BR112018077067A2 - processo para preparar um composto. - Google Patents

processo para preparar um composto.

Info

Publication number
BR112018077067A2
BR112018077067A2 BR112018077067A BR112018077067A BR112018077067A2 BR 112018077067 A2 BR112018077067 A2 BR 112018077067A2 BR 112018077067 A BR112018077067 A BR 112018077067A BR 112018077067 A BR112018077067 A BR 112018077067A BR 112018077067 A2 BR112018077067 A2 BR 112018077067A2
Authority
BR
Brazil
Prior art keywords
preparing
compound
methyl
cyclopentadecanedione
pentadecenes
Prior art date
Application number
BR112018077067A
Other languages
English (en)
Other versions
BR112018077067B1 (pt
Inventor
Bru Roig Miriam
Ruedenauer Stefan
Original Assignee
Basf Se
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Basf Se filed Critical Basf Se
Publication of BR112018077067A2 publication Critical patent/BR112018077067A2/pt
Publication of BR112018077067B1 publication Critical patent/BR112018077067B1/pt

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/61—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups
    • C07C45/65—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups by splitting-off hydrogen atoms or functional groups; by hydrogenolysis of functional groups
    • C07C45/66—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups by splitting-off hydrogen atoms or functional groups; by hydrogenolysis of functional groups by dehydration
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/61—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups
    • C07C45/64—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups by introduction of functional groups containing oxygen only in singly bound form
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/61—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/78—Separation; Purification; Stabilisation; Use of additives
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C49/00—Ketones; Ketenes; Dimeric ketenes; Ketonic chelates
    • C07C49/587—Unsaturated compounds containing a keto groups being part of a ring
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
    • C07D307/77—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom ortho- or peri-condensed with carbocyclic rings or ring systems
    • C07D307/93—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom ortho- or peri-condensed with carbocyclic rings or ring systems condensed with a ring other than six-membered

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Heterocyclic Carbon Compounds Containing A Hetero Ring Having Oxygen Or Sulfur (AREA)
  • Fats And Perfumes (AREA)
  • Furan Compounds (AREA)

Abstract

a presente invenção se refere a um método para preparar 14-metil-16-oxabiciclo¬[10,3.1]pentadecenos em um sistema de duas etapas a partir de 3-metil-1,5-ciclopentadecano¬diona como material de partida.
BR112018077067-1A 2016-07-15 2017-07-14 Processo para preparar um composto BR112018077067B1 (pt)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP16179692.5 2016-07-15
EP16179692 2016-07-15
PCT/EP2017/067811 WO2018011386A1 (en) 2016-07-15 2017-07-14 Preparation of 14-methyl-16-oxabicyclo[10.3.1]pentadecenes from 3-methyl-1,5-cyclopentadecanedione

Publications (2)

Publication Number Publication Date
BR112018077067A2 true BR112018077067A2 (pt) 2019-04-02
BR112018077067B1 BR112018077067B1 (pt) 2022-05-31

Family

ID=56418410

Family Applications (1)

Application Number Title Priority Date Filing Date
BR112018077067-1A BR112018077067B1 (pt) 2016-07-15 2017-07-14 Processo para preparar um composto

Country Status (8)

Country Link
US (1) US10800724B2 (pt)
EP (1) EP3484844B1 (pt)
JP (1) JP7039551B2 (pt)
CN (1) CN109476577A (pt)
BR (1) BR112018077067B1 (pt)
ES (1) ES2954272T3 (pt)
MX (1) MX2019000664A (pt)
WO (1) WO2018011386A1 (pt)

