AU8013091A - Continuous solvent pulping and washing processes and apparatus - Google Patents

Continuous solvent pulping and washing processes and apparatus

Info

Publication number
AU8013091A
AU8013091A AU80130/91A AU8013091A AU8013091A AU 8013091 A AU8013091 A AU 8013091A AU 80130/91 A AU80130/91 A AU 80130/91A AU 8013091 A AU8013091 A AU 8013091A AU 8013091 A AU8013091 A AU 8013091A
Authority
AU
Australia
Prior art keywords
solvent
image
pressure
psi
practiced
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Abandoned
Application number
AU80130/91A
Inventor
Brian F. Greenwood
David J. Lebel
Joseph R. Phillips
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Alcell Technologies Inc
Original Assignee
Alcell Technologies Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Alcell Technologies Inc filed Critical Alcell Technologies Inc
Publication of AU8013091A publication Critical patent/AU8013091A/en
Assigned to ALCELL TECHNOLOGIES INC. reassignment ALCELL TECHNOLOGIES INC. Alteration of Name(s) of Applicant(s) under S113 Assignors: KAMYR INC.
Abandoned legal-status Critical Current

Links

Classifications

    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21CPRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
    • D21C1/00Pretreatment of the finely-divided materials before digesting
    • D21C1/02Pretreatment of the finely-divided materials before digesting with water or steam
    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21CPRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
    • D21C11/00Regeneration of pulp liquors or effluent waste waters
    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21CPRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
    • D21C3/00Pulping cellulose-containing materials
    • D21C3/20Pulping cellulose-containing materials with organic solvents or in solvent environment
    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21CPRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
    • D21C3/00Pulping cellulose-containing materials
    • D21C3/22Other features of pulping processes
    • D21C3/24Continuous processes
    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21CPRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
    • D21C7/00Digesters
    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21CPRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
    • D21C9/00After-treatment of cellulose pulp, e.g. of wood pulp, or cotton linters ; Treatment of dilute or dewatered pulp or process improvement taking place after obtaining the raw cellulosic material and not provided for elsewhere
    • D21C9/02Washing ; Displacing cooking or pulp-treating liquors contained in the pulp by fluids, e.g. wash water or other pulp-treating agents
    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21CPRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
    • D21C9/00After-treatment of cellulose pulp, e.g. of wood pulp, or cotton linters ; Treatment of dilute or dewatered pulp or process improvement taking place after obtaining the raw cellulosic material and not provided for elsewhere
    • D21C9/02Washing ; Displacing cooking or pulp-treating liquors contained in the pulp by fluids, e.g. wash water or other pulp-treating agents
    • D21C9/04Washing ; Displacing cooking or pulp-treating liquors contained in the pulp by fluids, e.g. wash water or other pulp-treating agents in diffusers ; Washing of pulp of fluid consistency without substantially thickening

Landscapes

  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Wood Science & Technology (AREA)
  • Paper (AREA)
  • Medicines Containing Antibodies Or Antigens For Use As Internal Diagnostic Agents (AREA)
  • Peptides Or Proteins (AREA)
  • Treatment Of Sludge (AREA)
  • Compositions Of Macromolecular Compounds (AREA)
  • Reinforced Plastic Materials (AREA)

Abstract

A continuous solvent pulping process is practiced with oxygen free gas (e.g. nitrogen) purges of all major treatment vessels (23, 24, 85, 103, 105) during the time when the process is arrested or terminated. The wood chips or other cellulosic fibrous material to be pulped is steamed in a first horizontal steaming zone (23) at a pressure of about 10-20 psi, and then in a second horizontal steaming zone (24) at a pressure of about 20-75 psi. Gases, including vaporized solvent (e.g. ethanol or other alcohol) are vented (via 30, 36) from the steaming zones, and solvent is added (at 39) to the steamed material prior to feeding to a high pressure feeder (11) . The high pressure feeder introduces the material into the top of a single digesting vessel (12), liquid and chips being separated at the top of the digester vessel without mechanical means that could cause a spark. Lignin containing liquid is withdrawn from a central portion (14) of the digester and passed through flash tanks (51-53) and ultimately for lignin and alcohol recovery. Washing -- which also may be practiced using solvent pulp from a batch system -- is accomplished by first continuously passing the pulp to a pressure diffuser (85), then to a first multi stage drum displacer washer (103), and then to a second multi stage drum displacer washer (105). <IMAGE> <IMAGE> <IMAGE>
AU80130/91A 1990-08-17 1991-07-03 Continuous solvent pulping and washing processes and apparatus Abandoned AU8013091A (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US56912690A 1990-08-17 1990-08-17
US569126 1990-08-17

Related Child Applications (1)

Application Number Title Priority Date Filing Date
AU80442/94A Division AU683314B2 (en) 1990-08-17 1994-12-14 Continuous solvent pulping and washing processes and apparatus

Publications (1)

Publication Number Publication Date
AU8013091A true AU8013091A (en) 1992-02-20

Family

ID=24274194

Family Applications (2)

