1996-03-08 | 1997-09-12 | James Bert Royston | Agglomerated high density detergent composition containing secondary alkyl sulfate surfactant and processes for making same |
| WO1997043399A1 (en) * | 1996-05-14 | 1997-11-20 | The Procter & Gamble Company | Process for making a low density detergent composition by agglomeration followed by dielectric heating |
| BR9710558A (en) * | 1996-07-26 | 1999-08-17 | Procter & Gamble | Preparation of low density detergent agglomerates containing silica |
| BR9710559A (en) * | 1996-07-26 | 1999-08-17 | Procter & Gamble | Preparation of low density detergent agglomerates containing silica |
| WO1998008925A1 (en) * | 1996-08-26 | 1998-03-05 | The Procter & Gamble Company | Agglomeration process for producing detergent compositions involving premixing modified polyamine polymers |
| TW397862B (en) * | 1996-09-06 | 2000-07-11 | Kao Corp | Detergent granules and method for producing the same, and high-bulk density detergent composition |
| US6281188B1 (en) * | 1996-10-04 | 2001-08-28 | The Procter & Gamble Company | Process for making a low density detergent composition |
| US6156719A (en) * | 1996-10-04 | 2000-12-05 | The Procter & Gamble Company | Process for making a low density detergent composition by non-tower process |
| WO1999003964A1 (en) * | 1997-07-14 | 1999-01-28 | The Procter & Gamble Company | Process for making a low density detergent composition by controlled agglomeration in a fluid bed dryer |
| CA2296553C (en) * | 1997-07-14 | 2003-05-20 | Millard Sullivan | Process for making a low density detergent composition by controlling agglomeration via particle size |
| CA2296304C (en) | 1997-07-15 | 2003-05-27 | Scott William Capeci | Process for making high-active detergent agglomerates by multi-stage surfactant paste injection |
| WO2000003223A2 (en) * | 1998-07-08 | 2000-01-20 | Midwest Research Institute | Method for measuring volatile organic compounds and a kit for sa me |
| US20040110306A1 (en) * | 1998-07-08 | 2004-06-10 | Beimesch Wayne Edward | Method for measuring volatile organic compounds and a kit for same |
| US6440342B1 (en) | 1998-07-08 | 2002-08-27 | The Procter & Gamble Company | Process for making a low density detergent composition by controlling nozzle height in a fluid bed dryer |
| US6794354B1 (en) * | 1998-09-18 | 2004-09-21 | The Procter & Gamble Company | Continuous process for making detergent composition |
| DE19858859A1 (en) * | 1998-12-19 | 2000-06-21 | Henkel Kgaa | Production of storage-stable, homogeneous detergent optionally containing heavy components by agglomeration in a rotatable mixer with anionic surfactant introduced in acid form |
| US6596683B1 (en) | 1998-12-22 | 2003-07-22 | The Procter & Gamble Company | Process for preparing a granular detergent composition |
| EP1141229A1 (en) * | 1998-12-22 | 2001-10-10 | The Procter & Gamble Company | Process for making a low bulk density detergent composition by agglomeration |
| US6858572B1 (en) | 1999-03-09 | 2005-02-22 | The Procter & Gamble Company | Process for producing coated detergent particles |
| CN1343250A (en) * | 1999-03-09 | 2002-04-03 | 宝洁公司 | Process for producing coated detergent particles |
| US7022660B1 (en) | 1999-03-09 | 2006-04-04 | The Procter & Gamble Company | Process for preparing detergent particles having coating or partial coating layers |
| EP1159395B1 (en) * | 1999-03-09 | 2006-08-09 | The Procter & Gamble Company | Detergent particles having coating or partial coating layers |
| GB9927653D0 (en) * | 1999-11-22 | 2000-01-19 | Unilever Plc | Process for preparing granular detergent compositions |
| US20040014629A1 (en) * | 2002-07-17 | 2004-01-22 | Unilever Home & Personal Care Usa, Division Of Conopco, Inc. | Process for the production of detergent granules |
| US20080261857A1 (en) * | 2004-06-16 | 2008-10-23 | Henkel Kgaa | Targeted Granulation Achieved by Neutralisation in a Compomix-Type Machine |
| JP2008521995A (en) * | 2004-11-30 | 2008-06-26 | エルジー ハウスホールド アンド ヘルス ケア エルティーディー. | Powder detergent composition capable of improving the touch of clothing and method for producing the same |
| EP1832648A1 (en) | 2006-03-08 | 2007-09-12 | Unilever Plc | Laundry detergent composition and process |
| KR101392380B1 (en) | 2007-02-21 | 2014-05-07 | 주식회사 엘지생활건강 | Powder detergent granule containing acidic water-soluble polymer and manufacturing method thereof |
| US20110166370A1 (en) | 2010-01-12 | 2011-07-07 | Charles Winston Saunders | Scattered Branched-Chain Fatty Acids And Biological Production Thereof |
| BR112013019684A2 (en) | 2011-02-17 | 2016-10-18 | Procter & Gamble | biobased linear alkyl phenyl sulfonates |
