CA1306954C - Hard durable nail polish and method of forming - Google Patents

Hard durable nail polish and method of forming

Info

Publication number
CA1306954C
CA1306954C CA000533901A CA533901A CA1306954C CA 1306954 C CA1306954 C CA 1306954C CA 000533901 A CA000533901 A CA 000533901A CA 533901 A CA533901 A CA 533901A CA 1306954 C CA1306954 C CA 1306954C
Authority
CA
Canada
Prior art keywords
nail
layer
gel
polish
primer
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CA000533901A
Other languages
French (fr)
Inventor
Yosh Hokama
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
International Beauty Design Inc
Original Assignee
International Beauty Design Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by International Beauty Design Inc filed Critical International Beauty Design Inc
Application granted granted Critical
Publication of CA1306954C publication Critical patent/CA1306954C/en
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Classifications

    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q3/00Manicure or pedicure preparations
    • A61Q3/02Nail coatings
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/84Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
    • A61K8/87Polyurethanes
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/80Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
    • A61K2800/81Preparation or application process involves irradiation
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/80Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
    • A61K2800/95Involves in-situ formation or cross-linking of polymers

Landscapes

  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Veterinary Medicine (AREA)
  • Birds (AREA)
  • Epidemiology (AREA)
  • Cosmetics (AREA)

Abstract

HARD DURABLE NAIL POLISH AND
METHOD OF FORMING

ABSTRACT OF THE DISCLOSURE

A method of strengthening a fingernail or toenail is disclosed, the method includes:
a) cleaning the nail surface, b) applying a layer of liquid hydrocarbon primer to the surface to condition same, and allowing the primer layer to dry, c) applying at least one layer of a nail polish composition consisting essentially of:
i) a U.V. hardenable gel, and ii) colorant particles distributed throughout the gel to form a mix, the particles having powder size and forming with the gel a hard, durable polish matrix when the mix, applied as a layer on the nail is hardened under U.V.
radiation.

d) the curing of at least one of said polish layers including subjecting that layer to ultra violet radiation treatment.

Description

6~S~
BACKGROt~ND OF THE INVENTION

This invention relates generally ~o nail polish applicable to fingernails and toenails; more specifically, it concerns a process employing co:Lor coatings applied to nails and ultra violet radiation treatment of such coatinas, to produce extremely durable polishes, which also act to support and protect nails. The latter include natural nails, and alternatively natural and artificial nail composites.
There is need for extremely durable nail polishes that do not easily chip. There is also need for a simple, effective, reliable process to pr~duce nail polish hardened and protected natural, and also composite natural and artiicial, fingernails and toenaiis. Prior nail polishes lacked the unusual application steps and improved results, i.e. extremely durab~e polishes, and polish protected nails characterized by the present invention.

.
SVMI~SARY OF THE INVENTI ON

It is a major object of the invention to provide a nail polish, and a polish forming or application process, meeting the above needs. Basically, the process of the invention comprises the steps:
a) cleaning the nail surface, b) applying a lay~r of liquid hydrocarbon primer to said surface 1:o condition same, and allowing the primer layer to dry, `` ~3~

c) applying at least one layer of a nail polish composition to said dried primer, and curing s~e to form a first coating, said composition consisting essentially of:
i) a U.V. hardenable gel, and ii) colorant particles distribu,ed throughout the gel to form a mix, the particles having powder size and forming with the gel a hard, durable polish matrix when the mix is applied as a layer on the nail and hardened under lD such U.V~ radiation.

d) the curing ~f at least one of said polish layers including subjecting said layer to ultra violet radiation treatment.
Additionalfeatures and steps of the invention include: the application of a second layer ~f the polish composition to the U.V. cured first layer, the gel in each layer ~onsisting of a U.V. polymer gel containing primarily urethane acrylate; the applieation of the polish composition to both nat~ral and artificial nails tv build ~p protective and polish forming layers extensively overlap~ing bot~ ~uch nails, which are only initially ~oined at their terminals, and the application of one or more su~h layers to 2 nail orm used to build up a nail extension forwardly of the tip of a natural nail, the resultant nail extension being colored throughout.
These and ~ther objects and advantag~s of the invention, as well as the details of an illustrati~e embodiment, will be more fully understood from the ~ollo~-ing specifica~ion and drawings, in whieh:

