AU2017320463B2 - Improved system and method for the production of blended powders - Google Patents
Improved system and method for the production of blended powders Download PDFInfo
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- AU2017320463B2 AU2017320463B2 AU2017320463A AU2017320463A AU2017320463B2 AU 2017320463 B2 AU2017320463 B2 AU 2017320463B2 AU 2017320463 A AU2017320463 A AU 2017320463A AU 2017320463 A AU2017320463 A AU 2017320463A AU 2017320463 B2 AU2017320463 B2 AU 2017320463B2
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F23/00—Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
- B01F23/60—Mixing solids with solids
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F23/00—Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
- B01F23/60—Mixing solids with solids
- B01F23/69—Mixing systems, i.e. flow charts or diagrams; Arrangements, e.g. comprising controlling means
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
- B01F27/05—Stirrers
- B01F27/07—Stirrers characterised by their mounting on the shaft
- B01F27/072—Stirrers characterised by their mounting on the shaft characterised by the disposition of the stirrers with respect to the rotating axis
- B01F27/0723—Stirrers characterised by their mounting on the shaft characterised by the disposition of the stirrers with respect to the rotating axis oblique with respect to the rotating axis
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
- B01F27/05—Stirrers
- B01F27/07—Stirrers characterised by their mounting on the shaft
- B01F27/072—Stirrers characterised by their mounting on the shaft characterised by the disposition of the stirrers with respect to the rotating axis
- B01F27/0726—Stirrers characterised by their mounting on the shaft characterised by the disposition of the stirrers with respect to the rotating axis having stirring elements connected to the stirrer shaft each by a single radial rod, other than open frameworks
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
- B01F27/60—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a horizontal or inclined axis
- B01F27/70—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a horizontal or inclined axis with paddles, blades or arms
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F33/00—Other mixers; Mixing plants; Combinations of mixers
- B01F33/70—Mixers specially adapted for working at sub- or super-atmospheric pressure, e.g. combined with de-foaming
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F35/00—Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
- B01F35/181—Preventing generation of dust or dirt; Sieves; Filters
- B01F35/187—Preventing generation of dust or dirt; Sieves; Filters using filters in mixers, e.g. during venting
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F35/00—Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
- B01F35/71—Feed mechanisms
- B01F35/717—Feed mechanisms characterised by the means for feeding the components to the mixer
- B01F35/718—Feed mechanisms characterised by the means for feeding the components to the mixer using vacuum, under pressure in a closed receptacle or circuit system
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F2101/00—Mixing characterised by the nature of the mixed materials or by the application field
- B01F2101/06—Mixing of food ingredients
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Dairy Products (AREA)
Abstract
Blending the constituent powders for the production of blended powders under unregulated environmental conditions may cause them to disintegrate at a particulate level, and/or may damage their agglomerate structure. Hence disclosed herein a blender in the production of product including a blend of powders, including a milk powder, wherein the blender includes a blending chamber, an agitator disposed within the blending chamber, and an inlet for introduction of powders into the blending chamber, characterised in that an environment-regulating means is associated with the blender via at least one interface point, for regulating the environment inside the blending chamber, wherein the environment-regulating means is configured to regulate the environment inside the blending chamber prior to blending of powders inside the blending chamber. In providing a blender configured to subject the constituent powders to environmental regulation prior to blending, the present invention may help to minimise disintegration or damage to the powders.
Description
The present invention relates to a system and method for the production of blended powders with a
milk powder base. Although not limited to this use, the invention has particular application for the
production of infant formula.
Conventional methods of manufacturing infant formula consist of blending a number of constituent
powders to produce a homogeneous mix beforedeoxidating prior to packaging. These powders may
consist of the individual base ingredients, or of a number of these ingredients which have already
been pre-formulated and spray-dried.
More complex methods involve combining a variety of different milk powders and derivatives. It is
standard practice to add so-called "minor ingredients," or "minors and macros," at this stage (also in
powder form), to complete the formulation.
There is typically no regulation of atmospheric conditions (notably, ambient oxygen levels) during
the manufacturing process. The constituent powders progress through the process in a relatively
exposed and unregulated ambient environment.
Atmospheric regulation only takes place towards the end of the process. Atmospheric regulation
typically consists in removing air under vacuum and restoring atmospheric pressure with a mixture
of carbon dioxide and nitrogen gases. The purpose of this is to achieve substantial "deoxidation",
such that the residual oxygen level is sufficiently low to be suitable to the preservation of the
oxygen-sensitive powders.
Atmospheric regulation may commonly take place immediately prior to the canning stage. This is
referred to in the art as "pre-gassing", and forms part of what is known as "modified atmosphere
packing systems" (MAPS).
A variation of MAPS involves what is known as "post-gassing", wherein atmospheric regulation of
the powder is effected after it is canned but prior to sealing of the can.
This is problematic as certain of the constituent powders are oxygen-sensitive; that is to say,
exposure to oxygen (even for a relatively brief period of time) may be detrimental to the particulate
properties of the powder. Thus a lengthy manufacturing process in exposed atmospheric conditions
can lead to one or more of these constituent powders beginning to disintegrate at a particulate
level.
This may be exacerbated by the blending stage of the manufacturing process. Blending involves
mixing the constituent powders to form a homogenous mass. During this process the powder may
be aerated (also referred to in the art as "fluidised") in the ambient air environment within the
blender chamber, adding to the oxygen exposure of the oxygen-sensitive powders. The dynamism of
the blending process may further exacerbate the effects of this on the powders, potentially
worsening their disintegration on a particulate level.
This exposure to ambient atmospheric conditions throughout the manufacturing process may mean
that the final product is not at its optimum by the time it reaches thede-oxidation and packing
stages.
Paradoxically, the de-oxidation stage itself can compound the problem of powder breakdown. The
product may often be left sitting for considerable periods of time (typically 30 minutes or more) in
exposed atmospheric conditions as it awaits transfer to an appropriate station to undergo one or
more de-oxidation steps.
