BR0211582A - Processo para preparar resinas absorventes de água - Google Patents
Processo para preparar resinas absorventes de águaInfo
- Publication number
- BR0211582A BR0211582A BR0211582-4A BR0211582A BR0211582A BR 0211582 A BR0211582 A BR 0211582A BR 0211582 A BR0211582 A BR 0211582A BR 0211582 A BR0211582 A BR 0211582A
- Authority
- BR
- Brazil
- Prior art keywords
- acrylic acid
- crude
- separation
- reaction gases
- water absorbing
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F220/00—Copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and only one being terminated by only one carboxyl radical or a salt, anhydride ester, amide, imide or nitrile thereof
- C08F220/02—Monocarboxylic acids having less than ten carbon atoms; Derivatives thereof
- C08F220/04—Acids; Metal salts or ammonium salts thereof
- C08F220/06—Acrylic acid; Methacrylic acid; Metal salts or ammonium salts thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L15/00—Chemical aspects of, or use of materials for, bandages, dressings or absorbent pads
- A61L15/16—Bandages, dressings or absorbent pads for physiological fluids such as urine or blood, e.g. sanitary towels, tampons
- A61L15/22—Bandages, dressings or absorbent pads for physiological fluids such as urine or blood, e.g. sanitary towels, tampons containing macromolecular materials
- A61L15/24—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L15/00—Chemical aspects of, or use of materials for, bandages, dressings or absorbent pads
- A61L15/16—Bandages, dressings or absorbent pads for physiological fluids such as urine or blood, e.g. sanitary towels, tampons
- A61L15/42—Use of materials characterised by their function or physical properties
- A61L15/60—Liquid-swellable gel-forming materials, e.g. super-absorbents
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
- C07C51/21—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen
- C07C51/215—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of saturated hydrocarbyl groups
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
- C07C51/21—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen
- C07C51/23—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of oxygen-containing groups to carboxyl groups
- C07C51/235—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of oxygen-containing groups to carboxyl groups of —CHO groups or primary alcohol groups
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
- C07C51/21—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen
- C07C51/25—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of unsaturated compounds containing no six-membered aromatic ring
- C07C51/252—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of unsaturated compounds containing no six-membered aromatic ring of propene, butenes, acrolein or methacrolein
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/42—Separation; Purification; Stabilisation; Use of additives
- C07C51/43—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/42—Separation; Purification; Stabilisation; Use of additives
- C07C51/43—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
- C07C51/44—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation by distillation