Families Citing this family (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP3170828A1 (de) * 2015-11-23 2017-05-24 Basf Se Verfahren zur herstellung von verbindungen mit 16-oxabicyclo[10.3.1]pentadecengerüst und deren folgeprodukten
EP3481844B1 (en) 2016-07-11 2024-04-17 Sage Therapeutics, Inc. C7, c12, and c16 substituted neuroactive steroids and their methods of use
JP7239557B2 (ja) * 2017-11-01 2023-03-14 フイルメニツヒ ソシエテ アノニム 二環式エノールエーテルを製造する方法
JP7074869B2 (ja) * 2018-09-28 2022-05-24 花王株式会社 環状エノールエーテル化合物の製造方法
CN113302195A (zh) * 2019-01-17 2021-08-24 国际香料和香精公司 14-甲基-16-氧杂二环[10.3.1]十六碳-12-烯的合成
JP7121187B2 (ja) * 2019-03-18 2022-08-17 花王株式会社 α－アリル化シクロアルカノンを製造する方法
US11685705B2 (en) 2019-03-18 2023-06-27 Kao Corporation Method for producing α-allylated cycloalkanone
EP3870587A1 (en) * 2019-04-15 2021-09-01 Firmenich SA Process for preparing bicyclic enolether
GB202011259D0 (en) * 2020-07-21 2020-09-02 Givaudan Sa Method for the production of musk fragrance ingredient
JP2023151195A (ja) * 2022-03-31 2023-10-16 花王株式会社 環状ジケトン化合物の製造方法
JP2023151194A (ja) * 2022-03-31 2023-10-16 花王株式会社 環状ジケトン化合物の製造方法

Family Cites Families (25)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CH513791A (de) * 1966-12-08 1971-10-15 Firmenich & Cie Verfahren zur Herstellung von makrocyclischen Verbindungen
CH519454A (de) 1966-02-08 1972-02-29 Firmenich & Cie Verfahren zur Herstellung von makrocyclischen Verbindungen
CH503680A (de) 1966-12-08 1971-02-28 Firmenich & Cie Verfahren zur Herstellung von makrocyclischen Ketonen
DE2916418A1 (de) 1979-04-23 1980-11-06 Basf Ag Verfahren zur herstellung von 14- methyl-bicyclo- eckige klammer auf 10.3.0. eckige klammer zu -pentadecen- eckige klammer auf 1(12) eckige klammer zu und neue zwischenprodukte dieses verfahrens
CH642342A5 (fr) * 1979-09-13 1984-04-13 Firmenich & Cie Procede pour la preparation de muscone.
EP0584477B1 (fr) * 1992-07-30 1997-09-24 Firmenich Sa Utilisation d'une cyclopentadécénone à titre d'ingrédient parfumant
ATE411270T1 (de) * 2004-02-16 2008-10-15 Firmenich & Cie Verfahren zur herstellung von optisch aktiven cyclohexenonen
ES2367229T3 (es) * 2008-02-01 2011-10-31 Firmenich S.A. Ciclohexenonas sustituidas.
US9896644B2 (en) * 2014-01-14 2018-02-20 Firmenich Sa Powdery, musky odorant macrocycles
US20170275225A1 (en) 2014-09-09 2017-09-28 Basf Se Method for the preparation of 2-alkoxy cyclohexanol
US20170283352A1 (en) 2014-09-09 2017-10-05 Basf Se Method for producing an aroma substance
US10160931B2 (en) 2014-09-26 2018-12-25 Basf Se Use of isomerically pure or highly isomer-enriched cis- or trans-(2-isobutyl-4-methyl-tetrahydropyran-4-yl)acetate
CN107001201A (zh) 2014-11-18 2017-08-01 巴斯夫欧洲公司 制备1‑(2,6,6‑三甲基环己基)‑链烷‑3‑醇的方法
JP6612349B2 (ja) 2014-12-19 2019-11-27 ビーエーエスエフ ソシエタス・ヨーロピア 新規香料としての１−（７，１０，１０−トリメチル−４−ビシクロ［６．２．０］デカニル）エタノン
WO2016104474A1 (ja) * 2014-12-26 2016-06-30 花王株式会社 環状ジケトン化合物の製造方法
EP3265451B1 (de) 2015-03-05 2020-08-26 Basf Se Verfahren zur herstellung von tetrahydropyranylestern
WO2016184948A1 (en) 2015-05-20 2016-11-24 Basf Se Process for preparing a macrocyclic diketone
US20180171262A1 (en) 2015-05-29 2018-06-21 Basf Se Novel aroma chemicals having a 1,2,2-trimethylcyclopentan-1-yl moiety
CN107709283B (zh) 2015-06-03 2021-02-02 巴斯夫欧洲公司 制备3-甲基环十五烷-1,5-二酮的方法
CN108026062B (zh) 2015-07-10 2022-04-12 巴斯夫欧洲公司 将2-取代丁二烯醛化的方法及其次要产物，特别是降龙涎香醚的生产方法
JP2018522007A (ja) 2015-07-15 2018-08-09 ビーエーエスエフ ソシエタス・ヨーロピアＢａｓｆ Ｓｅ アリールプロペンの調製方法
WO2017009458A1 (en) 2015-07-15 2017-01-19 Basf Se Process for preparing an arylpropene
ES2779460T3 (es) 2015-08-18 2020-08-17 Basf Se Proceso de preparación del alfa-damascona
MX2018003591A (es) 2015-09-22 2018-06-18 Basf Se Proceso para preparar 3-metilciclopentadecano-1, 5-diol.
EP3170828A1 (de) 2015-11-23 2017-05-24 Basf Se Verfahren zur herstellung von verbindungen mit 16-oxabicyclo[10.3.1]pentadecengerüst und deren folgeprodukten