Another problem with conventional manufacturing methods is that the relative complexity of the
process (i.e. the number of stages the powder must progress through) may mean that the
production plant is physically relatively large. Thus the powder may have to travel a significant way
(typically in the region of 30 to 40 metres) between the start and end of the process.
Powder of this kind is often delicate in nature; its agglomerate structure tends to be prone to
breaking down on impact (which manifests as an increase in bulk density). The integrity of the
agglomerate structure may be critical to the quality of the final product; especially with respect to its
performance when dissolved ("wettability") by the end consumer. Manufacturers of infant formula
and similar powdered products are aware of the importance of preventing damage to the
agglomerate structure of such powders.
It follows that the more stages are involved in the manufacturing process, the greater may be the
risk and extent of damage to the powder as it is subjected to impact forces in transit. This may be
especially an issue in the case of production plants which are arranged in a vertical, or "tower,"
configuration, in which the powder is first transferred by vacuum transport to the top of the tower
and then allowed to pass from one stage to the next under the force of gravity.
This problem may be further exacerbated by the fact that the powder mixture is typically stored in
large "hoppers" while awaiting transfer to a successive stage of the process. A typical batch of infant
formula may include at least several hundred kilograms of powder. Thus the fragile powder risks
being damaged under its own weight as it sits piled up in the hopper, in addition to the effects of the
drop or transit itself. Furthermore, the mass flow dynamics as the hopper is emptied may subject the
powder to yet further forces, risking damage to its agglomerate structure as well as potentially
resulting in dissimilar particle segregation.
Thus it will be appreciated that the various problems posed by conventional infant formula
manufacturing processes are related to each other, and that measures designed to mitigate one
issue may tend to exacerbate others.
In particular, the need to deoxidate the final product entails both additional apparatus (and hence
additional transfer distance of the powder) and also adds to the duration of the manufacturing
process, and hence the time the powder mixture spends exposed to unregulated atmospheric
conditions while also often being subjected to its own weight in a storage hopper or the like.
Additionally, the large amount of apparatus required for conventional manufacturing processes may
entail an environment that is inconvenient to clean and maintain, as well as requiring a relatively
expansive premises and/or building to accommodate the required apparatus.
All references, including any patents or patent applications that may be cited in this specification are
hereby incorporated by reference. No admission is made that any such reference constitutes prior
art. The discussion of the references states what their authors assert, and the applicants reserve the
right to challenge the accuracy and pertinency of the cited documents. It will be clearly understood
that, although a number of prior art publications may be referred to herein, this reference does not
constitute an admission that any of these documents form part of the common general knowledge
in the art, in New Zealand or in any other country.
Unless the context clearly requires otherwise, throughout the description and the claims, the words
"comprise", "comprising", and the like, are to be construed in an inclusive sense as opposed to an
exclusive or exhaustive sense, that is to say, in the sense of "including, but not limited to".
It is an object of the present invention to address the foregoing problems or at the very least to
provide the public with a useful choice.
According to one aspect of the present invention, there is provided a blender for use in the
production of product including a blend of powders, wherein at least one of the powders is a milk
powder, wherein the blender includes:
a blending chamber;
an agitator disposed within the blending chamber; and
an inlet for introduction of powders into the blending chamber
characterised in that
an environment-regulating means is associated with the blender via at least one interface point, for
regulating the environment inside the blending chamber, wherein the environment-regulating
means is configured to regulate the environment inside the blending chamber prior to blending of
powders inside the blending chamber.
According to another aspect of the present invention, there is provided a system for the production
of product including a blend of powders, wherein at least one of the powders is a milk powder,
wherein the system includes:
a blender, wherein the blender includes:
a blending chamber;
an agitator disposed within the blending chamber; and
an inlet for introduction of powders into the blending chamber; environment-regulating means associated with the blender via at least one interface point, for regulating the environment inside the blending chamber characterised in that the environment-regulating means is configured to regulate the environment inside the blending chamber prior to blending of powders inside the blending chamber.
According to yet another aspect of the present invention, there is provided a method for the
production of product including a blend of powders, wherein at least one of the powders is a milk
powder, using the system substantially as described above, wherein the method includes the steps
of:
a) introducing powders to be blended into a blending chamber of a blender;
b) regulating the environment inside the blending chamber; and then
c) blending the powders inside the blending chamber.
According to yet another aspect of the present invention, there is provided an apparatus for use in
the introduction of powders into a blending chamber of a blender, wherein the apparatus includes:
a filter associated with the blender, wherein the filter includes:
a main compartment;
an extraction pipe;
a plurality of filter surfaces disposed within the main compartment;
a gas feed pipe connected to the main compartment; and
a feedback pipe.
According to yet another aspect of the present invention, there is provided a blender for use in the
production of product including a blend of powders, wherein the blender includes:
a blending chamber;
an agitator disposed within the blending chamber; and
an inlet for powders to be introduced into the blending chamber via a supply line
characterised in that
a filter is associated with the blender, the filter including a main compartment; an extraction pipe; a
plurality of filter surfaces disposed within the main compartment; a gas feed pipe; and a feedback
pipe.
The present invention provides a system and method for manufacturing product including a blend of
powders. In some embodiments of the invention, at least one of the powders is a milk powder. The
invention is intended in particular for use in a processing facility for the manufacture of such
product.
In exemplary embodiments of the invention, the product includes infant formula but this is not
meant to be limiting. Other products may also be produced using the present invention, such as
protein powder mixes for use in preparing sports supplement drinks.
The system and method disclosed in the present invention allows several of the steps in the
manufacturing and blending process to be undertaken in situ inside the blender, rather than the
powders being transferred to separate apparatus for each step, as may be the case in conventional
manufacturing methods.
Specifically, both the environment-regulation step, as well as blending itself, can be performed
inside the blender; and following blending, the final product can proceed directly to the packaging stage, without the need for any further vacuum ordegassing steps. Furthermore, optional additional steps (such as a pre-blending step, discussed below) can also be performed inside the blender. Thus the powder may only need to be transferred once, as opposed to three or four times. Furthermore, use of the blender for multiple steps in this way may significantly reduce the amount of apparatus required for the manufacturing process.
