BR0315006A - Composição de revestimento capaz de ser eletrodepositada, método para preparar a mesma e método para eletro-revestir um substrato condutor - Google Patents
Composição de revestimento capaz de ser eletrodepositada, método para preparar a mesma e método para eletro-revestir um substrato condutorInfo
- Publication number
- BR0315006A BR0315006A BR0315006-2A BR0315006A BR0315006A BR 0315006 A BR0315006 A BR 0315006A BR 0315006 A BR0315006 A BR 0315006A BR 0315006 A BR0315006 A BR 0315006A
- Authority
- BR
- Brazil
- Prior art keywords
- coating
- composition
- preparing
- electro
- conductive substrate
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/44—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes for electrophoretic applications
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/08—Processes
- C08G18/16—Catalysts
- C08G18/22—Catalysts containing metal compounds
- C08G18/24—Catalysts containing metal compounds of tin
- C08G18/242—Catalysts containing metal compounds of tin organometallic compounds containing tin-carbon bonds
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/08—Processes
- C08G18/0804—Manufacture of polymers containing ionic or ionogenic groups
- C08G18/0809—Manufacture of polymers containing ionic or ionogenic groups containing cationic or cationogenic groups
- C08G18/0814—Manufacture of polymers containing ionic or ionogenic groups containing cationic or cationogenic groups containing ammonium groups or groups forming them
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
- C08G18/40—High-molecular-weight compounds
- C08G18/58—Epoxy resins
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
- C08G18/40—High-molecular-weight compounds
- C08G18/64—Macromolecular compounds not provided for by groups C08G18/42 - C08G18/63
- C08G18/6415—Macromolecular compounds not provided for by groups C08G18/42 - C08G18/63 having nitrogen
- C08G18/643—Reaction products of epoxy resins with at least equivalent amounts of amines
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/70—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the isocyanates or isothiocyanates used
- C08G18/72—Polyisocyanates or polyisothiocyanates
- C08G18/80—Masked polyisocyanates
- C08G18/8003—Masked polyisocyanates masked with compounds having at least two groups containing active hydrogen
- C08G18/8006—Masked polyisocyanates masked with compounds having at least two groups containing active hydrogen with compounds of C08G18/32
- C08G18/8009—Masked polyisocyanates masked with compounds having at least two groups containing active hydrogen with compounds of C08G18/32 with compounds of C08G18/3203
- C08G18/8012—Masked polyisocyanates masked with compounds having at least two groups containing active hydrogen with compounds of C08G18/32 with compounds of C08G18/3203 with diols
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/70—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the isocyanates or isothiocyanates used
- C08G18/72—Polyisocyanates or polyisothiocyanates
- C08G18/80—Masked polyisocyanates
- C08G18/8003—Masked polyisocyanates masked with compounds having at least two groups containing active hydrogen
- C08G18/8006—Masked polyisocyanates masked with compounds having at least two groups containing active hydrogen with compounds of C08G18/32
- C08G18/8009—Masked polyisocyanates masked with compounds having at least two groups containing active hydrogen with compounds of C08G18/32 with compounds of C08G18/3203
- C08G18/8012—Masked polyisocyanates masked with compounds having at least two groups containing active hydrogen with compounds of C08G18/32 with compounds of C08G18/3203 with diols
- C08G18/8019—Masked aromatic polyisocyanates
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/70—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the isocyanates or isothiocyanates used
