CA2203726A1 - Silanized silica - Google Patents
Silanized silicaInfo
- Publication number
- CA2203726A1 CA2203726A1 CA002203726A CA2203726A CA2203726A1 CA 2203726 A1 CA2203726 A1 CA 2203726A1 CA 002203726 A CA002203726 A CA 002203726A CA 2203726 A CA2203726 A CA 2203726A CA 2203726 A1 CA2203726 A1 CA 2203726A1
- Authority
- CA
- Canada
- Prior art keywords
- pyrogenically
- produced silica
- silanized
- mixing
- provides
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B82—NANOTECHNOLOGY
- B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
- B82Y30/00—Nanotechnology for materials or surface science, e.g. nanocomposites
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B33/00—Silicon; Compounds thereof
- C01B33/113—Silicon oxides; Hydrates thereof
- C01B33/12—Silica; Hydrates thereof, e.g. lepidoic silicic acid
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B33/00—Silicon; Compounds thereof
- C01B33/113—Silicon oxides; Hydrates thereof
- C01B33/12—Silica; Hydrates thereof, e.g. lepidoic silicic acid
- C01B33/18—Preparation of finely divided silica neither in sol nor in gel form; After-treatment thereof
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/34—Silicon-containing compounds
- C08K3/36—Silica
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
- C09C1/00—Treatment of specific inorganic materials other than fibrous fillers; Preparation of carbon black
- C09C1/28—Compounds of silicon
- C09C1/30—Silicic acid
- C09C1/3081—Treatment with organo-silicon compounds
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/42—Gloss-reducing agents
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09G—POLISHING COMPOSITIONS; SKI WAXES
- C09G1/00—Polishing compositions
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K3/00—Materials not provided for elsewhere
- C09K3/10—Materials in mouldable or extrudable form for sealing or packing joints or covers
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/60—Particles characterised by their size
- C01P2004/64—Nanometer sized, i.e. from 1-100 nanometer
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/10—Solid density
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/11—Powder tap density
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/12—Surface area
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/19—Oil-absorption capacity, e.g. DBP values
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/22—Rheological behaviour as dispersion, e.g. viscosity, sedimentation stability
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/80—Compositional purity
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/80—Compositional purity
- C01P2006/82—Compositional purity water content
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/90—Other properties not specified above
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K2200/00—Chemical nature of materials in mouldable or extrudable form for sealing or packing joints or covers
- C09K2200/02—Inorganic compounds
- C09K2200/0243—Silica-rich compounds, e.g. silicates, cement, glass
- C09K2200/0247—Silica
Abstract
The present invention provides a silanized pyrogenically-produced silica with the following physico-chemical properties:
Specific surface area m2/g 80 - 400 Primary particle size nm 7 - 40 Tamped density g/l 50 - 300 pH value 3 - 10 Carbon content % 0.1 - 15 DBP number % < 200.
The invention also provides a method of producing the above silanized pyrogenically-produced silica, comprising spraying pyrogenically-produced silica in a mixing container under intensive mixing, first with water or dilute acid and then with hexamethyldisilazane, mixing for 15 to 30 minutes, and tempering at a temperature of 100 to 400°C for a period of 1 to 6 h.
Specific surface area m2/g 80 - 400 Primary particle size nm 7 - 40 Tamped density g/l 50 - 300 pH value 3 - 10 Carbon content % 0.1 - 15 DBP number % < 200.
The invention also provides a method of producing the above silanized pyrogenically-produced silica, comprising spraying pyrogenically-produced silica in a mixing container under intensive mixing, first with water or dilute acid and then with hexamethyldisilazane, mixing for 15 to 30 minutes, and tempering at a temperature of 100 to 400°C for a period of 1 to 6 h.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE19616781.7 | 1996-04-26 | ||