In its broadest form, according to one aspect of the invention the system includes a blender and
environment-regulating means associated with the blender.
Throughout the present specification, the term "blender" should be understood to mean an
apparatus designed to effect the blending, mixing, or agitation of at least one powder.
The blender should be understood to include a blending chamber with an internally-mounted
agitator for effecting the blending of powders. Throughout the remainder of the specification,
reference to the inside of the blender should be understood to mean the blending chamber.
The blender also includes an inlet for the introduction of powders into the blending chamber. In
preferred embodiments, powders are introduced into the blending chamber via a supply line.
Accordingly, reference will be made throughout the remainder of the present specification to a
supply line. However, this is not intended to be limiting. Preferably, the blender also includes an
outlet via which the product may exit the blending chamber for further processing or packaging.
It will be understood that the blender should be of a kind that is capable of withstanding
substantially vacuum conditions (as will be understood by one skilled in the art) and thus the
blending chamber is appropriately configured to this. Furthermore, the inlet and/or outlet may be
provided with appropriate valves and/or sealing surfaces in order to maintain the desired
environment in the blending chamber.
The blender may be of any make and model configured to effect the blending, mixing or agitation of
powders, as long as it is able, or is modified to be able, to withstand substantially vacuum
conditions. A person skilled in the art will readily envisage apparatus suitable for this purpose.
The inventors have found that the present invention works particularly well with a suitably modified
3500-litre Chem-Plant PHLAUER blender. However, this is not intended to be limiting and persons
skilled in the art will appreciate that other blenders may readily be employed for use in the present
system if appropriately configured or modified.
It will likewise be understood that the system may include just one blender, or a plurality of
blenders. In embodiments including a plurality of blenders, the number and configuration of other
components of the system may need to be adapted appropriately. The skilled person will readily
appreciate appropriate means of achieving this.
For instance, in an exemplary embodiment the system includes two blenders, each having
associated therewith an environment-regulating means. In this embodiment, a single supply line is
configured to introduce powders into both blenders via inlets in the respective blenders. However,
this is not intended to be limiting, and the skilled person will readily appreciate suitable variations on
this configuration; as well as other suitable configurations.
Throughout the present specification, the term "environment-regulating means" should be
understood to mean a means for regulating the atmospheric environment inside the blender such
that the environment established inside the blender is substantially inert with respect to the
powders to be blended therein.
In preferred embodiments, the environment-regulating means may regulate the environment inside
the blender in a preconfigured manner, such as by being automated. However, this is not intended
to be limiting.
In exemplary embodiments of the invention, some or all of the powders to be blended are oxygen
sensitive (such as constituents of infant formula). Accordingly, the environment established inside
the blender may be a "deoxidated" environment. A "deoxidated" environment should be
understood to mean one which is substantially devoid of oxygen, such that the residual oxygen level
is suitable for the preservation of the oxygen-sensitive powders, i.e. wherein the powders do not
disintegrate at a particulate level. However, this is not intended to be limiting.
It will be understood that the atmospheric environment inside the blender is regulated by, firstly,
establishing substantially a vacuum inside the blender (the "vacuum step"); and, secondly,
introducing one or more gases into the blender; such as until standard atmospheric pressure is
substantially restored.
In preferred embodiments, the environment regulating means includes a vacuum pump, as that
term will be understood to one skilled in the art. In use, the vacuum pump operates to establish
substantially a vacuum inside the blender at the vacuum step.
In preferred embodiments, the environment-regulating means also includes or provides for a
compressed gas supply, a pressure-regulating valve and an automated supply valve operatively
connected to the compressed gas supply. These may be communicative, wirelessly or otherwise,
with a pressure transmitter to control the environment within the blender as required.
In preferred embodiments, the vacuum pump may be separate from the other components of the
environment-regulating means. However, this is not intended to be limiting.
In particularly preferred embodiments, a "deep vacuum" is established inside the blender at the
vacuum step (such as in the region of -95 kPa relative to standard atmospheric pressure at sea level).
This is close to the lowest pressure that can be achieved in practical terms; and may result in the
environment inside the blender being deoxidated to the greatest extent possible. For example, residual oxygen levels following the establishment of a "deep vacuum" may be less than 3 per cent.
In particularly preferred embodiments, the residual oxygen levels are less than 1 per cent.
However, this is not intended to be limiting; and higher pressures at the vacuum step (such as in the
region of -60 kPa) may still be functionally effective. Alternatively, or additionally, a higher residual
oxygen level may be permitted at this step, and mitigated by means of further gassing steps
following blending.
It will be understood that the one or more gases introduced into the blender following the vacuum
step are gases which are substantially inert with respect to the powders to be blended; by which is
meant that the powders are substantially non-reactive with, and/or non-sensitive to, the one or
more gases.
In an exemplary embodiment, wherein the powders to be blended are constituents of infant
formula, the one or more gases introduced into the blender may include nitrogen gas, carbon
dioxide gas, or a mixture thereof. An environment is thereby established inside the blender which is
substantially devoid of oxygen, to which some or all of the powders may be sensitive, and in which
pressure has been restored via a gas or gases which are substantially inert with respect to the
powders.
Regulating the environment inside the blender prior to blending means that, during subsequent
blending, the powders are not forced into contact with pockets of gas to which they are sensitive or
reactive. This may significantly mitigate the breaking down of the powders in the course of blending.
Furthermore, it may eliminate the need for the powders to undergo further vacuum anddegassing
steps following blending as the product may already be in a substantially inert environment that
mitigates its deterioration. Accordingly, this may allow the product to proceed from the blender
directly to packaging.
It will be understood that the environment-regulating means is associated with the blender via at
least one interface point (such as in the style of an inlet), via which air is extracted from the blender
at the vacuum step and a gas or gases are subsequently introduced into the blender. In preferred
embodiments, there are a plurality of interface points.