- C08G18/72—Polyisocyanates or polyisothiocyanates
- C08G18/80—Masked polyisocyanates
- C08G18/8061—Masked polyisocyanates masked with compounds having only one group containing active hydrogen
- C08G18/8064—Masked polyisocyanates masked with compounds having only one group containing active hydrogen with monohydroxy compounds
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/44—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes for electrophoretic applications
- C09D5/4419—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes for electrophoretic applications with polymers obtained otherwise than by polymerisation reactions only involving carbon-to-carbon unsaturated bonds
- C09D5/443—Polyepoxides
- C09D5/4457—Polyepoxides containing special additives, e.g. pigments, polymeric particles
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/44—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes for electrophoretic applications
- C09D5/4488—Cathodic paints
- C09D5/4492—Cathodic paints containing special additives, e.g. grinding agents
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Polymers & Plastics (AREA)
- Medicinal Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Molecular Biology (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Inorganic Chemistry (AREA)
- Manufacturing & Machinery (AREA)
- Paints Or Removers (AREA)
- Polyurethanes Or Polyureas (AREA)
Abstract
"COMPOSIçãO DE REVESTIMENTO CAPAZ DE SER ELETRODEPOSITADA, MéTODO PARA PREPARAR A MESMA E MéTODO PARA ELETRO-REVESTIR UM SUBSTRATO CONDUTOR". Proporciona-se uma composição de revestimento capaz de ser eletrodepositada de uma fase resinosa dispersada em um meio aquoso, sendo que a fase resinosa inclui (a) uma resina que contém um grupo de sal catiónico, que contém hidrogênio ativo; e (b) pelo menos um agente de cura de poliisocianato bloqueado pelo menos parcialmente. A composição contém um catalisador de organo-estanho que é um composto de dialquilestanho, ou é derivado do mesmo, que tem a estrutura (I): [R1] [R2] -Sn=O, onde R~ 1~ e R~ 2~ são os mesmos ou diferentes e cada um independentemente representa um grupo de hidrocarboneto monovalente em que a soma dos átomos de carbono em R~ 1~ e R~ 2~ é maior do que 8. O catalisador encontra-se presente em uma quantidade suficiente para efetuar a cura sob uma temperatura de 171,1<198>C (340<198>F) ou abaixo da mesma. Proporcionam-se igualmente métodos para a preparação e utilização da composição.
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US41514602P | 2002-10-01 | 2002-10-01 | |
US60/415,146 | 2002-10-01 | ||
PCT/US2003/031258 WO2004031306A1 (en) | 2002-10-01 | 2003-10-01 | Electrodepositable coating compositions and related methods |
Publications (2)
Publication Number | Publication Date |
---|---|
BR0315006A true BR0315006A (pt) | 2005-08-09 |
BR0315006B1 BR0315006B1 (pt) | 2014-06-17 |
Family
ID=32069817
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
BRPI0315006-2A BR0315006B1 (pt) | 2002-10-01 | 2003-10-01 | Composição de revestimento capaz de ser eletrodepositada e método para preparar a composição de revestimento capaz de ser eletrodepositada |
Country Status (12)
Country | Link |
---|---|
US (2) | US7497936B2 (pt) |
EP (1) | EP1546271B1 (pt) |
JP (2) | JP2006501357A (pt) |
KR (1) | KR100791701B1 (pt) |
CN (1) | CN100582172C (pt) |
AU (1) | AU2003277236B2 (pt) |
BR (1) | BR0315006B1 (pt) |
CA (1) | CA2500436C (pt) |
ES (1) | ES2572974T3 (pt) |
HU (1) | HUE029209T2 (pt) |
MX (1) | MXPA05003458A (pt) |
WO (1) | WO2004031306A1 (pt) |
Families Citing this family (20)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US20050008821A1 (en) * | 2003-07-07 | 2005-01-13 | Pricone Robert M. | Process and apparatus for fabricating precise microstructures and polymeric molds for making same |