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/42—Separation; Purification; Stabilisation; Use of additives
- C07C51/487—Separation; Purification; Stabilisation; Use of additives by treatment giving rise to chemical modification
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Health & Medical Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Life Sciences & Earth Sciences (AREA)
- Crystallography & Structural Chemistry (AREA)
- Materials Engineering (AREA)
- Epidemiology (AREA)
- Hematology (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Dispersion Chemistry (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- General Chemical & Material Sciences (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
- Solid-Sorbent Or Filter-Aiding Compositions (AREA)
Abstract
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE10138150A DE10138150A1 (de) | 2001-08-03 | 2001-08-03 | Verfahren zur Herstellung wasserabsorbierender Harze |
DE10138150.6 | 2001-08-03 | ||
PCT/EP2002/008646 WO2003014172A2 (de) | 2001-08-03 | 2002-08-02 | Verfahren zur herstellung wasserabsorbierender harze |
Publications (2)
Publication Number | Publication Date |
---|---|
BR0211582A true BR0211582A (pt) | 2004-07-13 |
BR0211582B1 BR0211582B1 (pt) | 2012-11-27 |
Family
ID=7694285
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
BRPI0211582-4A BR0211582B1 (pt) | 2001-08-03 | 2002-08-02 | processo para preparar resinas absorventes de água. |
Country Status (8)
Country | Link |
---|---|
US (1) | US7179875B2 (pt) |
EP (1) | EP1417164B1 (pt) |
CN (1) | CN1264796C (pt) |
AT (1) | ATE486836T1 (pt) |
BR (1) | BR0211582B1 (pt) |
DE (2) | DE10138150A1 (pt) |
MY (1) | MY131004A (pt) |
WO (1) | WO2003014172A2 (pt) |
Families Citing this family (53)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE10257449A1 (de) * | 2002-12-09 | 2003-11-06 | Basf Ag | Verfahren zur Herstellung geruchsarmer Hydrogel-bildender Polymerisate |
DE102004034316B4 (de) * | 2004-07-15 | 2015-07-16 | Evonik Degussa Gmbh | Ein Verfahren zur Herstellung von (Meth)Acrylsäure |
DE102005005439A1 (de) * | 2005-02-08 | 2006-08-17 | Stockhausen Gmbh | Verfahren zur Rückgewinnung von organischer Verbindungen von (Meth)Acrylsäurehaltigen Gemischen durch Extraktion mit einem protischen Lösungsmittel |
TWI522092B (zh) * | 2005-02-28 | 2016-02-21 | 贏創德固賽有限責任公司 | 丙烯酸和基於可再生原料之吸水聚合物結構及二者之製備方法 |
TWI529181B (zh) | 2005-02-28 | 2016-04-11 | 贏創德固賽有限責任公司 | 以可更新原料為基之吸水聚合物結構及其生產的方法 |
TWI353360B (en) | 2005-04-07 | 2011-12-01 | Nippon Catalytic Chem Ind | Production process of polyacrylic acid (salt) wate |
US8481664B2 (en) | 2005-04-12 | 2013-07-09 | Nippon Shokubai Co., Ltd. | Particulate water absorbing agent including polyacrylic acid (polyacrylate) based water absorbing resin as a principal component, method for production thereof, water-absorbent core and absorbing article in which the particulate water absorbing agent is used |
US20090068440A1 (en) * | 2005-06-20 | 2009-03-12 | Gunther Bub | Production of acrolein, acrylic acid and water-absorbent polymer structures made from glycerine |
US7649112B2 (en) * | 2005-07-25 | 2010-01-19 | Saudi Basic Industries Corporation | Integrated plant for producing 2-ethyl-hexanol and methacrylic acid and a method based thereon |
