CA1095801A - Manufacture of particulate detergents - Google Patents
Manufacture of particulate detergentsInfo
- Publication number
- CA1095801A CA1095801A CA263,655A CA263655A CA1095801A CA 1095801 A CA1095801 A CA 1095801A CA 263655 A CA263655 A CA 263655A CA 1095801 A CA1095801 A CA 1095801A
- Authority
- CA
- Canada
- Prior art keywords
- accordance
- slurry
- detergent
- water
- microwave
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 239000003599 detergent Substances 0.000 title claims abstract description 53
- 238000004519 manufacturing process Methods 0.000 title claims description 5
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 42
- 239000002002 slurry Substances 0.000 claims abstract description 36
- 239000000203 mixture Substances 0.000 claims abstract description 30
- 230000001413 cellular effect Effects 0.000 claims abstract description 16
- 230000000694 effects Effects 0.000 claims abstract description 8
- 238000000034 method Methods 0.000 claims description 27
- 238000010438 heat treatment Methods 0.000 claims description 16
- 235000019832 sodium triphosphate Nutrition 0.000 claims description 13
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 claims description 10
- 239000002671 adjuvant Substances 0.000 claims description 6
- 150000003839 salts Chemical class 0.000 claims description 6
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 5
- 239000007787 solid Substances 0.000 claims description 5
- 125000000129 anionic group Chemical class 0.000 claims description 4
- 239000004615 ingredient Substances 0.000 claims description 4
- 239000007921 spray Substances 0.000 claims description 4
- 238000006703 hydration reaction Methods 0.000 claims description 3
- 230000036571 hydration Effects 0.000 claims 1
- 230000015572 biosynthetic process Effects 0.000 abstract description 3
- 238000009835 boiling Methods 0.000 abstract description 3
- 238000002425 crystallisation Methods 0.000 abstract description 2
- 238000001704 evaporation Methods 0.000 abstract description 2
- 230000008020 evaporation Effects 0.000 abstract description 2
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 18
- 239000000306 component Substances 0.000 description 16
- 239000000463 material Substances 0.000 description 14
- 239000000047 product Substances 0.000 description 13
- 239000000843 powder Substances 0.000 description 11
- UNXRWKVEANCORM-UHFFFAOYSA-I triphosphate(5-) Chemical compound [O-]P([O-])(=O)OP([O-])(=O)OP([O-])([O-])=O UNXRWKVEANCORM-UHFFFAOYSA-I 0.000 description 8
- 239000004115 Sodium Silicate Substances 0.000 description 7
- 238000001035 drying Methods 0.000 description 7
- 229910052911 sodium silicate Inorganic materials 0.000 description 7
- 235000015096 spirit Nutrition 0.000 description 7
- 238000001816 cooling Methods 0.000 description 6
- 235000011121 sodium hydroxide Nutrition 0.000 description 6
- NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 description 6
- 229920002134 Carboxymethyl cellulose Polymers 0.000 description 5
- 229910019142 PO4 Inorganic materials 0.000 description 5
- 239000001768 carboxy methyl cellulose Substances 0.000 description 5
- 239000008112 carboxymethyl-cellulose Substances 0.000 description 5
- 229940105329 carboxymethylcellulose Drugs 0.000 description 5
- 239000008187 granular material Substances 0.000 description 5
- 239000003112 inhibitor Substances 0.000 description 5
- 230000003287 optical effect Effects 0.000 description 5
- 239000010452 phosphate Substances 0.000 description 5