In a particularly preferred embodiment, the vacuum pump of the environment-regulating means is
associated with the blender via a separate interface point from the remaining components of the
environment-regulating means. However, the invention could also be configured to function with a
sole interface point although this may compromise the time required to establish a vacuum inside
the blender, and/or to introduce a gas or gases into the blender.
Preferably, each of the interface points is fitted with appropriate filter/diffusion material to
encourage the uniform dispersion of gas or gases entering the blender. This may help to ensure that
the powders become properly infused with the gas or gases.
Throughout the present specification, reference to "introducing" powders into the blender should
be understood to mean transferring or transporting the powders into the blender via the supply line;
in particular, into the blending chamber of the blender via the inlet.
Preferably, the total required quantities of powders to be blended are prepared and stored at an
external location pending transfer to the blender. The skilled person will appreciate that the
powders to be blended may remain segregated from one another while at the external location.
In a particularly preferred embodiment of the present invention, the total required quantity of base
milk powder is prepared and stored on the one hand; and on the other hand, the total required
quantity of additive powder, being a mixture of minor and macro ingredients and flush powder, is
prepared and stored, and preferably also pre-sifted.
In an exemplary embodiment of the invention, 1300 kg of base milk powder, and at least 200 kg of
additive powder (such as essential elements or the like), are prepared and stored at the external
location. However, this is given by way of example only and is not intended to be limiting. The
amount of powders used will depend on the size of the blenders, whether there is more than one
blender operable at any one time, the overall size of the processing plant in which the system of the
present invention is to be used, and other factors which will be readily appreciated by one skilled in
the art.
In preferred embodiments, powders are transferred to the blender by creating vacuum suction in
the supply line connecting the external location to the blender (this may entail also creating vacuum
suction inside the blender itself). The inventors have found that vacuum suction is a convenient and
effective means of transferring industrial quantities of powders into the blender. This may be
effected using the environment-regulating means associated with the blender. However, this is not
intended to be limiting. The person skilled in the art will envisage alternative methods of transferring
the powders to the blender.
In preferred embodiments, powders are introduced into the blender in a preconfigured sequence
wherein intermediate steps are performed on particular ingredients.
In a preferred embodiment, a "pre-blending" step is effected as part of introducing powders into the
blender. This step consists of introducing additive powder into the blender, further introducing a
small quantity of the base milk powder, and then blending these powders for 60 seconds under
either regulated or unregulated atmospheric conditions. The remainder of the base milk powder is
then added in, and the process continues as described above.
In a particularly preferred embodiment, powders are vacuum-transferred to the blender at the pre
blending step. A vacuum is established inside the blender. When the inlet of the blender is opened,
the vacuum in the blender causes a relatively powerful "suction" effect which may transfer the additive powder and the small quantity of base milk powder to the blender with a high degree of efficiency, and in a manner that results in little or no carry-over powder. In an especially preferred embodiment, the volume of the blender is greater than the total volume of powders used at the pre blending step. This may mean that the "suction" effect is especially effective at transferring the powders to the blender for pre-blending.
In preferred embodiments of the invention, the method is effected using at least two blenders. This
is advantageous as it may be conducive to the continuous production of product by minimising or
eliminating "turn-around time" between successive batches of powders to be blended.
In developing the present invention, the inventors configured two blenders to be connected to the
external location by a single set of supply lines, according to the configuration described above.
Once introduction of the powders into the first blender was complete, introduction of powders into
the second blender could commence while environment-regulation and blending (as well as
subsequent stages of the process, such as packing/canning of the product) were in progress in the
first blender. That is, the process could be 'staggered', resulting in superior production efficiency.
According to another aspect of the invention, there is provided an apparatus configured for use in
the introduction of powders into a blender, the apparatus including a filter associated with the
blender.
It will be understood that the blender may be substantially as described above. However, this is not
intended to be limiting and the skilled person will appreciate that the apparatus may also have
application with other types and/or configurations of blender.
The filter is configured to capture "carry-over" powder; that is to say, powder that has not properly
separated out. This should be understood to mean 'fine' powder that has been retained in the air
stream during introduction into the blender and hence has not successfully settled in the blender.
Powder that has not properly separated out may compromise its ability to achieve a homogenous
mix with other constituent powders during blending. In preferred embodiments, the blender may
include weighing paraphernalia such as scales, or "load cells", configured to monitor the mass of
powder that has settled in the blending chamber and hence determine whether carry-over powder
has successfully been captured.
The filter may include a housing or similar structure to contain its various components which shall
now be discussed.
The filter should be understood include a main compartment in which are disposed a plurality of
filter surfaces. In exemplary embodiments, the filter surfaces are pleated. This increases the
available surface area although it should be appreciated that this is not meant to be limiting.
The filter should be understood to include an extraction pipe. The extraction pipe may be connected
to the blender (in particular, to the blending chamber). Alternatively, or additionally, the extraction
pipe may be connected to the supply line, such as at a position proximate the inlet of the blender. In
use, this allows carry-over powder to be extracted from the blender and/or the supply line via the
extraction pipe, and drawn into the main compartment.
In a preferred embodiment, the filter may include more than one extraction pipe. For instance, the
filter may include an extraction pipe connected to the blending chamber, and another extraction
pipe connected to the supply line. However, this is not intended to be limiting.
The filter should further be understood to include a gas feed pipe connected to the main
compartment proximate the pleated filter surfaces.
In preferred embodiments, the filter may also include a collection compartment located on the
opposite side of the pleated filter surfaces from the gas feed pipe.
Finally, the filter should be understood to include a feedback pipe connected to the filter (and
preferably, the collection compartment of the filter). The feedback pipe may connect the filter to the
blender. Alternatively, the feedback pipe may connect the filter to, for example, the external
location where the powders are stored pending transfer to the blender. In some embodiments, the
extraction pipe and the feedback pipe may be provided by the same component. However, this is
not intended to be limiting.