DE102005039156B4 (de) * | 2005-08-17 | 2014-12-24 | Evonik Degussa Gmbh | Verfahren zur Herstellung von (Meth)Acrylsäure mit Schwersiedeaufarbeitung durch Kristallisation |
DE102005048818A1 (de) | 2005-10-10 | 2007-04-12 | Degussa Ag | Mikrobiologische Herstellung von 3-Hydroxypropionsäure |
TWI394789B (zh) | 2005-12-22 | 2013-05-01 | Nippon Catalytic Chem Ind | 吸水性樹脂組成物及其製造方法、吸收性物品 |
EP1837348B9 (en) | 2006-03-24 | 2020-01-08 | Nippon Shokubai Co.,Ltd. | Water-absorbing resin and method for manufacturing the same |
CN101495543B (zh) * | 2006-07-24 | 2012-03-14 | 住友精化株式会社 | 吸水性树脂的制造方法 |
DE102006039205A1 (de) | 2006-08-22 | 2008-03-20 | Stockhausen Gmbh | Auf nachwachsenden Rohstoffen basierende Acrylsäure und wasserabsorbierende Polymergebilde sowie Verfahren zu deren Herstellung mittels Dehydratisierung |
DE102006049939A1 (de) * | 2006-10-19 | 2008-04-24 | Basf Ag | Verfahren zur Trennung von in einem Produktgasgemisch einer partiellen heterogen katalysierten Gasphasenoxidation einer C3-Vorläuferverbindung der Acrylsäure enthaltener Acrylsäure und Benzoesäure |
JP2008115103A (ja) * | 2006-11-02 | 2008-05-22 | Nippon Shokubai Co Ltd | アクリル酸の製造方法、アクリル酸製造用装置、およびアクリル酸製造用組成物 |
DE102007004960A1 (de) | 2007-01-26 | 2008-07-31 | Basf Se | Verfahren zur Herstellung von Acrylsäure |
DE102007055086A1 (de) | 2007-11-16 | 2009-05-20 | Basf Se | Verfahren zur Herstellung von Acrylsäure |
WO2008133121A1 (ja) * | 2007-04-17 | 2008-11-06 | Arkray, Inc. | 基質濃度測定方法および基質濃度測定装置 |
US20090149954A1 (en) * | 2007-12-07 | 2009-06-11 | Xianbo Hu | Bone substitute |
EP2085376B1 (en) | 2008-01-30 | 2012-09-05 | Evonik Röhm GmbH | Process for preparation of high purity methacrylic acid |
US9457048B2 (en) * | 2008-02-05 | 2016-10-04 | Wellosophy Corporation | Absorbent ingestible agents and associated methods of manufacture and use |
DE102008002715A1 (de) | 2008-06-27 | 2009-12-31 | Evonik Röhm Gmbh | 2-Hydroxyisobuttersäure produzierende rekombinante Zelle |
CA2731936C (en) * | 2008-07-31 | 2016-08-16 | Dow Technology Investments Llc | Alkylene oxide recovery systems |
CN102112531B (zh) * | 2008-07-31 | 2013-05-01 | 巴斯夫欧洲公司 | 颜色稳定的超吸收剂 |
US8053586B2 (en) | 2008-07-31 | 2011-11-08 | Dow Technology Investments Llc | Alkylene oxide recovery systems |
FR2935971B1 (fr) * | 2008-09-16 | 2010-11-19 | Arkema France | Acide bio-acrylique de grade polymere et son procede de fabrication a partir de glycerol. |
DE102008060888A1 (de) * | 2008-12-09 | 2010-06-10 | Evonik Stockhausen Gmbh | Verfahren zur Herstellung von Acrolein umfassend die Aufarbeitung einer Rohglycerin-Phase |
EP2371801A4 (en) * | 2008-12-26 | 2012-10-17 | Nippon Catalytic Chem Ind | PROCESS FOR THE PRODUCTION OF ACRYLIC ACID |
DE102009027401A1 (de) | 2009-07-01 | 2010-02-18 | Basf Se | Verfahren der Abtrennung von Acrylsäure aus dem Produktgasgemisch einer heterogen katalysierten partiellen Gasphasenoxidation wenigstens einer C3-Vorläuferverbindung |
WO2011000808A2 (de) | 2009-07-01 | 2011-01-06 | Basf Se | Verfahren der abtrennung von acrylsäure aus dem produktgasgemisch einer heterogen katalysierten partiellen gasphasenoxidation wenigstens einer c3-vorläuferverbindung |