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 description 5
- 235000010948 carboxy methyl cellulose Nutrition 0.000 description 4
- 230000004907 flux Effects 0.000 description 4
- 238000013467 fragmentation Methods 0.000 description 4
- 238000006062 fragmentation reaction Methods 0.000 description 4
- 230000014759 maintenance of location Effects 0.000 description 4
- 150000002978 peroxides Chemical class 0.000 description 4
- 239000002253 acid Substances 0.000 description 3
- 150000004996 alkyl benzenes Chemical class 0.000 description 3
- 238000006243 chemical reaction Methods 0.000 description 3
- 238000002474 experimental method Methods 0.000 description 3
- SNQQPOLDUKLAAF-UHFFFAOYSA-N nonylphenol Chemical class CCCCCCCCCC1=CC=CC=C1O SNQQPOLDUKLAAF-UHFFFAOYSA-N 0.000 description 3
- 239000002245 particle Substances 0.000 description 3
- 238000001694 spray drying Methods 0.000 description 3
- BDHFUVZGWQCTTF-UHFFFAOYSA-N sulfonic acid Chemical compound OS(=O)=O BDHFUVZGWQCTTF-UHFFFAOYSA-N 0.000 description 3
- 239000004094 surface-active agent Substances 0.000 description 3
- ORACIQIJMCYPHQ-MDZDMXLPSA-N 2-[4-[(e)-2-[4-(1,3-benzoxazol-2-yl)phenyl]ethenyl]phenyl]-1,3-benzoxazole Chemical group C1=CC=C2OC(C3=CC=C(C=C3)/C=C/C=3C=CC(=CC=3)C=3OC4=CC=CC=C4N=3)=NC2=C1 ORACIQIJMCYPHQ-MDZDMXLPSA-N 0.000 description 2
- WBIQQQGBSDOWNP-UHFFFAOYSA-N 2-dodecylbenzenesulfonic acid Chemical compound CCCCCCCCCCCCC1=CC=CC=C1S(O)(=O)=O WBIQQQGBSDOWNP-UHFFFAOYSA-N 0.000 description 2
- 239000004604 Blowing Agent Substances 0.000 description 2
- IAYPIBMASNFSPL-UHFFFAOYSA-N Ethylene oxide Chemical compound C1CO1 IAYPIBMASNFSPL-UHFFFAOYSA-N 0.000 description 2
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 2
- IGFHQQFPSIBGKE-UHFFFAOYSA-N Nonylphenol Natural products CCCCCCCCCC1=CC=C(O)C=C1 IGFHQQFPSIBGKE-UHFFFAOYSA-N 0.000 description 2
- 101710194948 Protein phosphatase PhpP Proteins 0.000 description 2
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 description 2
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 2
- 239000007864 aqueous solution Substances 0.000 description 2
- LPTWEDZIPSKWDG-UHFFFAOYSA-N benzenesulfonic acid;dodecane Chemical compound OS(=O)(=O)C1=CC=CC=C1.CCCCCCCCCCCC LPTWEDZIPSKWDG-UHFFFAOYSA-N 0.000 description 2
- HWGNBUXHKFFFIH-UHFFFAOYSA-I pentasodium;[oxido(phosphonatooxy)phosphoryl] phosphate Chemical compound [Na+].[Na+].[Na+].[Na+].[Na+].[O-]P([O-])(=O)OP([O-])(=O)OP([O-])([O-])=O HWGNBUXHKFFFIH-UHFFFAOYSA-I 0.000 description 2
- 230000000717 retained effect Effects 0.000 description 2
- 239000011734 sodium Substances 0.000 description 2
- 229910052708 sodium Inorganic materials 0.000 description 2
- UGTZMIPZNRIWHX-UHFFFAOYSA-K sodium trimetaphosphate Chemical compound [Na+].[Na+].[Na+].[O-]P1(=O)OP([O-])(=O)OP([O-])(=O)O1 UGTZMIPZNRIWHX-UHFFFAOYSA-K 0.000 description 2
- 239000000243 solution Substances 0.000 description 2
- -1 sulpho Chemical class 0.000 description 2
- 241001391944 Commicarpus scandens Species 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- 229920000877 Melamine resin Polymers 0.000 description 1
- BPQQTUXANYXVAA-UHFFFAOYSA-N Orthosilicate Chemical compound [O-][Si]([O-])([O-])[O-] BPQQTUXANYXVAA-UHFFFAOYSA-N 0.000 description 1
- 239000004743 Polypropylene Substances 0.000 description 1
- 229920001213 Polysorbate 20 Polymers 0.000 description 1
- 238000007664 blowing Methods 0.000 description 1
- 230000001680 brushing effect Effects 0.000 description 1
- 239000001913 cellulose Substances 0.000 description 1