US8226880B2 (en) * | 2003-07-07 | 2012-07-24 | 10X Technology, Llc | Process for fabricating precise microstructures |
US6969754B2 (en) * | 2003-12-11 | 2005-11-29 | Valspar Sourcing, Inc. | Blocked isocyanate crosslinker solution |
US20070259172A1 (en) * | 2006-05-02 | 2007-11-08 | Scott Matthew S | Coating compositions exhibiting corrosion resistance properties, related coated articles and methods |
US20070256590A1 (en) * | 2006-05-02 | 2007-11-08 | Scott Matthew S | Coating compositions exhibiting corrosion resistance properties, related coated articles and methods |
US8748007B2 (en) * | 2006-05-02 | 2014-06-10 | Ppg Industries Ohio, Inc. | Coating compositions exhibiting corrosion resistance properties, related coated articles and methods |
US8039551B2 (en) | 2007-07-20 | 2011-10-18 | Ppg Industries Ohio, Inc. | Modified epoxy resins comprising the reaction product of rosin and a linking molecule and aqueous dispersions and coatings comprising such resins |
US7812101B2 (en) | 2007-07-20 | 2010-10-12 | Ppg Industries Ohio, Inc. | Modified epoxy resins comprising the reaction product of a biomass derived compound and an epoxy resin, and aqueous dispersions and coatings comprising such resins |
US8057592B2 (en) * | 2007-07-20 | 2011-11-15 | Ppg Industries Ohio, Inc. | Cationic electrodepositable coatings comprising rosin |
DE102007038824A1 (de) * | 2007-08-16 | 2009-02-19 | Basf Coatings Ag | Einsatz von Bismutsubnitrat in Elektrotauchlacken |
JP5721307B2 (ja) * | 2007-10-17 | 2015-05-20 | 関西ペイント株式会社 | 複層皮膜形成方法及び塗装物品 |
US20090143526A1 (en) * | 2007-11-29 | 2009-06-04 | Kansai Paint Co., Ltd. | Coating composition and coated article |
DE102008012085A1 (de) * | 2008-02-29 | 2009-09-10 | Basf Coatings Ag | Kathodischer Elektrotauchlack enthaltend metallorganische Verbindung |
US8574414B2 (en) * | 2010-07-14 | 2013-11-05 | Ppg Industries Ohio, Inc | Copper prerinse for electrodepositable coating composition comprising yttrium |
JP5473983B2 (ja) | 2011-04-28 | 2014-04-16 | トヨタ自動車株式会社 | カチオン電着塗料組成物及び塗装物品 |
JP5718753B2 (ja) * | 2011-07-19 | 2015-05-13 | 日本パーカライジング株式会社 | 金属表面処理用水性組成物、これを用いた金属表面処理方法及び皮膜付金属材料の製造方法並びにこれらを用いた金属表面処理皮膜 |
US9534074B2 (en) * | 2012-06-25 | 2017-01-03 | Ppg Industries Ohio, Inc. | Aqueous resinous dispersions that include a zinc (II) amidine complex and methods for the manufacture thereof |
ES2850286T3 (es) * | 2015-05-21 | 2021-08-26 | Swimc Llc | Agente antimicrobiano para la composición del recubrimiento |
CA3029554C (en) * | 2016-06-30 | 2021-01-26 | Ppg Industries Ohio, Inc. | Electrodepositable coating composition having improved crater control |
EP4077551A1 (en) * | 2019-12-20 | 2022-10-26 | PPG Industries Ohio Inc. | Electrodepositable coating composition including a phyllosilicate pigment and a dispersing agent |
Family Cites Families (20)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPH0676567B2 (ja) * | 1986-06-16 | 1994-09-28 | 関西ペイント株式会社 | カチオン電着塗料用樹脂組成物 |
AT390808B (de) | 1986-09-19 | 1990-07-10 | Vianova Kunstharz Ag | Verwendung von zinn-kondensationsprodukten zur katalysierung der vernetzungsreaktionen von kathodisch abscheidbaren lackbindemitteln |
JPH0832840B2 (ja) | 1987-09-09 | 1996-03-29 | 三共有機合成株式会社 | カチオン電着塗料用硬化触媒 |
US4981924A (en) | 1989-09-11 | 1991-01-01 | Air Products And Chemicals, Inc. | Cationic electrodepositable compositions of blocked polyisocyanates and amine-epoxy resins containing diorganotin bis-mercaptides and bis-carboxylates as catalysts |
US5116914A (en) | 1990-12-18 | 1992-05-26 | E. I. Du Pont De Nemours And Company | Cathodic electrodeposition coatings containing alkyl metal acetonate catalyst |
JP2983370B2 (ja) | 1991-04-16 | 1999-11-29 | 関西ペイント株式会社 | 電着塗料組成物 |