Application Number Title Priority Date Filing Date
AU80130/91A Abandoned AU8013091A (en) 1990-08-17 1991-07-03 Continuous solvent pulping and washing processes and apparatus
AU80442/94A Ceased AU683314B2 (en) 1990-08-17 1994-12-14 Continuous solvent pulping and washing processes and apparatus

Family Applications After (1)

Application Number Title Priority Date Filing Date
AU80442/94A Ceased AU683314B2 (en) 1990-08-17 1994-12-14 Continuous solvent pulping and washing processes and apparatus

Country Status (11)

Country Link
US (2) US5681427A (en)
EP (2) EP0472820B1 (en)
JP (1) JPH04240283A (en)
AT (1) ATE159778T1 (en)
AU (2) AU8013091A (en)
BR (1) BR9102275A (en)
CA (1) CA2042885A1 (en)
DE (1) DE69128059T2 (en)
FI (1) FI913315A (en)
NO (1) NO913210L (en)
ZA (1) ZA914032B (en)

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US5788812A (en) * 1985-11-05 1998-08-04 Agar; Richard C. Method of recovering furfural from organic pulping liquor
DE69628029D1 (en) * 1995-06-29 2003-06-12 K Reijo Salminen CONTINUOUS COOKER
FI960438A (en) * 1995-09-11 1997-03-12 Ahlstrom Machinery Oy Apparatus and method for cleaning a pulp scrubber from stickies
AU2400697A (en) * 1996-03-25 1997-10-17 Alcell Technologies Inc. Ozone-bleached organosolv pulps
US6284095B1 (en) 1999-02-04 2001-09-04 Andritz-Ahlstrom Inc. Minimization of malodorous gas release from a cellulose pulp mill feed system
WO2002081816A1 (en) * 2001-04-06 2002-10-17 Gerischer Guenter Friedrich Ru Wood chip treatment
SE517674E8 (en) * 2001-05-02 2015-10-20 Metso Paper Sweden Ab Method of washing liquid supply to boiling process for cellulose pulp
US6497791B1 (en) 2001-08-30 2002-12-24 Jack T. Baker Apparatus for pre-treatment of wood chips
WO2004005608A1 (en) * 2002-07-02 2004-01-15 Andritz, Inc. Solvent pulping of biomass
US20090176286A1 (en) * 2005-11-23 2009-07-09 O'connor Ryan P Process for Fractionating Lignocellulosic Biomass into Liquid and Solid Products
US20090062516A1 (en) * 2006-05-08 2009-03-05 Biojoule Limited Lignin and other products isolated from plant material, methods for isolation and use, and compositions containing lignin and other plant-derived products
CA2651628C (en) * 2006-05-08 2015-01-06 Biojoule Ltd. Process for the production of biofuel from plant materials
US7976677B2 (en) * 2006-12-18 2011-07-12 International Paper Company Process of bleaching hardwood pulps in a D1 or D2 stage in a presence of a weak base
US7976676B2 (en) * 2006-12-18 2011-07-12 International Paper Company Process of bleaching softwood pulps in a D1 or D2 stage in a presence of a weak base
JP5215706B2 (en) * 2007-08-01 2013-06-19 三井造船株式会社 Solid-gas two-phase material pushing device
AU2008293139A1 (en) * 2007-08-31 2009-03-05 Vertichem Corporation Lignin and other products isolated from plant material, and methods and compositions therefor
FI121885B (en) * 2007-11-09 2011-05-31 Chempolis Oy A process for making a sugar product
GB0818093D0 (en) * 2008-10-02 2008-11-05 Weyland As Method
GB0819406D0 (en) 2008-10-22 2008-11-26 Weyland As Process
US8378020B1 (en) 2009-05-28 2013-02-19 Lignol Innovations Ltd. Processes for recovery of derivatives of native lignin
CA2798161C (en) 2009-05-28 2018-06-19 Lignol Innovations Ltd. Derivatives of native lignin from softwood feedstocks
CA2763742C (en) 2009-05-28 2013-01-08 Lignol Innovations Ltd. Resin compositions comprising lignin derivatives
EP2536780A4 (en) 2010-02-15 2013-11-13 Lignol Innovations Ltd Carbon fibre compositions comprising lignin derivatives
CA2824446C (en) 2010-02-15 2018-09-18 Lignol Innovations Ltd. Binder compositions comprising lignin derivatives
GB2488918B (en) 2010-06-26 2014-03-05 Virdia Ltd Sugar mixtures and methods for production and use thereof
IL206678A0 (en) 2010-06-28 2010-12-30 Hcl Cleantech Ltd A method for the production of fermentable sugars
EP2588664B1 (en) 2010-06-30 2017-01-18 Fibria Innovations Inc. Organosolv process
IL207329A0 (en) 2010-08-01 2010-12-30 Robert Jansen A method for refining a recycle extractant and for processing a lignocellulosic material and for the production of a carbohydrate composition
IL207945A0 (en) 2010-09-02 2010-12-30 Robert Jansen Method for the production of carbohydrates
PT106039A (en) 2010-12-09 2012-10-26 Hcl Cleantech Ltd PROCESSES AND SYSTEMS FOR PROCESSING LENHOCELLULOSIC MATERIALS AND RELATED COMPOSITIONS
CN103459511A (en) 2011-03-24 2013-12-18 丽格诺创新有限公司 Compositions comprising lignocellulosic biomass and organic solvent
GB2505148B8 (en) 2011-04-07 2016-12-07 Virdia Ltd Lignocellulose conversion processes and products
US9617608B2 (en) 2011-10-10 2017-04-11 Virdia, Inc. Sugar compositions
US9493851B2 (en) 2012-05-03 2016-11-15 Virdia, Inc. Methods for treating lignocellulosic materials
SG11201407183SA (en) 2012-05-03 2014-12-30 Virdia Ltd Methods for treating lignocellulosic materials
US9657146B2 (en) 2013-03-14 2017-05-23 Virdia, Inc. Methods for treating lignocellulosic materials
EP2992041B1 (en) 2013-05-03 2020-01-08 Virdia, Inc. Methods for treating lignocellulosic materials
KR20160007537A (en) 2013-05-03 2016-01-20 버디아, 인크. Methods for preparing thermally stable lignin fractions
JP6687594B2 (en) 2014-07-09 2020-04-22 ヴァーディア, インコーポレイテッド Method for separating and purifying lignin from black liquor and composition thereof
CN112226466A (en) 2015-01-07 2021-01-15 威尔迪亚公司 Method for extracting and converting hemicellulose sugars
CN107849620B (en) 2015-05-27 2022-01-11 威尔迪亚有限责任公司 Integrated process for treating lignocellulosic material
SE1650664A1 (en) 2016-05-17 2017-10-17 Valmet Oy Method for generation of clean steam in a continuous digester system
EP3612511A4 (en) 2017-04-20 2021-01-20 Spero Renewables, Llc. Extraction of natural ferulate and coumarate from biomass
CN116084197A (en) * 2022-12-27 2023-05-09 中国海诚工程科技股份有限公司 Straw ethanol-process displacement cooking process