- 229920002678 cellulose Polymers 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 230000002844 continuous effect Effects 0.000 description 1
- 238000010924 continuous production Methods 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 230000003247 decreasing effect Effects 0.000 description 1
- 230000018044 dehydration Effects 0.000 description 1
- 238000006297 dehydration reaction Methods 0.000 description 1
- 230000003292 diminished effect Effects 0.000 description 1
- ZLCCLBKPLLUIJC-UHFFFAOYSA-L disodium tetrasulfane-1,4-diide Chemical compound [Na+].[Na+].[S-]SS[S-] ZLCCLBKPLLUIJC-UHFFFAOYSA-L 0.000 description 1
- 230000035611 feeding Effects 0.000 description 1
- 239000011152 fibreglass Substances 0.000 description 1
- 238000009472 formulation Methods 0.000 description 1
- 239000003517 fume Substances 0.000 description 1
- 230000005484 gravity Effects 0.000 description 1
- BHEPBYXIRTUNPN-UHFFFAOYSA-N hydridophosphorus(.) (triplet) Chemical compound [PH] BHEPBYXIRTUNPN-UHFFFAOYSA-N 0.000 description 1
- 238000011065 in-situ storage Methods 0.000 description 1
- 229940060367 inert ingredients Drugs 0.000 description 1
- JDSHMPZPIAZGSV-UHFFFAOYSA-N melamine Chemical compound NC1=NC(N)=NC(N)=N1 JDSHMPZPIAZGSV-UHFFFAOYSA-N 0.000 description 1
- 229920000609 methyl cellulose Polymers 0.000 description 1
- 239000001923 methylcellulose Substances 0.000 description 1
- 235000010981 methylcellulose Nutrition 0.000 description 1
- 229920000847 nonoxynol Polymers 0.000 description 1
- 238000012856 packing Methods 0.000 description 1
- 239000002798 polar solvent Substances 0.000 description 1
- 239000000256 polyoxyethylene sorbitan monolaurate Substances 0.000 description 1
- 239000004810 polytetrafluoroethylene Substances 0.000 description 1
- 229920001343 polytetrafluoroethylene Polymers 0.000 description 1
- XOFYZVNMUHMLCC-ZPOLXVRWSA-N prednisone Chemical compound O=C1C=C[C@]2(C)[C@H]3C(=O)C[C@](C)([C@@](CC4)(O)C(=O)CO)[C@@H]4[C@@H]3CCC2=C1 XOFYZVNMUHMLCC-ZPOLXVRWSA-N 0.000 description 1
- 230000000750 progressive effect Effects 0.000 description 1
- 235000019812 sodium carboxymethyl cellulose Nutrition 0.000 description 1
- 239000011780 sodium chloride Substances 0.000 description 1
- 159000000000 sodium salts Chemical class 0.000 description 1
- 235000019794 sodium silicate Nutrition 0.000 description 1
- 229910052938 sodium sulfate Inorganic materials 0.000 description 1
- 235000011152 sodium sulphate Nutrition 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 230000008961 swelling Effects 0.000 description 1
- 230000004580 weight loss Effects 0.000 description 1
Classifications
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F26—DRYING
- F26B—DRYING SOLID MATERIALS OR OBJECTS BY REMOVING LIQUID THEREFROM
- F26B3/00—Drying solid materials or objects by processes involving the application of heat
- F26B3/32—Drying solid materials or objects by processes involving the application of heat by development of heat within the materials or objects to be dried, e.g. by fermentation or other microbiological action
- F26B3/34—Drying solid materials or objects by processes involving the application of heat by development of heat within the materials or objects to be dried, e.g. by fermentation or other microbiological action by using electrical effects
- F26B3/347—Electromagnetic heating, e.g. induction heating or heating using microwave energy
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D11/00—Special methods for preparing compositions containing mixtures of detergents
Landscapes