| EP2678410B1 (en) | 2011-02-17 | 2017-09-13 | The Procter and Gamble Company | Composiitons comprising mixtures of c10-c13 alkylphenyl sulfonates |
| JP7381740B2 (en) | 2019-11-27 | 2023-11-15 | ザ プロクター アンド ギャンブル カンパニー | liquid laundry detergent composition |
Family Cites Families (22)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CA886828A (en) * | 1971-11-30 | Weinstein Bernard | Process for the production of a homogeneous dry and stable chlorine bleach powder | |
| US3640875A (en) * | 1968-08-14 | 1972-02-08 | Lever Brothers Ltd | Process for preparing a light density bleach composition |
| ZA72295B (en) * | 1971-02-01 | 1973-09-26 | Colgate Palmolive Co | Method for neutralization of detergent acid |
| GB1517713A (en) * | 1974-10-31 | 1978-07-12 | Unilever Ltd | Preparation of detergent formulations |
| ZA776948B (en) * | 1976-12-02 | 1979-06-27 | Colgate Palmolive Co | Low density detergent compositions |
| US4115308A (en) * | 1976-12-27 | 1978-09-19 | The Procter & Gamble Company | High-shear process for preparing silicate-containing paste-form detergent compositions |
| US4151266A (en) * | 1978-06-22 | 1979-04-24 | Allied Chemical Corporation | Method for the conversion of anhydrous sodium carbonate to Wegscheider's Salt |
| PH15525A (en) * | 1979-02-15 | 1983-02-09 | Unilever Nv | Medium density powdered detergent composition and process for making same |
| CA1297376C (en) * | 1985-11-01 | 1992-03-17 | David Philip Jones | Detergent compositions, components therefor, and processes for theirpreparation |
| US4734224A (en) * | 1986-09-15 | 1988-03-29 | The Dial Corporation | Dry neutralization process for detergent slurries |
| US4992079A (en) * | 1986-11-07 | 1991-02-12 | Fmc Corporation | Process for preparing a nonphosphate laundry detergent |
| GB8710292D0 (en) * | 1987-04-30 | 1987-06-03 | Unilever Plc | Detergent compositions |
| GB8710291D0 (en) * | 1987-04-30 | 1987-06-03 | Unilever Plc | Preparation of granular detergent composition |
| GB8710290D0 (en) * | 1987-04-30 | 1987-06-03 | Unilever Plc | Preparation of granular detergent composition |
| GB8817386D0 (en) * | 1988-07-21 | 1988-08-24 | Unilever Plc | Detergent compositions & process for preparing them |
| DE68925938T2 (en) * | 1988-11-02 | 1996-08-08 | Unilever Nv | Process for producing a granular detergent composition with high bulk density |
| GB8907187D0 (en) * | 1989-03-30 | 1989-05-10 | Unilever Plc | Detergent compositions and process for preparing them |
| US5205958A (en) * | 1989-06-16 | 1993-04-27 | The Clorox Company | Zeolite agglomeration process and product |
| GB9008013D0 (en) * | 1990-04-09 | 1990-06-06 | Unilever Plc | High bulk density granular detergent compositions and process for preparing them |
| US5108646A (en) * | 1990-10-26 | 1992-04-28 | The Procter & Gamble Company | Process for agglomerating aluminosilicate or layered silicate detergent builders |
| US5366652A (en) * | 1993-08-27 | 1994-11-22 | The Procter & Gamble Company | Process for making high density detergent agglomerates using an anhydrous powder additive |
| EP0653481A1 (en) * | 1993-11-11 | 1995-05-17 | The Procter & Gamble Company | Granular detergent composition |
-
1995
- 1995-10-04 US US08/539,212 patent/US5576285A/en not_active Expired - Fee Related
-
1996
- 1996-10-01 AT AT96933959T patent/ATE205251T1/en not_active IP Right Cessation
- 1996-10-01 BR BR9610810A patent/BR9610810A/en unknown
- 1996-10-01 CN CN96198635A patent/CN1111595C/en not_active Expired - Fee Related
- 1996-10-01 JP JP9514348A patent/JPH11512775A/en active Pending
- 1996-10-01 DE DE69615042T patent/DE69615042D1/en not_active Expired - Lifetime
- 1996-10-01 EP EP96933959A patent/EP0858500B1/en not_active Expired - Lifetime
- 1996-10-01 WO PCT/US1996/015648 patent/WO1997012955A1/en not_active Ceased
- 1996-10-01 CA CA002234086A patent/CA2234086C/en not_active Expired - Fee Related
- 1996-10-04 AR ARP960104596A patent/AR003789A1/en unknown
Also Published As
| Publication number | Publication date |
|---|---|
| EP0858500B1 (en) | 2001-09-05 |
| ATE205251T1 (en) | 2001-09-15 |
| BR9610810A (en) | 1999-07-13 |
| DE69615042D1 (en) | 2001-10-11 |
| US5576285A (en) | 1996-11-19 |
| CA2234086C (en) | 2001-12-18 |
| CN1202928A (en) | 1998-12-23 |
| CN1111595C (en) | 2003-06-18 |
| EP0858500A1 (en) | 1998-08-19 |
| AR003789A1 (en) | 1998-09-09 |
| JPH11512775A (en) | 1999-11-02 |
| MX9802733A (en) | 1998-09-30 |
| WO1997012955A1 (en) | 1997-04-10 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| EEER | Examination request | ||
| MKLA | Lapsed |