DE102010001228A1 (de) | 2010-01-26 | 2011-02-17 | Basf Se | Verfahren der Abtrennung von Acrylsäure aus dem Produktgasgemisch einer heterogen katalysierten partiellen Gasphasenoxidation wenigstens einer C3-Vorläuferverbindung |
BR112012005901A2 (pt) | 2009-09-16 | 2019-09-24 | Basf Se | superabsorvente, processo para produzir um superabsorvente, artigo para absorver fluidos, e, processo para produzir artigos para absorver fluidos |
US8815770B2 (en) | 2009-09-17 | 2014-08-26 | Basf Se | Color-stable superabsorber |
WO2011040472A1 (ja) | 2009-09-29 | 2011-04-07 | 株式会社日本触媒 | 粒子状吸水剤及びその製造方法 |
JP2013511608A (ja) | 2009-11-23 | 2013-04-04 | ビーエーエスエフ ソシエタス・ヨーロピア | 色安定性が改善された吸水性ポリマー粒子の製造方法 |
US8703876B2 (en) | 2010-03-15 | 2014-04-22 | Basf Se | Process for producing water absorbing polymer particles with improved color stability |
FR2957594B1 (fr) * | 2010-03-18 | 2013-04-26 | Arkema France | Procede de fabrication d'acide acrylique bio-ressource de grade polymere a partir de glycerol |
DE102010028781A1 (de) | 2010-05-10 | 2011-11-10 | Evonik Stockhausen Gmbh | Abtrennung von Acrylsäure mittels einer einen Seitenabzug aufweisenden Destillationskolonne |
KR20130096218A (ko) | 2010-06-14 | 2013-08-29 | 바스프 에스이 | 개선된 색 안정성을 갖는 수분-흡수 중합체 입자 |
DE102011076931A1 (de) * | 2011-06-03 | 2012-12-06 | Basf Se | Wässrige Lösung, enthaltend Acrylsäure und deren konjugierte Base |
US20130274520A1 (en) | 2012-04-11 | 2013-10-17 | The Procter & Gamble Company | Purification Of Bio Based Acrylic Acid To Crude And Glacial Acrylic Acid |
WO2013163806A1 (en) | 2012-05-03 | 2013-11-07 | Evonik Industries Ag | Process for preparation of highly pure, non-yellowing methacrylic acid |
BR112014030203B1 (pt) | 2012-06-08 | 2021-10-13 | Cj Cheiljedang Corporation | Processo para produção de produtos de ácido acrílico de base biológica |
TWI531390B (zh) * | 2012-10-24 | 2016-05-01 | 贏創德固賽有限公司 | 氣味與顏色穩定之吸水組合物 |
JP6494520B2 (ja) * | 2012-11-26 | 2019-04-03 | ビーエーエスエフ ソシエタス・ヨーロピアBasf Se | 再生原料に基づく超吸収体の製造方法 |
EP2975065A4 (en) * | 2013-03-11 | 2016-11-16 | Sumitomo Seika Chemicals | METHOD FOR PRODUCING A WATER ABSORBENT RESIN |
WO2016162175A1 (de) * | 2015-04-07 | 2016-10-13 | Basf Se | Verfahren zur dehydratisierung von 3-hydroxypropionsäure zu acrylsäure |
EP3331847B1 (en) | 2015-08-07 | 2019-10-09 | Basf Se | Process for production of acrylic acid |
CN112969529B (zh) * | 2018-11-14 | 2023-11-10 | 巴斯夫欧洲公司 | 制备超吸收剂的方法 |
CN113769699B (zh) * | 2021-09-22 | 2022-10-21 | 安徽蓝科新材料有限公司 | 一种耐热丙烯酸脂树脂单体的制备设备及方法 |
WO2024146794A1 (de) * | 2023-01-05 | 2024-07-11 | Basf Se | Verfahren zur herstellung von superabsorbern |
Family Cites Families (19)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE2241714A1 (de) * | 1972-08-24 | 1974-03-28 | Basf Ag | Verfahren zur abtrennung von acrylsaeure aus den reaktionsgasen der propylenoder acroleinoxydation |
DE3641996A1 (de) * | 1986-12-09 | 1988-06-16 | Basf Ag | Verfahren zum abtrennen von aldehyden aus (alpha),(beta)-olefinisch ungesaettigten carbonsaeuren |
DE4308087C2 (de) | 1993-03-13 | 1997-02-06 | Basf Ag | Verfahren zur Abtrennung von Acrylsäure aus den Reaktionsgasen der katalytischen Oxidation von Propylen und/oder Acrolein |
DE4335172A1 (de) * | 1993-10-15 | 1995-04-20 | Basf Ag | Verfahren zur Reinigung von Roh-(Meth)acrylsäure |
US5759358A (en) * | 1994-05-31 | 1998-06-02 | Rohm And Haas Company | Process for pure grade acrylic acid |