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US3530034A (en) * 1969-05-16 1970-09-22 Itt Rayonier Inc Continuous aqueous prehydrolysis of wood chips
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CA1079008A (en) * 1975-10-24 1980-06-10 Cp Associates Limited Solvent pulping process
US4096027A (en) * 1976-02-19 1978-06-20 Kamyr Inc. System for presteaming wood chips at or near atmospheric pressure with minimum displacement of air
FI58953B (en) * 1977-12-22 1981-01-30 Valmet Oy EXTENSION OF MEASUREMENT OF THERMAL MECHANICAL MASS OF BODY MACHINERY
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CA1147105A (en) * 1980-04-24 1983-05-31 Morris Wayman Process for depolymerization and extraction of lignin
SE422604B (en) * 1980-08-29 1982-03-15 Modo Chemetics Ab PROCEDURE FOR FLOOD PREPARATION
US4430029A (en) 1980-11-21 1984-02-07 Kamyr, Inc. High pressure feeder deflection compensation
DE3212767A1 (en) * 1982-04-06 1983-10-06 Nicolaus Md Verwaltungsges METHOD AND REACTOR FOR CONTINUOUSLY UNLOCKING PLANT FIBER MATERIAL
SE451605B (en) * 1983-06-27 1987-10-19 Mo Och Domsjoe Ab PROCEDURE AND DEVICE FOR PROCESSING LIGNOCELLULOSAMATERIAL
US4516887A (en) 1983-07-27 1985-05-14 Kamyr, Inc. Feeder deflection compensation
US4764596A (en) 1985-11-05 1988-08-16 Repap Technologies Inc. Recovery of lignin
CA1278294C (en) * 1987-09-17 1990-12-27 George S. Ritchie Method for fractionation of lignins from steam exploded lignocellulosics to provide fractions with different, but reproducible properties,and some methods for their interconversions and the products so produced
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US5053108A (en) * 1989-06-28 1991-10-01 Kamyr Ab High sulfidity cook for paper pulp using black liquor sulfonization of steamed chips

Also Published As

Publication number Publication date
FI913315A (en) 1992-02-18
BR9102275A (en) 1992-04-28
NO913210D0 (en) 1991-08-16
NO913210L (en) 1992-02-18
FI913315A0 (en) 1991-07-09
JPH04240283A (en) 1992-08-27
AU683314B2 (en) 1997-11-06
AU8044294A (en) 1995-02-16
EP0472820A3 (en) 1992-12-23
US5865948A (en) 1999-02-02
ATE159778T1 (en) 1997-11-15
EP0472820B1 (en) 1997-10-29
CA2042885A1 (en) 1992-02-18
ZA914032B (en) 1992-02-26
EP0763622A2 (en) 1997-03-19
DE69128059T2 (en) 1998-02-26
DE69128059D1 (en) 1997-12-04
US5681427A (en) 1997-10-28
EP0763622A3 (en) 1999-08-25
EP0472820A2 (en) 1992-03-04

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