The filter extracts carry-over powder from the blender and/or the supply line via the extraction pipe
and captures it on the pleated filter surfaces. The carry-over powder is subsequently blown off the
filter surfaces by a high-velocity stream of air directed over the filter surfaces via the gas feed pipe
using a "back pulse" system (as will be understood by one skilled in the art) and settles in the
collection compartment. It is then conveyed from the collection compartment via the feedback pipe
using vacuum suction. Depending on the configuration of a given embodiment, the feedback pipe
may deliver the carry-over powder to the blender, or alternatively to the external powder storage
location.
In a particularly preferred embodiment, wherein the filter is used in conjunction with a blender
having an environment-regulating means, the vacuum pump of the environment-regulating means
may be configured to effect the operation of the filter in the manner described above. A vacuum
may be established in the main compartment, after which the main compartment may be allowed to
return to standard atmospheric pressure. This may create a suction effect whereby carry-over
powder is drawn into the main compartment via the extraction pipe. A vacuum may then be created
in the blender, and the blender subsequently allowed to return to standard atmospheric pressure,
resulting in a suction effect that draws the powder from the collection compartment into the
blender via the feedback pipe.
In this embodiment, the system may be configured such that the filter is located between the
blender and the vacuum pump of the environment-regulating means. The vacuum pump may
thereby effect the operation of the filter in the above manner.
In a particularly preferred embodiment, the extraction/feedback pipe of the filter may also serve as
the interface point between the vacuum pump of the environment-regulating means and the
blender.
Furthermore, the system may be configured to selectively establish an "open path" through the
filter, such that the vacuum pump of the environment-regulating means may create a vacuum inside
the blender, both at the filter step and for the purposes of environmental regulation inside the
blender prior to blending, as discussed further above. The skilled person will readily envisage ways in
which the system can be configured to selectively establish an "open path". For instance, selective
connection of the vacuum pump to the filter and/or the blender may be achieved using
appropriately configured valve(s).
However, this is not intended to be limiting.
The inclusion of an apparatus including a filter as herein described may be advantageous. It may
ensure that powder which is transferred from the external location is ultimately introduced into the
blender with a high degree of efficiency and is properly separated out.
Furthermore, the fact that the filter is associated with though distinct from the blender, as opposed
to being located inside it, may mean that the interior surfaces of the blender can be relatively
smooth. Hence the interior of the blender may be devoid of sharp geometry where powder could
accumulate in a manner that could compromise its uniform blending. In embodiments wherein the
blender also includes an environment-regulating means, the smooth interior surfaces of the blender may also enhance the relatively uniform and complete infusion of the powders with inert gas upon introduction of same into the blender.
It will be appreciated that the apparatus may be used in conjunction with the method described
above. In preferred embodiments, the method is effected using two blenders, as discussed above. In
a particularly preferred embodiment of the method, a filter is associated with at least one of the
blenders and is configured to extract carry-over powder (in the manner discussed above) after
introduction of powders into the first blender but before introduction of powders into the second
blender. The filter of the apparatus thereby effectively "flushes" the supply line to help ensure it is
substantially devoid of carry-over powder prior to introduction of powder into the second blender.
The invention has a number of advantages over conventional systems and techniques for producing
blended powders with a milk powder base, including:
• Reduction of exposure to atmospheric oxygen during the manufacturing process of the
blended powder through regulating the atmospheric environment for at least a part of the
process (including, importantly, the blending step), and hence potentially substantial
reduction of powder breakdown due to contact with oxygen;
• Reduction of the distance the powder must travel during the manufacturing process, and
hence potentially substantial reduction of damage to/disintegration of the powder on a
particle level as a result of impact/forces it is subjected to during manufacture;
• Reduction of the amount of equipment required for the manufacturing process, and hence
reduction of operating/maintenance costs as well as of workplace hazards for employees;
• Relatedly, reduction of the size of the manufacturing plant (such as the height of the tower),
entailing lesser building costs.
At the very least, the present invention provides the public with a useful choice.
Figure 1 is a flow chart showing the essential steps of conventional methods of
manufacturing milk powder;
Figure 2 is a flow chart showing one exemplary embodiment of the method disclosed by
the present invention;
Figure 3 is a schematic view showing a conventional blending system used in the
manufacture of blended milk powder;
Figure 4 is a schematic view showing one exemplary embodiment of the blending system
of the present invention for use in the manufacture of blended milk powder;
Figure 5 is a schematic view showing one exemplary embodiment of the blender of the
present invention;
Figure 6 is a schematic view showing an end elevation of the blender of Figure 5;
Figure 7 is a schematic view showing a plan elevation of the blender of Figure 5; and
Figure 8 is a schematic view showing one exemplary embodiment of the filter apparatus
of the present invention.
Figure 1 is a flow chart showing the essential steps involved in conventional methods (generally
indicated by arrow 100) of manufacturing milk powder.
Powders to be blended are firstly introduced into the system at a bag tip stage (101). They are then
vacuum-transferred to a blender (102) for blending. The resulting product is then transferred into a
blender hopper (103), where it sits while awaiting transfer to a sifter stage (104).
Following this, the product is transferred to a pregasser (105), where atmospheric regulation takes
place to ensure the product is in an inert environment pending packing or canning. Finally, the
product is transferred to a can filling station (106).
Thus the powders are transferred into the blender (102) for the blending step, then transferred
again for the pregassing step (105). This adds to both the distance travelled by the powders (and
hence the damaging forces they are subjected to in transit) and the time spent waiting to be
transferred to a successive step. During this delay period the oxygen-sensitive powders sit in
unregulated atmospheric conditions, and in large industrial hoppers which can also expose the
powders to being damaged under their own weight.
Moreover, the blending step (102) itself takes place in unregulated atmospheric conditions, which
forces pockets of air into the oxygen-sensitive powders, and furthermore, causes the powders to
collide with these air pockets in a vigorous way that exacerbates their deterioration.
Turning now to Figure 2, this is a flow chart showing the steps involved in an exemplary embodiment
of the method (generally indicated by arrow 200) of the present invention.