CA2084455C (en) * | 1991-12-06 | 1996-09-17 | Toshiyuki Ishii | Hydrophilic resin containing oxazolidone rings and coating composition containing same |
JPH05271582A (ja) | 1992-03-27 | 1993-10-19 | Kansai Paint Co Ltd | 電着塗料組成物 |
US5356529A (en) | 1993-05-03 | 1994-10-18 | Ppg Industries, Inc. | Electrodepositable compositions containing triorganotin catalysts |
US5446077A (en) * | 1993-05-17 | 1995-08-29 | Nippon Paint Company, Ltd. | Oxazolidone ring-containing modified epoxy resins and cathodic electrodeposition paints containing same |
US5718817A (en) | 1993-07-28 | 1998-02-17 | Elf Atochem North America, Inc. | Catalyst for low temperature cure of blocked isocyanates |
ATE173488T1 (de) * | 1994-10-25 | 1998-12-15 | Ppg Industries Inc | Elektrotauchlackzusammensetzungen mit verbesserten härtungseigenschaften |
US5767191A (en) | 1994-10-25 | 1998-06-16 | Ppg Industries, Inc. | Electrodepositable coating compositions and method for improved cure response |
US5630922A (en) * | 1995-12-26 | 1997-05-20 | Ppg Industries, Inc. | Electrodepositable coating composition containing diorganotin dicarboxylates |
DE19613685C1 (de) * | 1996-04-05 | 1997-09-11 | Herberts Gmbh | Säurefreie Katalysatorpaste, deren Herstellung und Verwendung bei der kathodischen Elektrotauchlackierung |
WO1999006493A1 (fr) * | 1997-07-29 | 1999-02-11 | Kansai Paint Co., Ltd. | Composition de revetement pour electrodeposition cationique |
US5972189A (en) * | 1998-05-29 | 1999-10-26 | Ppg Industries Ohio, Inc. | Electrodepositable coating composition containing bismuth diorganodithiocarbamates and method of electrodeposition |
US6123822A (en) | 1998-12-09 | 2000-09-26 | E. I. Du Pont De Nemours And Company | Clear cathodic electrocoating compositions |
EP1233992A1 (en) * | 1999-03-17 | 2002-08-28 | E.I. Du Pont De Nemours And Company | High solid epoxy, melamine and isocyanate compositions |
JP3490991B2 (ja) * | 2001-09-17 | 2004-01-26 | 関西ペイント株式会社 | カチオン性塗料組成物 |
-
2003
- 2003-10-01 HU HUE03799399A patent/HUE029209T2/en unknown
- 2003-10-01 EP EP03799399.5A patent/EP1546271B1/en not_active Expired - Lifetime
- 2003-10-01 WO PCT/US2003/031258 patent/WO2004031306A1/en active Application Filing
- 2003-10-01 MX MXPA05003458A patent/MXPA05003458A/es active IP Right Grant
- 2003-10-01 US US10/677,019 patent/US7497936B2/en active Active
- 2003-10-01 CA CA002500436A patent/CA2500436C/en not_active Expired - Fee Related
- 2003-10-01 JP JP2004542058A patent/JP2006501357A/ja active Pending
- 2003-10-01 KR KR1020057005642A patent/KR100791701B1/ko not_active IP Right Cessation
- 2003-10-01 ES ES03799399.5T patent/ES2572974T3/es not_active Expired - Lifetime
- 2003-10-01 BR BRPI0315006-2A patent/BR0315006B1/pt not_active IP Right Cessation
- 2003-10-01 CN CN200380100876A patent/CN100582172C/zh not_active Expired - Lifetime
- 2003-10-01 AU AU2003277236A patent/AU2003277236B2/en not_active Ceased
-
2008
- 2008-01-11 JP JP2008005066A patent/JP2008144181A/ja not_active Withdrawn
- 2008-12-31 US US12/346,933 patent/US8168700B2/en active Active
Also Published As
Publication number | Publication date |
---|---|
HUE029209T2 (en) | 2017-02-28 |
AU2003277236A1 (en) | 2004-04-23 |
US7497936B2 (en) | 2009-03-03 |
EP1546271B1 (en) | 2016-03-30 |
AU2003277236B2 (en) | 2007-02-08 |
US8168700B2 (en) | 2012-05-01 |
JP2008144181A (ja) | 2008-06-26 |
EP1546271A1 (en) | 2005-06-29 |
JP2006501357A (ja) | 2006-01-12 |
CN1703469A (zh) | 2005-11-30 |
BR0315006B1 (pt) | 2014-06-17 |
CN100582172C (zh) | 2010-01-20 |
US20090111916A1 (en) | 2009-04-30 |
CA2500436C (en) | 2009-12-15 |
WO2004031306A1 (en) | 2004-04-15 |
MXPA05003458A (es) | 2005-09-12 |
KR20050052522A (ko) | 2005-06-02 |
KR100791701B1 (ko) | 2008-01-03 |
US20040069637A1 (en) | 2004-04-15 |
CA2500436A1 (en) | 2004-04-15 |
ES2572974T3 (es) | 2016-06-03 |
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