- Engineering & Computer Science (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Microbiology (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Physics & Mathematics (AREA)
- Electromagnetism (AREA)
- Health & Medical Sciences (AREA)
- Biomedical Technology (AREA)
- Biotechnology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Molecular Biology (AREA)
- Mechanical Engineering (AREA)
- General Engineering & Computer Science (AREA)
- Detergent Compositions (AREA)
Applications Claiming Priority (4)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| ZA6587A ZA756587B (en) | 1975-10-20 | 1975-10-20 | Manufacture of particulate detergents |
| ZA75/6587 | 1975-10-20 | ||
| ZA76/0345 | 1976-01-21 | ||
| ZA76345 | 1976-01-21 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CA1095801A true CA1095801A (en) | 1981-02-17 |
Family
ID=27131132
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CA263,655A Expired CA1095801A (en) | 1975-10-20 | 1976-10-19 | Manufacture of particulate detergents |
Country Status (6)
| Country | Link |
|---|---|
| US (1) | US4118333A (https=) |
| CA (1) | CA1095801A (https=) |
| DE (1) | DE2646953C2 (https=) |
| DK (1) | DK473976A (https=) |
| FR (1) | FR2328767A1 (https=) |
| SE (1) | SE433618B (https=) |
Families Citing this family (16)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2744753C2 (de) * | 1977-10-05 | 1986-08-28 | Joh. A. Benckiser Gmbh, 6700 Ludwigshafen | Verfahren zur Herstellung von Granulaten |
| US4457908A (en) * | 1979-10-24 | 1984-07-03 | Colgate-Palmolive Company | Stabilization of carrageenan-containing toothpaste |
| US4353890A (en) * | 1979-10-24 | 1982-10-12 | Colgate-Palmolive Company | Stabilization of carrageenan-containing toothpaste |
| BE1004876A5 (fr) * | 1991-05-27 | 1993-02-16 | Serstevens Albert T | Perfectionnement pour l'obtention de poudres a lessiver par micro-ondes. |
| US6689305B1 (en) * | 1993-05-05 | 2004-02-10 | Ecolab Inc. | Process for consolidating particulate solids and cleaning products therefrom II |
| ES2165874T3 (es) * | 1993-05-05 | 2002-04-01 | Henkel Ecolab Gmbh & Co Ohg | Procedimiento para consolidar solidos en particulas y los productos de limpieza a partir de ellos. |
| US5858299A (en) * | 1993-05-05 | 1999-01-12 | Ecolab, Inc. | Process for consolidating particulate solids |
| GB9316900D0 (en) * | 1993-08-13 | 1993-09-29 | Hecht Samuel I | Soap product |
| DE4429550A1 (de) * | 1994-08-19 | 1996-02-22 | Henkel Kgaa | Verfahren zur Herstellung von Wasch- oder Reinigungsmitteltabletten |
| EP0912717B1 (en) * | 1996-05-14 | 2002-12-11 | The Procter & Gamble Company | Process for making a low density detergent composition by agglomeration followed by dielectric heating |
| US5961663A (en) * | 1997-05-29 | 1999-10-05 | Colgate-Palmolive Co. | Microwave-dried amorphous alkali metal silicate powders and their use as builders in detergent compositions |
| JP3604623B2 (ja) * | 2000-10-23 | 2004-12-22 | 花王株式会社 | アニオン界面活性剤粉粒体の製造方法 |
| JP4187995B2 (ja) * | 2002-04-19 | 2008-11-26 | 花王株式会社 | アニオン界面活性剤粉粒体の製造法 |
| US20040149742A1 (en) * | 2003-01-30 | 2004-08-05 | Lescano Ricardo Andres | System to heat liquids |
| DE102004003430A1 (de) * | 2004-01-23 | 2005-05-25 | Henkel Kgaa | Verfahren zur Verarbeitung von Wasch- oder Reinigungsmitteln |
| CZ304481B6 (cs) * | 2013-06-11 | 2014-05-21 | Ústav Chemických Procesů Akademie Věd České Republiky | Způsob sušení tenzidů |
Family Cites Families (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| BE608466A (https=) * | 1960-09-23 | |||