Firstly, powders to be blended are deposited at an external location (201a). They are then
introduced into the system at a bag-tip point (201) and are vacuum-transferred into a blender (202).
The environment inside the blender is then regulated (203a), after which the powders are blended
(203b) inside the blender under regulated environmental conditions. The product is then transferred
from the blender to a sifter (204), and subsequently to a can filling station, all still under regulated
environmental conditions.
Figure 3 is a schematic showing the common features involved in a conventional system (generally
indicated by arrow 300) for the manufacture of milk powder. The powders to be blended are
introduced into the system at a bag-tip point (301). The powder is then vacuum-transferred via a
supply line (304) to the blender (302) where blending takes place under unregulated atmospheric
conditions. The product is then placed in a hopper (302a) while awaiting transfer to a sifter (306).
Finally, it progresses to the pregasser (307) where the environment is regulated by introduction of
inert gases (305) into the pregasser. Finally, the product proceeds to a can-filling station (308).
Figure 4 is a schematic of a preferred embodiment of the disclosed system (generally indicated by
arrow 400). The system comprises a number of valves, discussed below. In their default position, the
valves are closed.
The powders to be blended are introduced into the system at a bag-tip point (401). Although not
shown, the base milk powder is deposited separately from an additive mixture (comprising a mixture
of minor- and macro- ingredients and flush powder).
In the embodiment of Figure 4, a pre-blending step is performed. A combination of the base powder
and the additive mixture is introduced into the system (400) at a bag-tip point (401) and transferred
via a supply line (404) to a first blender (402). Transferring of the powders is achieved by creating a
vacuum in the first blender using the vacuum pump (409) of the environment-regulating means
(generally indicated by arrow 410), the vacuum pump being connected to the system via a vacuum
line (409A).
Valves 420 and 422 on the blender, as well as 426, and 430 associated with the vacuum pump (409)
of the environment-regulating means (410), are open and the vacuum pump establishes a vacuum in
the first blender (402) and supply line (404). Valve 422 is then closed and a valve (401A) associated
with the bag-tip point (401) is opened. This creates a suction effect in the supply line (404) as atmospheric pressure is restored in the first blender (402), causing the additive mixture and base milk powder to be transferred to the first blender.
The powders are then pre-blended under ordinary atmospheric conditions for a relatively short
period of time.
The remainder of the base milk powder is subsequently introduced into the first blender (402) by
means of vacuum transfer, for the purposes of which valves 420, 422, 426 and 430 are again open.
In the embodiment of Figure 4, a filter apparatus (403) having an extraction / feedback pipe (413,
413A, 413B) extracts carry-over powder from the system and delivers it back to the first blender
(402) after the transfer is complete. This ensures that substantially the total amount of powder
introduced into the system is delivered to, and properly settles in, the blender. The blender may be
configured with load cells (not shown) to monitor whether this has occurred.
To extract carry-over powder and deliver it back to the blender, valve 420 is closed, while valves 422,
426 and 430 are open to form an open path through the extraction pipe (413, 413A) to the vacuum
pump (409). The vacuum pump operates to establish a pressure of (in this embodiment) > -10kPa
relative to standard atmospheric pressure. This causes a suction effect that extracts carry-over
powder from the blender (402) and causes it to settle on the filter surfaces (not shown in Figure 4) of
the filter.
Valves 426 and 430 are then closed, isolating the filter apparatus (403) while it is still under low
pressure. Closing valve 426 also means that low pressure is retained in the blender (402), since
valves 420 and 426 to either side of the blender are now closed.
A valve (412) associated with the external environment via a gas feed pipe (411) is then opened,
restoring the filter apparatus (403) to standard atmospheric pressure. Due to the abrupt restoration
of pressure in the filter apparatus, a high-velocity stream of air is directed onto the filter surfaces via the gas feed pipe, causing the carry-over powder to be blown off the filter surfaces and settle in the collection compartment (not labelled in Figure 4) at the bottom of the filter.
Valve 428 is then opened, to establish an open path through the feedback pipe (413, 413B) to the
blender (402). Opening valve 428 has the effect of abruptly restoring the blender to standard
atmospheric pressure. This creates a suction effect that transfers the carry-over powder back to the
blender.
The vacuum pump (409) forms part of the environment-regulating means (410) of the system (400)
according to this embodiment, and is configured to effect operation of the filter apparatus (403) as
described above, as well as to regulate the environment in the blender (402) itself.
After carry-over powder has been transferred to the first blender (402), an open path is established
between the first blender and the vacuum pump (409) by opening valves 422, 426 and 430. The
vacuum pump operates to establish a deep vacuum (such as in the region of -95kPa relative to
standard atmospheric pressure at sea level) inside the first blender for a prescribed soak time.
Pressure in the first blender (402) is then restored by introducing a combination of nitrogen gas and
carbon dioxide gas into the first blender through multiple fluidising points (not shown), using the
compressed gas supply and other components (generally indicated by 405) of the environment
regulating means (410). Once pressure has been restored, the powders are blended in this regulated
atmospheric environment for a prescribed time.
The powder is then discharged from the first blender (402) through a sifter (406); and is transferred
to a buffer hopper (407) to await transfer to a can-filling station (408); all the while being maintained
in environmentally-regulated conditions.
In this embodiment, after transfer of carry-over powder to the first blender (402) has been
completed, the above process begins in respect of a second blender (not shown), the second blender (not shown) likewise having environment-regulating means (not shown) associated therewith and also being associated with the filter apparatus (403). Accordingly, the production process may be "staggered" by utilising two blenders, such that the process begins in the second blender once the supply line (404) is free following introduction of powders into the first blender
(402).
Turning to Figures 5 to 7, these are schematic views of a blender (generally indicated by arrow 500)
according to one exemplary embodiment of the present invention. It will be seen that the blender
includes a blending chamber (501) with an agitator (502) having blades (502a) disposed in the
blending chamber.