DRAWING DESCRIPTION

Fig. 1 is a process flow diagram;
, ~ ~3-6~S4 Fig. 2 is a vertical section taken through a fingernail onto which a hardened polish layer, or layers, have been applied;
Fig. 3 is a view like Fig. 2 also showing a fingernail tip, i.e. artificial fingernail, to which the hardened polish layer, or layers, have been appl1ed;
Fig. 4 is a view like Fig. 2 but also sho~ling the use of a removable form onto which the har~ened polish layer, or layers, have been applied;
Fig. 5 is a vertical section showin~ ultraviolet radiation treatment of fingernails to which a polish layer or layers have been applied; and Fig. 6 is an enlarged section, showing the polish matrix of particles and hardened gel, applied to a nail.

DETAILED DESCRIPTION

In Fig. 2, fingernail 10 is to undergo treatment.
- It is first buffed at 20 (in Fig. 1) to roughen its top surface. Next, it is cleaned at 21, as by application of a liquid hydrocarbon cleaner, and preferably trichloroethane.
After during, a primer coat 11 is brushed onto the cleaned nail surface, as indicated at 22 in Fig. 1, to condition tha-t surface. The primer preferably has an acrylate base, and preferably consis-ts of mixture of methacrylic acid isobutyl methacrylate, and benzyl alcohol, in the following 25 proportions W _ght %
methacrylic acid about 74%
isobutyl methacrylate about 24 benzyl alcohol about 2%

,.

After drying o the primer, for about 4~ seconds, indicated at 23, a viscous flowable polish layer 12 is brushed i.e., applied unto the dried primer layer 11, this step shown at 24. Layer or coating 12 is ultra -:iolet radiation sensitive, and adapted to harden and protect, when such radiation is applied. The layer 12 contalns a U.V.
sensitive polymer gei, and the gel by way oi e~a~?le may have the following composition, for very good results:
Ingredients Relative weights Urethane acrylate about 60 acrylic ester monomers (such as ethyl and/or methyl methacrylate) about 15 aromatic amine (such as phenyl diethanolamine) tPhoto initiator) about ~dditive/Adhesion about Promotors (such as - Silane The above ingredients in base gel for~, may vary in weight percent as follows:

Base gel Ingredient Weight percent urethane acrylate 50-85 acrylic ester monomers 5-35 photo initïator ~ 1-10 additive/adhesion promotor C 3 The base gel is sold by International Beauty Products, Gardena, California, under the trademark "SOFT-LIGH~ GEL" and has the following physical properties:

695~
Boiling point: Does not pour at 10C
% Volatiles by volume: ~ 1 Solubility in H: Insoluble Evaporation Rate Butyl Acetate = 1): `;e lible Viscosity: 48-4 37,000 cpsat 25C
40-1 117,000 cps at 25~C
Flash Point: l90~F
The layer 12 also contains colorant ~æ~ticles distributed throughout the gel to iorm a mix, the particles having powder size and forming with the gel a ha~d, durable polish matrix when the mix is appl~ed as a layer on the nail and hardened under said U.V. radiation. The particles preferably consist essentially of pigments such as metal salts, such as selected from the grGup iron oxide (rusty red), mica bismuth oxychloride, titanium dioxide manganese oxide(violet) carbon black, chrome yellow primrose, pigment scarlet, alkali blue, cyclo~liphatic dye epoxides, dihyroxyl ether in selected pro- ~
portions to give the resultant hardened nail polish the desired oolor.
The gel after prior curing for about 1-3 minutes si allowed to cure under U.V. radiation, for a short time interval, i.e., between 1 and 3 minutes, and perferably about 2 minutes, as indicated at 25.
Fig. 5 shows a fingernail 40, coated as described, inserted into a recess 36a in a receptacle 36, the finger 40_ placed ~n a shelf 37 in the racetacle. An ultra~iolet light bulb 38 at predetermined distance above the fincernail, emits ultraviolet radiation 39 impinging on the nail. This treatment continued for betwee~ 1 an~ 4 minutes, prefereabl~ about 2 minutes, cures the gel coating to a hardened state. Thereafter, the treated nail is cleaned at 26, as with trichloroethane~
and the resul~ant nail is presented at 27 in clean~d and hard~ned state. Fig 6 sho~s a polish matrix 40 as on a nail .
. ...