| NL278464A (https=) * | 1961-05-15 | |||
| DE1277491B (de) * | 1962-08-04 | 1968-09-12 | Daiichi Seiyaku Co | Verfahren zum Herstellen von Wasch- oder Reinigungsmitteltabletten |
| US3431210A (en) * | 1966-03-01 | 1969-03-04 | Monsanto Co | Detergent processes |
| GB1303102A (https=) * | 1969-01-16 | 1973-01-17 | ||
| US3771234A (en) * | 1969-09-09 | 1973-11-13 | Exxon Research Engineering Co | Microwave drying process for synthetic polymers |
| ZA726290B (en) * | 1972-09-14 | 1974-04-24 | Chem Services Ltd | Production of detergents |
| US3932140A (en) * | 1973-04-30 | 1976-01-13 | E. I. Du Pont De Nemours & Co. | Forming highly absorbent, low bulk density sodium silicate by contacting with H2 O2 and heating to about 45° to 60°C |
-
1976
- 1976-10-18 DE DE2646953A patent/DE2646953C2/de not_active Expired
- 1976-10-18 US US05/733,561 patent/US4118333A/en not_active Expired - Lifetime
- 1976-10-19 CA CA263,655A patent/CA1095801A/en not_active Expired
- 1976-10-19 SE SE7611573A patent/SE433618B/xx not_active IP Right Cessation
- 1976-10-20 DK DK473976A patent/DK473976A/da not_active Application Discontinuation
- 1976-10-20 FR FR7631546A patent/FR2328767A1/fr active Granted
Also Published As
| Publication number | Publication date |
|---|---|
| SE433618B (sv) | 1984-06-04 |
| US4118333A (en) | 1978-10-03 |
| FR2328767B1 (https=) | 1981-01-09 |
| FR2328767A1 (fr) | 1977-05-20 |
| DE2646953C2 (de) | 1986-06-26 |
| DK473976A (da) | 1977-04-21 |
| SE7611573L (sv) | 1977-04-21 |
| DE2646953A1 (de) | 1977-04-21 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CA1095801A (en) | Manufacture of particulate detergents | |
| US3450494A (en) | Amorphous sodium silicate having inherent binding properties and method of producing same | |
| DE60132282T2 (de) | Verfahren zur Herstellung eines anionischen Tensidpulvers | |
| US3868227A (en) | Agglomerating fine alkali metal silicate particles to form hydrated, amorphous, granules | |
| JPH03146599A (ja) | 高嵩密度洗剤組成物の製造方法 | |
| DE2235891A1 (de) | Verfahren zum trocknen hitzelabiler tenside | |
| SU1012784A3 (ru) | Способ увеличени объема табака | |
| WO2001010780A1 (en) | Method and apparatus for producing zeolite | |
| US5409643A (en) | Method of making a granular product with a high specific weight | |
| US5198145A (en) | Dry detergent compositions | |
| CA2142222C (en) | Process for producing foamed material from waste paper and the like | |
| WO1996014391A1 (de) | Verfahren zur herstellung von wasch- und reinigungsmitteltabletten durch mikrowellen- und heissluftbehandlung | |
| DE69717816T2 (de) | Verfahren zur herstellung eines waschmittels mit niedrigem schüttgewicht durch agglomeration und anschliessender dielektrischer erwärmung | |
| US3770644A (en) | Sodium tripolyphosphate | |
| EP0560802A1 (en) | Process for the production of granular zeolites. | |
| JPS59130315A (ja) | アクリロニトリル重合体を「鎔」融紡糸する連続液相工程 | |
| EP0122289B1 (en) | Process for improving the solubility of a difficultly soluble gelling agent | |
| JPH02107514A (ja) | すぐに溶け、固化しない食品等級のトリポリリン酸ナトリウム | |
| US2798544A (en) | System for producing high density detergents | |
| US2791562A (en) | Method of producing dry detergent | |
| US3129091A (en) | Granular ureaform fertilizer | |
| RU2142960C1 (ru) | Способ получения водорастворимой очищенной гидроксиэтилцеллюлозы | |
| CN115259208A (zh) | 利用废铜箔高纯浸出液喷雾热解生产无水硫酸铜的工艺 | |
| US1621506A (en) | Manufacture of a finely-divided dry soap product | |
| JPH10132997A (ja) | 放射性廃棄物の固化処理方法およびその装置 |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| MKEX | Expiry |