The blender (500) also includes an inlet (503) via which powders are introduced into the blending
chamber (501) via a supply line (not shown); as well as an outlet (510) via which the powders are
extracted from the blending chamber following blending. The inlet and outlet are provided with
appropriate sealing means in order that the environment inside the blending chamber may be
regulated.
The blender is associated with a filter (not shown) which in this embodiment includes a pipe (504)
that acts both as the extraction pipe and the feedback pipe, allowing carry-over powder to be
extracted into the filter (not shown) and subsequently delivered back to the blending chamber (501).
In other embodiments not illustrated in Figure 5, a separate extraction pipe may be associated with
the supply line for extracting carry-over powder from the supply line.
The blending chamber (501) is associated with an environment-regulating means that includes a
vacuum pump (not shown). In this embodiment, the vacuum pump (not shown) of the environment
regulating means functions both to establish a vacuum inside the blending chamber and to effect
operation of the filter (not shown). For the former purpose, an "open path" is established through
the filter (not shown), such that the pipe (504) functions as the interface point between the blending chamber and the vacuum pump (not shown), allowing the vacuum pump (not shown) to establish a vacuum in the blending chamber. This is achieved using appropriately-configured valves, as discussed above.
After powders have been introduced into the blending chamber (501), the vacuum pump (not
shown) first establishes a vacuum in the blending chamber through the pipe (504). A mixture of
nitrogen and carbon dioxide gases is then introduced into the blending chamber from a compressed
supply (506) via a fluidiser pipe (507) via a plurality of interface points (508), to restore atmospheric
pressure inside the blending chamber. The interface points are fitted with filter/diffusion material
(not shown) to encourage the uniform dispersion of the inert gas on entering the blending chamber.
Turning now to Figure 8, this is a detailed schematic of an off-board filter apparatus (generally
indicated by arrow 403) according to one exemplary embodiment of the present invention, shown
connected to the blender (402) and vacuum pump (409). The off-board filter apparatus includes a
main compartment (801) in which are located a plurality of pleated filter panels (802). At least one
extraction/feedback pipe (413, 413A, 413B) connects the main compartment to the blender. A gas
feed pipe (411) having a valve (412) is connected to the main compartment proximate the pleated
filter panels. A collection chamber (804) is located on the opposite side of the pleated filter panels
from the gas feed pipe.
By configuring the valves of the system as described above with reference to Figure 4, the carry-over
powder is conveyed to the main compartment (801) via the extraction pipe (413, 413A), and settles
on the pleated filter panels (802). It is then blown off the panels by a high-velocity stream of air
channelled through the gas feed pipe (411), and settles in the collection chamber (804) before being
conveyed to the blender (402) via the feedback pipe (413, 413B).
Reference to any prior art in this specification is not, and should not be taken as, an
acknowledgement or any form of suggestion that that prior art forms part of the common general
knowledge in the field of endeavour in any country in the world.
The invention may also be said broadly to consist in the parts, elements and features referred to or
indicated in the specification of the application, individually or collectively, in any or all combinations
of two or more of said parts, elements or features.
Where in the foregoing description reference has been made to integers or components having
known equivalents thereof, those integers are herein incorporated as if individually set forth.
It should be noted that various changes and modifications to the presently preferred embodiments
described herein will be apparent to those skilled in the art. Such changes and modifications may be
made without departing from the spirit and scope of the invention and without diminishing its
attendant advantages. It is therefore intended that such changes and modifications be included
within the present invention.
The invention may also be said broadly to consist in the parts, elements and features referred to or
indicated in the specification of the application, individually or collectively, in any or all combinations
of two or more of said parts, elements or features.
Aspects of the present invention have been described by way of example only and it should be
appreciated that modifications and additions may be made thereto without departing from the
scope thereof.
1. A method for the production of a milk product from a blend of powders, the method including
the use of a blender which includes:
a blending chamber;
an agitator disposed within the blending chamber;
an inlet for introduction of powders into the blending chamber;
an outlet for product exiting the blending chamber; and
a filter associated with the blender, wherein the filter includes a main compartment, an
extraction pipe, a plurality of filter surfaces disposed within the main compartment, a gas
feed pipe connected to the main compartment, and a feedback pipe;
and wherein
an environment-regulating means is associated with the blender via at least one interface point
for regulating the environment inside the blending chamber, wherein the environment
regulating means is configured to selectively establish substantially adeoxidated environment
inside the blending chamber prior to blending of powders inside the blending chamber, the
method including the steps of:
a) selectively establishing substantially a deoxidated environment inside the blending
chamber of the blender;
b) introducing the powders, wherein one of the powders is a milk powder, to be blended
into the blending chamber;
c) regulating the environment inside the blending chamber; and then
d) blending the powders inside the blending chamber.