DE19616781A DE19616781A1 (en) | 1996-04-26 | 1996-04-26 | Silanized silica |
Publications (2)
Publication Number | Publication Date |
---|---|
CA2203726A1 true CA2203726A1 (en) | 1997-10-26 |
CA2203726C CA2203726C (en) | 2001-08-07 |
Family
ID=7792574
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CA002203726A Expired - Lifetime CA2203726C (en) | 1996-04-26 | 1997-04-25 | Silanized silica |
Country Status (6)
Country | Link |
---|---|
EP (1) | EP0808880B1 (en) |
JP (1) | JP3553315B2 (en) |
KR (1) | KR100260325B1 (en) |
CN (1) | CN1083397C (en) |
CA (1) | CA2203726C (en) |
DE (2) | DE19616781A1 (en) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US8062670B2 (en) | 2005-08-05 | 2011-11-22 | 3M Innovative Properties Company | Compositions exhibiting improved flowability |
Families Citing this family (48)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
ATE166023T1 (en) * | 1990-03-22 | 1998-05-15 | Fanuc Ltd | INJECTION MOLDING MACHINE OF AUTOMATIC MOLD CHANGE TYPE |
DE19800022A1 (en) * | 1998-01-02 | 1999-07-08 | Huels Silicone Gmbh | Process for the preparation of silicone polymer-solid mixtures for flowable RTV2 silicone compositions with a low yield point |
DE19929845A1 (en) * | 1999-06-29 | 2001-01-11 | Degussa | Surface-modified pyrogenic titanium dioxide, used in cosmetics e.g. sun-protection agents, is treated with ammonium-functional silane |
GB2357497A (en) | 1999-12-22 | 2001-06-27 | Degussa | Hydrophobic silica |
ATE496098T1 (en) | 2000-10-21 | 2011-02-15 | Evonik Degussa Gmbh | RADIATION CURING PAINT SYSTEMS |
EP1199335B1 (en) * | 2000-10-21 | 2010-12-22 | Evonik Degussa GmbH | Functionalized silicic acids |
EP1199336B1 (en) | 2000-10-21 | 2014-01-15 | Evonik Degussa GmbH | Functionalized, structure modified silicic acids |
DE10105750A1 (en) * | 2001-02-08 | 2002-10-10 | Degussa | Precipitated silicas with a narrow particle size distribution |
DE10138491A1 (en) | 2001-08-04 | 2003-02-13 | Degussa | Process for the production of a hydrophobic precipitated silica with a high degree of whiteness and extremely low moisture absorption |
DE10138490A1 (en) | 2001-08-04 | 2003-02-13 | Degussa | Hydrophobic precipitated silica with a high degree of whiteness and extremely low moisture absorption |
DE10138492A1 (en) * | 2001-08-04 | 2003-02-13 | Degussa | Hydrophobic, non-tempered precipitated silica with a high degree of whiteness |
DE10145162A1 (en) * | 2001-09-13 | 2003-04-10 | Wacker Chemie Gmbh | Silylated silica with low levels of silicon-bonded hydroxy groups useful in toners, developers, charge control agents and flow improvers for powder systems and in crosslinkable polymer and resin compositions |
JP3965497B2 (en) * | 2001-12-28 | 2007-08-29 | 日本アエロジル株式会社 | Low viscosity fumed silica and slurry thereof |
EP1541525A1 (en) * | 2002-03-30 | 2005-06-15 | Degussa AG | Pyrogenic silica having narrow particle size distribution |
DE10239424A1 (en) * | 2002-08-28 | 2004-03-11 | Degussa Ag | silicas |
DE10239423A1 (en) * | 2002-08-28 | 2004-03-11 | Degussa Ag | Silica |
DE10250712A1 (en) * | 2002-10-31 | 2004-05-19 | Degussa Ag | Powdery substances |
DE10258858A1 (en) * | 2002-12-17 | 2004-08-05 | Degussa Ag | Fumed silica |
EP1431245A1 (en) * | 2002-12-17 | 2004-06-23 | Degussa-Hüls Aktiengesellschaft | Surface modified structural silica of aerogel-type |
KR100954073B1 (en) * | 2002-12-18 | 2010-04-23 | 에보닉 데구사 게엠베하 | Structurally coated silica |
AU2003276260A1 (en) | 2002-12-18 | 2004-07-09 | Degussa Ag | Surface-modified, aerogel-type, structured silica |
WO2004055105A1 (en) * | 2002-12-18 | 2004-07-01 | Degussa Ag | Texture-coated silica |
DE10337198A1 (en) * | 2003-08-13 | 2005-03-17 | Degussa Ag | Carriers based on granules produced from pyrogenically prepared silicon dioxides |
DE102004010755A1 (en) * | 2004-03-05 | 2005-09-22 | Degussa Ag | silicone rubber |
DE102004010756A1 (en) * | 2004-03-05 | 2005-09-22 | Degussa Ag | Silanized silicas |
EP1736505B1 (en) * | 2005-06-25 | 2008-08-27 | Evonik Degussa GmbH | Thermoplastic matrix comprising silanised pyrogenic silica |
US20080070146A1 (en) * | 2006-09-15 | 2008-03-20 | Cabot Corporation | Hydrophobic-treated metal oxide |
US8202502B2 (en) | 2006-09-15 | 2012-06-19 | Cabot Corporation | Method of preparing hydrophobic silica |