Also Published As

Publication number Publication date
JP2019521141A (ja) 2019-07-25
US20190300467A1 (en) 2019-10-03
BR112018077067B1 (pt) 2022-05-31
US10800724B2 (en) 2020-10-13
MX2019000664A (es) 2019-05-20
WO2018011386A1 (en) 2018-01-18
JP7039551B2 (ja) 2022-03-22
ES2954272T3 (es) 2023-11-21
EP3484844A1 (en) 2019-05-22
CN109476577A (zh) 2019-03-15
EP3484844B1 (en) 2023-06-14

Similar Documents

Publication Publication Date Title
BR112018077067A2 (pt) processo para preparar um composto.
BR112014019909A8 (pt) Processo para produção de compostos úteis como antagonistas do receptor de orexina-2
BR112014026802A2 (pt) processo para a preparação de um a, \omega-cn diol.
PL2994229T3 (pl) Sposób wytwarzania 1,3-butadienu
EP3080078B8 (en) Process for preparing alkanesulfonic acids
MX2016007297A (es) Proceso para purificar 2,5-diclorofenol.
IL265319A (en) Process for preparing 2-exo-(2-methylbenzyloxy)-1-methyl-4-isopropyl-7-oxabicyclo[2.2.1]heptane
BR112017001177A2 (pt) processo para a purificação de poliovírus a partir de culturas celulares
IN2014MU00455A (pt)
BR112017009205A2 (pt) método para preparar bifenilaminas a partir de azobenzenos por catálise de rutênio
IN2013CH04023A (pt)
MX2015015151A (es) Metodo para producir 4-hidroxi-4-metil-tetrahidropiranos 2-sustituidos, donde dicho proceso usa reciclado.
WO2015169738A3 (de) Verfahren und vorrichtung zur strukturweisen herstellung eines hydridspeichers mit einem 3d-drucker
BR112018002930A2 (pt) processo para preparação de um composto.
CO2017000010A2 (es) Proceso para la preparacion de ácidos 3-hidroxipicolínicos
BR112017018993A2 (pt) Processo para preparar 3-cloro-2- vinilfenilassulfonatos
BR112017011275A2 (pt) composição, e, processo para a produção de xarope de glicose.
BR112015020725A2 (pt) ariloxi-ftalocianinas de metais do grupo iv
CL2018000962A1 (es) Oportunidades para el proceso de aumento de recuperación según se aplica a la producción de molibdeno
BR112014015890A8 (pt) processo para a produção de 1, 3-butadieno
EP3511313A4 (en) PROCESS FOR THE PREPARATION OF 1,3-CYCLOHEXANEDIMETHANOL
BR112015009563A2 (pt) processo para preparação de um produto olefínico.
BR112014031249A2 (pt) composição estabilizadora, composição de batelada mestre, e, processo para produzir um artigo moldado.
IN2013MU02726A (pt)
BR112014018492A8 (pt) Processo aperfeiçoado para a produção de etileno 1,1-disubstituído

Legal Events

Date Code Title Description
B350 Update of information on the portal [chapter 15.35 patent gazette]
B06W Patent application suspended after preliminary examination (for patents with searches from other patent authorities) chapter 6.23 patent gazette]
B09A Decision: intention to grant [chapter 9.1 patent gazette]
B16A Patent or certificate of addition of invention granted [chapter 16.1 patent gazette]

Free format text: PRAZO DE VALIDADE: 20 (VINTE) ANOS CONTADOS A PARTIR DE 14/07/2017, OBSERVADAS AS CONDICOES LEGAIS