Claims (1)
- 2. The method of claim 1, wherein the method includes a preliminary step, prior to step a), of;i) preparing and storing the powders to be blended at an external location; and/orii) pre-sifting at least one of the powders to be blended; and/oriii) introducing a predetermined quantity of the powders to be blended into the blendingchamber and blending the predetermined quantity of powders inside the blending chamberunder unregulated environmental conditions, wherein the predetermined quantity of thepowders is smaller than a total quantity of the powders to be blended.3. The method of either claim 1 or claim 2, wherein the powders are introduced into the blendingchamber by means of vacuum suction.4. The method of any of claims 1 to 4, wherein step a) includes:1) establishing substantially a vacuum condition inside the blending chamber via the at leastone interface point, wherein establishing substantially a vacuum condition includesestablishing a pressure inside the blending chamber of substantially:i) -60kPa relative to standard atmospheric pressure at sea level, via the at least oneinterface point; orii) -95kPa relative to standard atmospheric pressure at sea level, via the at least oneinterface point;and/or2) introducing at least one gas into the blending chamber via the at least one interface pointafter substantially a vacuum condition has been established inside the blending chamber,wherein the at least one gas is substantially inert with respect to the powders to beblended, wherein the at least one gas includes nitrogen gas, carbon dioxide gas, or both.5. The method of claim 4, wherein the at least one gas is introduced into the blending chambervia the at least one interface point until standard atmospheric pressure is substantially restoredinside the blending chamber.6. The method of any one of claims 1 to 5, wherein there is an additional step of directing a streamof gas from the gas feed pipe at the plurality of filter surfaces to blow off any powder thereupon.7. The method of claim 6, wherein the blown off powder is conveyed back to the blender via thefeedback pipe using vacuum suction. 8. The method of any one of claims 1 to 7, wherein the milk product is infant formula.9. A blender when used in the method of producing a milk product from a blend of powders asclaimed in claim 1, wherein the blender includes:a blending chamber;an agitator disposed within the blending chamber;an inlet for introduction of powders into the blending chamber;an outlet for product exiting the blending chamber; anda filter associated with the blender, wherein the filter includes a main compartment, anextraction pipe, a plurality of filter surfaces disposed within the main compartment, a gasfeed pipe connected to the main compartment, and a feedback pipe;and whereinan environment-regulating means is associated with the blender via at least one interface pointfor regulating the environment inside the blending chamber, wherein the environmentregulating means is configured to selectively establish substantially adeoxidated environmentinside the blending chamber prior to blending of powders inside the blending chamber.10. The blender of claim 9, wherein the environment-regulating means includes one or more of: a compressed gas supply; and/or a pressure-regulating valve; and/or a supply valve operatively connected to the compressed gas supply; and/or a pressure transmitter.11. The blender of claim 10, wherein the compressed gas supply includes at least one gas that issubstantially inert with respect to the powders to be blended.12. The blender of claim 11, wherein the compressed gas supply includes nitrogen gas, carbondioxide gas, or both.13. The blender of any one of claims 9 to 12, wherein the plurality of filter surfaces aresubstantially pleated.14. The blender of any one of claims 9 to 13, wherein the gas feed pipe is connected to the maincompartment proximate the plurality of filter surfaces.15. The blender of claim 14, wherein the gas feed pipe is configured to direct a stream of gas atthe plurality of filter surfaces.16. The blender of any one of claims 9 to 15, wherein the filter includes a collection compartment.17. The blender of claim 16, wherein the collection compartment is disposed at a substantiallyopposite side of the main compartment from the gas feed pipe.18. The blender of any one of claims 9 to 17, wherein the filter includes a housing.
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| NZ72379716 | 2016-08-31 | ||
| NZ723797 | 2016-08-31 | ||
| PCT/NZ2017/050112 WO2018044179A1 (en) | 2016-08-31 | 2017-08-31 | Improved system and method for the production of blended powders |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| AU2017320463A1 AU2017320463A1 (en) | 2019-04-18 |
| AU2017320463B2 true AU2017320463B2 (en) | 2022-04-21 |
Family
ID=61309423
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| AU2017320463A Active AU2017320463B2 (en) | 2016-08-31 | 2017-08-31 | Improved system and method for the production of blended powders |
Country Status (4)
| Country | Link |
|---|---|
| EP (1) | EP3506766B1 (en) |
| AU (1) | AU2017320463B2 (en) |
| DK (1) | DK3506766T3 (en) |
| WO (1) | WO2018044179A1 (en) |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3432307A (en) * | 1964-06-17 | 1969-03-11 | Christiaan Marie Van Ginneken | Method and apparatus for preparing a mixed product |
| US5054933A (en) * | 1988-11-07 | 1991-10-08 | Dr. Herfeld Gmbh & Co., Kg | Mixing device with means to introduce and extract gaseous material |
| US5945150A (en) * | 1997-05-24 | 1999-08-31 | Lipp Mischtechnik Gmbh | Method for production of chocolate |
| JP2000176271A (en) * | 1998-12-14 | 2000-06-27 | Okawara Mfg Co Ltd | Stir processing equipment |
| CN201969531U (en) * | 2010-12-24 | 2011-09-14 | 宿迁娃哈哈恒枫食品有限公司 | Automatic powder mixing system |
| CN202346925U (en) * | 2011-12-05 | 2012-07-25 | 山东泰丰源生物科技有限公司 | Powdery fertilizer dust-free production device |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH03188932A (en) * | 1989-12-18 | 1991-08-16 | Sumitomo Metal Ind Ltd | Method for mixing superfine powder |
-
2017
- 2017-08-31 EP EP17847078.7A patent/EP3506766B1/en active Active
- 2017-08-31 AU AU2017320463A patent/AU2017320463B2/en active Active
- 2017-08-31 DK DK17847078.7T patent/DK3506766T3/en active
- 2017-08-31 WO PCT/NZ2017/050112 patent/WO2018044179A1/en not_active Ceased
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3432307A (en) * | 1964-06-17 | 1969-03-11 | Christiaan Marie Van Ginneken | Method and apparatus for preparing a mixed product |
| US5054933A (en) * | 1988-11-07 | 1991-10-08 | Dr. Herfeld Gmbh & Co., Kg | Mixing device with means to introduce and extract gaseous material |
| US5945150A (en) * | 1997-05-24 | 1999-08-31 | Lipp Mischtechnik Gmbh | Method for production of chocolate |
| JP2000176271A (en) * | 1998-12-14 | 2000-06-27 | Okawara Mfg Co Ltd | Stir processing equipment |
| CN201969531U (en) * | 2010-12-24 | 2011-09-14 | 宿迁娃哈哈恒枫食品有限公司 | Automatic powder mixing system |
| CN202346925U (en) * | 2011-12-05 | 2012-07-25 | 山东泰丰源生物科技有限公司 | Powdery fertilizer dust-free production device |
Also Published As
| Publication number | Publication date |
|---|---|
| EP3506766A1 (en) | 2019-07-10 |
| EP3506766A4 (en) | 2020-06-17 |
| AU2017320463A1 (en) | 2019-04-18 |
| WO2018044179A1 (en) | 2018-03-08 |
| DK3506766T3 (en) | 2023-08-07 |
| EP3506766B1 (en) | 2023-05-03 |
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| FGA | Letters patent sealed or granted (standard patent) |