US5482597A (en) * | 1994-11-23 | 1996-01-09 | Basf Aktiengesellschaft | Purification of crude (meth)acrylic acid |
US5961790A (en) * | 1994-12-14 | 1999-10-05 | Basf Aktiengesellschaft | Separation of (meth) acrylic acid by rectification |
FR2730732B1 (fr) | 1995-02-17 | 1997-04-30 | Atochem Elf Sa | Procede de valorisation, sous la forme d'un ester, de l'acide acetique contenu dans les fractions legeres de purification de l'acide acrylique |
FR2736912B1 (fr) | 1995-07-18 | 1997-08-22 | Atochem Elf Sa | Procede de purification de l'acide acrylique obtenu par oxydation catalytique du propylene |
DE19600955A1 (de) * | 1996-01-12 | 1997-07-17 | Basf Ag | Verfahren zur Herstellung von Acrylsäure und deren Ester |
DE19634614A1 (de) | 1996-08-27 | 1998-03-05 | Basf Ag | Verfahren zur destillativen Abtrennung von Rein-(Meth)acrylsäure aus Gemischen, die im wesentlichen frei sind von Komponenten, deren Siedepunkt niedriger als der der (Meth)acrylsäure ist |
FR2753445B1 (fr) | 1996-09-16 | 1998-10-30 | Atochem Elf Sa | Procede perfectionne de purification de l'acide acrylique |
DE59812096D1 (de) * | 1997-08-07 | 2004-11-11 | Basf Ag | Verfahren zur stabilisierung von (meth)acrylsäureestern gegen unerwünschte radikalische polymerisation |
DE19746689A1 (de) * | 1997-10-22 | 1999-04-29 | Basf Ag | Verfahren zur Herstellung von (Meth)acrylsäure |
US6444744B1 (en) * | 1998-03-11 | 2002-09-03 | Nippon Shokubai Co., Ltd. | Hydrophilic resin, absorbent article, and acrylic acid for polymerization |
MY122671A (en) * | 1999-03-06 | 2006-04-29 | Basf Ag | Fractional condensation of a product gas mixture containing acrylic acid |
WO2000053560A1 (de) * | 1999-03-06 | 2000-09-14 | Basf Aktiengesellschaft | Verfahren zur herstellung von acrylsäure |
JP3948855B2 (ja) * | 1999-06-10 | 2007-07-25 | 株式会社日本触媒 | (メタ)アクリル酸の製造方法 |
DE19955168A1 (de) * | 1999-11-16 | 2001-05-17 | Basf Ag | Verfahren der katalytischen Gasphasenoxidation von Propen zu Acrylsäure |
-
2001
- 2001-08-03 DE DE10138150A patent/DE10138150A1/de not_active Withdrawn
-
2002
- 2002-08-01 MY MYPI20022892A patent/MY131004A/en unknown
- 2002-08-02 BR BRPI0211582-4A patent/BR0211582B1/pt not_active IP Right Cessation
- 2002-08-02 US US10/485,484 patent/US7179875B2/en not_active Expired - Fee Related
- 2002-08-02 WO PCT/EP2002/008646 patent/WO2003014172A2/de active Application Filing
- 2002-08-02 CN CNB028152220A patent/CN1264796C/zh not_active Expired - Fee Related
- 2002-08-02 AT AT02767312T patent/ATE486836T1/de active
- 2002-08-02 DE DE50214752T patent/DE50214752D1/de not_active Expired - Lifetime
- 2002-08-02 EP EP02767312A patent/EP1417164B1/de not_active Expired - Lifetime
Also Published As
Publication number | Publication date |
---|---|
DE50214752D1 (de) | 2010-12-16 |
CN1538948A (zh) | 2004-10-20 |
MY131004A (en) | 2007-07-31 |
DE10138150A1 (de) | 2003-02-13 |
US7179875B2 (en) | 2007-02-20 |
EP1417164B1 (de) | 2010-11-03 |
WO2003014172A2 (de) | 2003-02-20 |
US20040236049A1 (en) | 2004-11-25 |
BR0211582B1 (pt) | 2012-11-27 |
WO2003014172A3 (de) | 2003-11-27 |
ATE486836T1 (de) | 2010-11-15 |
CN1264796C (zh) | 2006-07-19 |
EP1417164A2 (de) | 2004-05-12 |
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