B

~16~5~
41, with particles 42 uniformly distributed in the cured gel to form the tough, hardened, non-chipping nail polish matrix.
Fig. 1 also illustrates an alterna i;e p-ocessing path, after step 23, Step 28 is the same as s.e~ 24, and comprises a second polish coat or layer app'~c_tion. The next steps 29 and 30 are the same as steps 2S and 26 described above. After cleaning at 30, the resultant ~e-y hard polished and protected nail is presented at 31.
A typical U.V. bulb 38 is of 4 watt po.;er, delivers between .25 and .75 milliwatts per square cen~imeter ~preferably about .5 milliwatts per cm2) at the location of the fingernail.
~ig. 3 snows application of the process to a nail composite which includes the natural nail 10 of Fig. 2, and also ~ nail tip, i.e. artificial, or plastic nail 100 attached at 101 to nail 10. See for example ~.S. paten. 4,135,526 to Matranga et al. "Five second" glue may be ap?lied at 102 to the top surface junction between the nails 10 and 100.
One such glue is known as "KRAZY GLUE," a product of Krazy Glue, Inc., Itaska, Illinois. Primer 11 as referred to above is applied to the natural nail as described above; and primer lla as referred to above is applied to the top surface of the nail tip. That primer may ~onsist of SIL~E, a product (A 187) of Union Carbide Corp.
The polish layer 12, as aescribed above, is applied to the primer layers 11 and lla as described above, bu~ layer lla should be sli.ghtly damp The sequence 25-27 is then fsllowed, or in addition sequence 28-31.
* TRADEMARK

~36~54 Fig. 4 shows application of the process to a nail 10 and nail form, i.e. support, 200 projecting forwardly of nail 10. The form may be put in place aEter steps 20 and 21 of Fig. 1 are carried out. Sequence 22-27, or sequence 22-25 and 28-31 may be employed, after which the form is removed, whereby a hardened nail extension is provided as at 201.
The polish layers ex-tending at 204 forwardly of the natural nail are colored throughout, color being visible on top and bottom sides of the layers at 204.

~ ~ ~ , .

.
, ' - .

; ' ` `
.'. ' .
.. . . ..... ~

Claims (11)

1. The method of strengthening a natural fingernail or toenail, that includes a) presenting the nail surface, and an artificial surface adjacent to and projecting forwardly of the forward edge portion of the natural nail, b) applying a layer of liquid hydrocarbon primer to said nail surface to condition same and to the artificial surface and allowing the primer layer to dry, c) applying to the dried primer over both said surfaces at least one layer of a nail polish composition consisting essentially of:
i) a U.V. radiation hardenable gel, and ii) colorant substance distributed throughout the gel to form a mix, said substance forming with the gel a hard, durable polish matrix when the mix is applied as a layer on the nail and hardened under said U.V.
radiation, d) the curing of at least one of said polish layers including subjecting said layer to ultra violet radiation treatment that includes applying between .25 and .75 milliwatts per square centimeter of said radiation for between 1 and 4 minutes, e) said gel consisting essentially of a liquid mixture defined as follows:

2. The method of claim 1, wherein said U.V.
radiation treatment is continued for about 2 minutes.
3. The method of claim 1 wherein a second layer of said nail polish composition is then applied onto said cured first coating and allowed to cure, said curing including U.V. treatment.
4. The method of claim 1 wherein said gel consists primarily of urethane acrylate.
5. The method of claim 1 wherein said colorant includes particles that consist essentially of metal salts.
6. The method of claim 5 wherein the colorant particles are selected from the group that includes iron oxide, mica bismuth, oxychloride, titanium dioxide, and manganese oxide.
7. The method of claim 1 which includes cleaning said dried polymer layer with trichloroethane.
8. The method of claim 5 which includes cleaning said cured first coating with trichloroethane prior to applying said second layer thereto.
9. The method of claim 1 wherein said primer consists essentially of a mixture of methacrylic acid benzyl alcohol, and isobutyl methacrylate.
10. The method of claim 1 wherein said artificial surface is defined by an artificial nail attached to said natural nail and projecting beyond the end thereof to provide a common nail surface to which said layers of steps b) - c) of claim 1 are applied.
11. The method of claim 1 wherein said artificial surface is defined by a nail form with its upper surface projecting endwise of and beyond the end of the natural nail surface, said layers of steps b) and c) of claim 1, being applied to said form upper surface, and including carrying out said step d) with respect to said layers applied to said form; and finally removing said form.
CA000533901A 1986-04-07 1987-04-06 Hard durable nail polish and method of forming Expired - Fee Related CA1306954C (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US849,011 1977-11-07
US84901186A 1986-04-07 1986-04-07