US8455165B2 (en) | 2006-09-15 | 2013-06-04 | Cabot Corporation | Cyclic-treated metal oxide |
US8435474B2 (en) * | 2006-09-15 | 2013-05-07 | Cabot Corporation | Surface-treated metal oxide particles |
DE102006048509A1 (en) * | 2006-10-13 | 2008-04-17 | Evonik Degussa Gmbh | Surface-modified, structurally modified fumed silicas |
DE102007024365A1 (en) * | 2007-05-22 | 2008-11-27 | Evonik Degussa Gmbh | Pyrogenated silanized and ground silicic acid |
DE102007025685A1 (en) * | 2007-06-01 | 2008-12-04 | Evonik Degussa Gmbh | RTV two-component silicone rubber |
DE102007026214A1 (en) | 2007-06-05 | 2008-12-11 | Evonik Degussa Gmbh | lamp black |
DE102007035952A1 (en) | 2007-07-30 | 2009-04-09 | Evonik Degussa Gmbh | Surface-modified, pyrogenic silicas |
EP2070992A1 (en) * | 2007-12-11 | 2009-06-17 | Evonik Degussa GmbH | Varnishing systems |
DE102008001433A1 (en) * | 2008-04-28 | 2009-10-29 | Evonik Degussa Gmbh | Hydrophobised silicon-iron mixed oxide |
DE102008001437A1 (en) * | 2008-04-28 | 2009-10-29 | Evonik Degussa Gmbh | Surface-modified, superparamagnetic oxide particles |
DE602008006681D1 (en) * | 2008-05-15 | 2011-06-16 | Evonik Degussa Gmbh | Electronic packaging |
DE102008001808A1 (en) | 2008-05-15 | 2009-11-19 | Evonik Degussa Gmbh | coating composition |
EP2123712A1 (en) | 2008-05-19 | 2009-11-25 | Evonik Degussa GmbH | Epoxy resin composition and electronic part |
DE102008001855A1 (en) | 2008-05-19 | 2009-11-26 | Evonik Degussa Gmbh | Two-component composition for the production of flexible polyurethane gelcoats |
EP2145929B1 (en) | 2008-07-18 | 2020-06-24 | Evonik Operations GmbH | Method for manufacturing redispersible, surface-modified silicon dioxide particles |
EP2145928B1 (en) | 2008-07-18 | 2017-09-13 | Evonik Degussa GmbH | Dispersion made of hydrophobic silicon dioxide particles and granulate made from same |
CN102391296B (en) * | 2011-07-13 | 2014-05-14 | 山东旭业新材料股份有限公司 | Preparation method of hydrophobic silane dispersing agent |
DE102013224206A1 (en) | 2013-11-27 | 2015-05-28 | Wacker Chemie Ag | Surface-modified particulate metal oxides |
JP7055294B2 (en) * | 2018-04-02 | 2022-04-18 | 株式会社トラディショナルインテリジェンス | Method of forming coating member and siliceous coating layer |
CN109320998B (en) * | 2018-10-10 | 2021-02-23 | 江苏联瑞新材料股份有限公司 | Method for modifying surface of submicron silicon micropowder |
Family Cites Families (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
IL41404A (en) * | 1972-02-17 | 1975-12-31 | Cabot Corp | Water-repellent coating compositions |
DE2403783C2 (en) * | 1974-01-26 | 1982-10-21 | Bayer Ag, 5090 Leverkusen | Process for the production of hydrophobic fumed silica |
US4208316A (en) * | 1978-06-29 | 1980-06-17 | Deutsche Gold- Und Silber-Scheideanstalt Vormals Roessler | Hydrophobic precipitated silicic acid and compositions containing same |
EP0466958B1 (en) * | 1990-07-19 | 1992-06-03 | Degussa Aktiengesellschaft | Surface-treated silica |
-
1996
- 1996-04-26 DE DE19616781A patent/DE19616781A1/en not_active Ceased
-
1997
- 1997-04-10 EP EP97105909A patent/EP0808880B1/en not_active Expired - Lifetime
- 1997-04-10 DE DE59709069T patent/DE59709069D1/en not_active Expired - Lifetime
- 1997-04-24 CN CN97111729A patent/CN1083397C/en not_active Expired - Lifetime
- 1997-04-24 JP JP10693797A patent/JP3553315B2/en not_active Expired - Lifetime
- 1997-04-25 CA CA002203726A patent/CA2203726C/en not_active Expired - Lifetime
- 1997-04-25 KR KR1019970015688A patent/KR100260325B1/en not_active IP Right Cessation
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US8062670B2 (en) | 2005-08-05 | 2011-11-22 | 3M Innovative Properties Company | Compositions exhibiting improved flowability |
Also Published As
Publication number | Publication date |
---|---|
CN1167729A (en) | 1997-12-17 |
EP0808880A2 (en) | 1997-11-26 |
EP0808880B1 (en) | 2003-01-08 |
DE19616781A1 (en) | 1997-11-06 |
KR100260325B1 (en) | 2000-07-01 |
CA2203726C (en) | 2001-08-07 |
DE59709069D1 (en) | 2003-02-13 |
KR970069878A (en) | 1997-11-07 |
JP3553315B2 (en) | 2004-08-11 |
CN1083397C (en) | 2002-04-24 |
JPH1087317A (en) | 1998-04-07 |
EP0808880A3 (en) | 1999-10-27 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
EEER | Examination request | ||
MKEX | Expiry |
Effective date: 20170425 |