Publications (1)

Publication Number Publication Date
CA1306954C true CA1306954C (en) 1992-09-01

Family

ID=25304851

Family Applications (1)

Application Number Title Priority Date Filing Date
CA000533901A Expired - Fee Related CA1306954C (en) 1986-04-07 1987-04-06 Hard durable nail polish and method of forming

Country Status (1)

Country Link
CA (1) CA1306954C (en)

Cited By (27)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2939620A1 (en) * 2008-12-17 2010-06-18 Oreal Coating a tip of polished nail, comprises applying a composition having a viscosity of specified value on the tip of the nails to form a wet edge having a specified thickness, where he composition is crosslinkable/polymerizable composition
WO2010070139A1 (en) 2008-12-19 2010-06-24 L'oreal Antiperspirant comprising components able to form covalent bonds between one another and two-stage method of treatment of sweating in humans
EP2221038A1 (en) 2009-02-23 2010-08-25 L'Oréal Make-up method with application of a base layer and system for implementing said method
EP2221037A1 (en) 2009-02-23 2010-08-25 L'Oréal Make-up method involving exposition to a specific radiation whereby protection of the resulting make-up is achieved with an optical agent
EP2221041A2 (en) 2009-02-23 2010-08-25 L'Oréal Developping photomake-up process
WO2010095118A2 (en) 2009-02-23 2010-08-26 L'oreal A cosmetic treatment method including the projection of an image onto the zone to be treated
WO2010095117A1 (en) 2009-02-23 2010-08-26 L'oreal A method of making up with light-sensitive makeup using a photochromic composition in the already-developed state
WO2010095116A1 (en) 2009-02-23 2010-08-26 L'oreal A method of removing makeup and a makeup remover
WO2010095120A1 (en) 2009-02-23 2010-08-26 L'oreal A method of making up using an addressable matrix light source
WO2010103420A2 (en) 2009-03-12 2010-09-16 L'oreal A method of making up with light-sensitive makeup with mechanical protection of the light-sensitive makeup
WO2011003771A2 (en) 2009-07-07 2011-01-13 L'oreal Method for smoothing out the skin by filling in recessed portions
WO2011003770A2 (en) 2009-07-07 2011-01-13 L'oreal Method for smoothing out the skin by filling in recessed portions
WO2012023116A1 (en) 2010-08-20 2012-02-23 L'oreal Cosmetic method
WO2012130603A1 (en) 2011-03-15 2012-10-04 L'oreal Photo-crosslinkable nail varnishes free of unsaturated monomers
WO2012130600A1 (en) 2011-03-15 2012-10-04 L'oreal Photo-crosslinkable nail varnishes free of unsaturated monomers
WO2012130604A1 (en) 2011-03-15 2012-10-04 L'oreal Photo-crosslinkable nail varnishes free of unsaturated monomers
WO2012130601A1 (en) 2011-03-15 2012-10-04 L'oreal Photo-crosslinkable nail varnishes free of unsaturated monomers
WO2012130602A1 (en) 2011-03-15 2012-10-04 L'oreal Photo-crosslinkable nail varnishes free of unsaturated monomers
WO2013013903A1 (en) 2011-07-22 2013-01-31 L'oreal Process for treating perspiration using an anhydrous composition comprising two reagents that together produce an antiperspirant effect in situ on the skin
WO2014086867A1 (en) 2012-12-05 2014-06-12 L'oreal Nail makeup method with photocrosslinkable varnish compositions
WO2014086875A2 (en) 2012-12-05 2014-06-12 L'oreal High-gloss photocrosslinkable cosmetic composition
WO2014086872A2 (en) 2012-12-05 2014-06-12 L'oreal Non-tacky photocrosslinkable cosmetic composition
WO2014086877A2 (en) 2012-12-05 2014-06-12 L'oreal Novel photocrosslinkable compositions for use as base coat
WO2014086869A1 (en) 2012-12-05 2014-06-12 L'oreal Photocrosslinkable nail makeup composition
WO2014086881A2 (en) 2012-12-05 2014-06-12 L'oreal Nail makeup method with photocrosslinkable varnish compositions
WO2015082336A1 (en) 2013-12-04 2015-06-11 L'oreal Photo-crosslinkable varnish compositions and application methods
CN110236283A (en) * 2018-03-08 2019-09-17 马语禧 Artificial nail piece and curing combination and method of using the same

Cited By (28)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2939620A1 (en) * 2008-12-17 2010-06-18 Oreal Coating a tip of polished nail, comprises applying a composition having a viscosity of specified value on the tip of the nails to form a wet edge having a specified thickness, where he composition is crosslinkable/polymerizable composition
WO2010070139A1 (en) 2008-12-19 2010-06-24 L'oreal Antiperspirant comprising components able to form covalent bonds between one another and two-stage method of treatment of sweating in humans
EP2221038A1 (en) 2009-02-23 2010-08-25 L'Oréal Make-up method with application of a base layer and system for implementing said method
EP2221037A1 (en) 2009-02-23 2010-08-25 L'Oréal Make-up method involving exposition to a specific radiation whereby protection of the resulting make-up is achieved with an optical agent
EP2221041A2 (en) 2009-02-23 2010-08-25 L'Oréal Developping photomake-up process
WO2010095118A2 (en) 2009-02-23 2010-08-26 L'oreal A cosmetic treatment method including the projection of an image onto the zone to be treated
WO2010095117A1 (en) 2009-02-23 2010-08-26 L'oreal A method of making up with light-sensitive makeup using a photochromic composition in the already-developed state
WO2010095116A1 (en) 2009-02-23 2010-08-26 L'oreal A method of removing makeup and a makeup remover
WO2010095120A1 (en) 2009-02-23 2010-08-26 L'oreal A method of making up using an addressable matrix light source
WO2010103420A2 (en) 2009-03-12 2010-09-16 L'oreal A method of making up with light-sensitive makeup with mechanical protection of the light-sensitive makeup
WO2011003771A2 (en) 2009-07-07 2011-01-13 L'oreal Method for smoothing out the skin by filling in recessed portions
WO2011003770A2 (en) 2009-07-07 2011-01-13 L'oreal Method for smoothing out the skin by filling in recessed portions
WO2012023116A1 (en) 2010-08-20 2012-02-23 L'oreal Cosmetic method
WO2012130603A1 (en) 2011-03-15 2012-10-04 L'oreal Photo-crosslinkable nail varnishes free of unsaturated monomers
WO2012130600A1 (en) 2011-03-15 2012-10-04 L'oreal Photo-crosslinkable nail varnishes free of unsaturated monomers
WO2012130604A1 (en) 2011-03-15 2012-10-04 L'oreal Photo-crosslinkable nail varnishes free of unsaturated monomers
WO2012130601A1 (en) 2011-03-15 2012-10-04 L'oreal Photo-crosslinkable nail varnishes free of unsaturated monomers
WO2012130602A1 (en) 2011-03-15 2012-10-04 L'oreal Photo-crosslinkable nail varnishes free of unsaturated monomers
WO2013013903A1 (en) 2011-07-22 2013-01-31 L'oreal Process for treating perspiration using an anhydrous composition comprising two reagents that together produce an antiperspirant effect in situ on the skin
WO2014086867A1 (en) 2012-12-05 2014-06-12 L'oreal Nail makeup method with photocrosslinkable varnish compositions
WO2014086875A2 (en) 2012-12-05 2014-06-12 L'oreal High-gloss photocrosslinkable cosmetic composition
WO2014086872A2 (en) 2012-12-05 2014-06-12 L'oreal Non-tacky photocrosslinkable cosmetic composition
WO2014086877A2 (en) 2012-12-05 2014-06-12 L'oreal Novel photocrosslinkable compositions for use as base coat
WO2014086869A1 (en) 2012-12-05 2014-06-12 L'oreal Photocrosslinkable nail makeup composition
WO2014086881A2 (en) 2012-12-05 2014-06-12 L'oreal Nail makeup method with photocrosslinkable varnish compositions
WO2015082336A1 (en) 2013-12-04 2015-06-11 L'oreal Photo-crosslinkable varnish compositions and application methods
CN110236283A (en) * 2018-03-08 2019-09-17 马语禧 Artificial nail piece and curing combination and method of using the same
CN110236283B (en) * 2018-03-08 2022-06-21 马语禧 Artificial nail plate and curing combination set and using method thereof

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